The reaction between chloranilic acid and water in alcohol was studied spectrophotometrically. The conditions of reaction were investigated in detail. The stable purple complex with an absorption wavelength at 530 nm ...The reaction between chloranilic acid and water in alcohol was studied spectrophotometrically. The conditions of reaction were investigated in detail. The stable purple complex with an absorption wavelength at 530 nm was produced from the reaction between chloranilic acid and water. As a method for determination of H2O, Beer’s law was obeyed in range of 0-6.0 % or 0-8.0 % (V/V) with the detection limit of 0.13 %. The relative standard deviation (RSD) was less than 2 %. The proposed method has been applied to determination of trace amount of water in ethanol, flour and food flavoring, respectively. The recoveries of water in samples were 97~102 %.展开更多
The syntheses, spec(?) complexes are of significance for understanding mechanisms of magnetic interaction between metal ions and the exploitation of the synthesis of molecular magnetic materials. There were a few work...The syntheses, spec(?) complexes are of significance for understanding mechanisms of magnetic interaction between metal ions and the exploitation of the synthesis of molecular magnetic materials. There were a few works reported previously on the syntheses and magnetic in-展开更多
文摘The reaction between chloranilic acid and water in alcohol was studied spectrophotometrically. The conditions of reaction were investigated in detail. The stable purple complex with an absorption wavelength at 530 nm was produced from the reaction between chloranilic acid and water. As a method for determination of H2O, Beer’s law was obeyed in range of 0-6.0 % or 0-8.0 % (V/V) with the detection limit of 0.13 %. The relative standard deviation (RSD) was less than 2 %. The proposed method has been applied to determination of trace amount of water in ethanol, flour and food flavoring, respectively. The recoveries of water in samples were 97~102 %.
基金Supported by the National Natural Science Foundation of China
文摘The syntheses, spec(?) complexes are of significance for understanding mechanisms of magnetic interaction between metal ions and the exploitation of the synthesis of molecular magnetic materials. There were a few works reported previously on the syntheses and magnetic in-