Co5 Sm/Cr bilayer films were deposited on Si and glass slides by means of a Direct-Current (DC) magnetron sputtering system with substrate heating. Magnetic properties measurements show that the sample with glass su...Co5 Sm/Cr bilayer films were deposited on Si and glass slides by means of a Direct-Current (DC) magnetron sputtering system with substrate heating. Magnetic properties measurements show that the sample with glass substrate has a comparatively large coercivity (He = 2 141.20e) with a rela- tively low optimal temperature ( Ts =350 ℃ ). X-ray diffraction patterns indicate that Cr presents a hexagonal-close-packed (hcp) texture on Si, while a body-centered-cubic (bcc) struc- ture on glass substrate, which leads to Cos Sm films having dif- ferent lattice constants on Si and glass substrates. At their opti- mal temperature, the grain size of the sample on glass slide is smaller with its size distribution more uniform. Concurrently, the shape of magnetic domain is more regular and ordered. The value of magnetic switching volume ( V ) for the film on glass is 1.65×10-18 cm3 , smaller than that for films on Si. For the film on glass, the magnetization reversal mechanism is mainly influenced by magnetocrystalline anisotropy, the shape of the crystal grain and the stress in the film.展开更多
RCo5(R=rare earth)sintered magnets have good temperature stability,so it is still widely used in high temperature field.In this paper,by the method of adding liquid phase SmCo1.7 to the main phase,Sm0.7Y0.3Co5 magnet ...RCo5(R=rare earth)sintered magnets have good temperature stability,so it is still widely used in high temperature field.In this paper,by the method of adding liquid phase SmCo1.7 to the main phase,Sm0.7Y0.3Co5 magnet was prepared by traditional powder metallurgical process.The results show the presence of a main phase RCo5,a minor phase R2 Co7,and a R-rich phase in the magnet.Contrasting the results of the XRD(X-ray diffraction)in random and oriented directions,the magnet has a well-aligned(00l)orientated texture,which is consistent with the result of the electron backscattered diffraction(EBSD).The Sm0.7Y0.3Co5 sintered magnet has good magnetic properties as remanence(Br)is 0.96 T,the coercivity(Hcj)is 1201.96 kA·m-1,and maximum magnetic energy product((BH)max)is 175.16 kJ m-3.展开更多
基金supported by National Science Foundation of China(10804026)Natural Science Foundation of Hebei Province(E2010000429)Foundation of Hebei Educational Committee(2006123)
文摘Co5 Sm/Cr bilayer films were deposited on Si and glass slides by means of a Direct-Current (DC) magnetron sputtering system with substrate heating. Magnetic properties measurements show that the sample with glass substrate has a comparatively large coercivity (He = 2 141.20e) with a rela- tively low optimal temperature ( Ts =350 ℃ ). X-ray diffraction patterns indicate that Cr presents a hexagonal-close-packed (hcp) texture on Si, while a body-centered-cubic (bcc) struc- ture on glass substrate, which leads to Cos Sm films having dif- ferent lattice constants on Si and glass substrates. At their opti- mal temperature, the grain size of the sample on glass slide is smaller with its size distribution more uniform. Concurrently, the shape of magnetic domain is more regular and ordered. The value of magnetic switching volume ( V ) for the film on glass is 1.65×10-18 cm3 , smaller than that for films on Si. For the film on glass, the magnetization reversal mechanism is mainly influenced by magnetocrystalline anisotropy, the shape of the crystal grain and the stress in the film.
基金financially supported by the State Key Program of Natural Science Foundation of China(Nos.51331003 and 51871005)the International S&T Cooperation Program of China(No.2015DFG52020)
文摘RCo5(R=rare earth)sintered magnets have good temperature stability,so it is still widely used in high temperature field.In this paper,by the method of adding liquid phase SmCo1.7 to the main phase,Sm0.7Y0.3Co5 magnet was prepared by traditional powder metallurgical process.The results show the presence of a main phase RCo5,a minor phase R2 Co7,and a R-rich phase in the magnet.Contrasting the results of the XRD(X-ray diffraction)in random and oriented directions,the magnet has a well-aligned(00l)orientated texture,which is consistent with the result of the electron backscattered diffraction(EBSD).The Sm0.7Y0.3Co5 sintered magnet has good magnetic properties as remanence(Br)is 0.96 T,the coercivity(Hcj)is 1201.96 kA·m-1,and maximum magnetic energy product((BH)max)is 175.16 kJ m-3.