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Analysis for the Defect of Chromatogram in 35kv Oil-immersed Electric Reactor
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作者 Yongdong Li Qingda Meng +2 位作者 Zheyuan Zhao Po Yang Yuzheng Wang 《Energy and Power Engineering》 2013年第4期838-841,共4页
A defect of chromatogram in a 35kV oil-immersed three-phase one-piece electric reactor in a 500kV substation。The initial analysis suggests that the defect is caused by the loose connection of the iron core magnet shi... A defect of chromatogram in a 35kV oil-immersed three-phase one-piece electric reactor in a 500kV substation。The initial analysis suggests that the defect is caused by the loose connection of the iron core magnet shield (magnet shield layer of iron core or earthling top). Examination of winding DC resistance, DGA and other relevant examinations were carried out to investigate the defect reasons., which is demonstrated by the dismantlement. In-depth study is taken and corresponding prevention measures are put forward in the paper. 展开更多
关键词 OIL-IMMERSED Electric REACTOR chromatogram defect MAGNET SHIELD Layer Partial DISCHARGE
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220kV电流互感器油色谱气体含量超标分析及防范措施 被引量:6
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作者 李明星 唐亮 +1 位作者 陈志勇 岳国良 《河北电力技术》 2008年第1期29-30,共2页
针对河北省南部电网近期发生的多起220 kV电流互感器油色谱气体含量超标的问题,对有缺陷的电流互感器进行解体检查和分析,在此基础上制定了电流互感器设备检测工作的重点及防范措施,以保证220 kV电流互感器在电网中的安全运行。
关键词 电流互感器 油色谱 超标 X蜡 缺陷
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变压器色谱超标缺陷的分析及处理
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作者 安琦 《华北电力技术》 CAS 2007年第A02期74-76,共3页
变压器色谱试验发现故障非常灵敏,但不能确定故障部位。针对秦皇岛发电有限责任公司4号主变压器色谱数值超标的问题,阐述了确定变压器缺陷部位的试验方法及缺陷的处理方法。
关键词 变压器 色谱 缺陷
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Separating Overlapped Peaks of SF6 Decomposed Products Based on Iterative Curve-fitting Method
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作者 ZHANG Xiao-xing XIE Yan-bin YAO Yao TANG Ju REN Jiang-bo 《高电压技术》 EI CAS CSCD 北大核心 2008年第12期2708-2712,共5页
The SF6 decomposed products are very alike,so the peaks of the SF6 decomposed products are overlapped.It make us hard to quantitatively calculate.This paper introduced a method to separate the overlapped chromatogram ... The SF6 decomposed products are very alike,so the peaks of the SF6 decomposed products are overlapped.It make us hard to quantitatively calculate.This paper introduced a method to separate the overlapped chromatogram peaks with iterative curve-fitting and Gauss function,and deduced the formula of the iterative curve-fitting;provided a method to calculate the initial value of the peaks intensity and width by iterative formula,and confirm the final peaks intensity and width to separate the overlapped signals.By the analysis of the real chromatogram data,it proved the validity of this method on the main components used in distinguishing the GIS internal defects.This method overcomes the influence of SF6 peak to the other thin concentration peaks,so it can be used in the study of the quantitative analysis of the decomposed products on different failures and different voltages. 展开更多
关键词 曲线拟合法 SF6分解组分 重叠色谱峰 分离 高斯函数
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银翘散煎剂与5种银翘解毒成药HPLC特征图谱的比较研究 被引量:11
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作者 贺倩 黄宝明 +5 位作者 陈威 叶炳皇 童国勇 卢文彪 赖小平 张军 《中药新药与临床药理》 CAS CSCD 北大核心 2012年第3期303-307,共5页
目的比较银翘散煎剂与5种相关成药(银翘解毒颗粒、银翘解毒片、银翘解毒丸、银翘解毒液、银翘解毒合剂等)的HPLC特征图谱、日服用生药及指标成分量的差异。方法采用HPLC色谱法,phenomenexluna色谱柱(4.6 mm×250 mm,5μm),甲醇-0.1... 目的比较银翘散煎剂与5种相关成药(银翘解毒颗粒、银翘解毒片、银翘解毒丸、银翘解毒液、银翘解毒合剂等)的HPLC特征图谱、日服用生药及指标成分量的差异。方法采用HPLC色谱法,phenomenexluna色谱柱(4.6 mm×250 mm,5μm),甲醇-0.1%磷酸溶液为流动相进行梯度洗脱,检测波长为230 nm,流速为1.0 mL/min。结果得到分离度较好的银翘散煎剂HPLC特征图谱,识别了其中的16个特征峰,上市银翘解毒成药如颗粒剂、片剂、丸剂、口服液、合剂分别保留了煎剂中6和10~13的特征峰,绿原酸、连翘酯苷A、牛蒡苷等指标成分日服用量与煎剂相比均有不同程度的降低。结论银翘散煎剂与5种银翘解毒成药HPLC特征图谱、日服用生药及指标成分量存在较大差异,提示基于临床汤剂研发与生产的成药制剂应关注并克服汤剂成药化缺陷。 展开更多
关键词 银翘散 特征图谱 汤剂成药化缺陷
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