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A Concise Total Synthesis of Amphidinin B
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作者 Dongdong Wu Jinlong Wu Wei-min Dai 《Chinese Journal of Chemistry》 SCIE CAS CSCD 2013年第1期105-110,共6页
A concise total synthesis of amphidinin B, a cytotoxic linear dicarboxylic acid associated with amphidinolide T marine macrolides, has been accomplished from the 19-membered cycloalkene intermediates designed for dive... A concise total synthesis of amphidinin B, a cytotoxic linear dicarboxylic acid associated with amphidinolide T marine macrolides, has been accomplished from the 19-membered cycloalkene intermediates designed for diverted total synthesis of amphidinolide T1 and T3-T5. The lH and 13C NMR spectra of the synthesized amphidinin B in C6D6 and CDC13 were compared with those for the natural and synthetic forms reported in the literature, showing solvent-dependence of the ^1H and ^13C NMR signals of amphidinin B in C6D6 and CDC13. 展开更多
关键词 amphidinin B cycloalkene DIHYDROXYLATION oxidative cleavage total synthesis
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