High-resolution transmission electron microscopy(TEM),X-ray diffractometry(XRD),energy dispersive spectroscopy(EDS)and hardness test were used to study the re-dissolution and re-precipitation behavior of nano-precipit...High-resolution transmission electron microscopy(TEM),X-ray diffractometry(XRD),energy dispersive spectroscopy(EDS)and hardness test were used to study the re-dissolution and re-precipitation behavior of nano-precipitates of the spray-formed fine-grained Al-Cu-Mg alloy during rapid cold stamping deformation.Results show that the extruded Al-Cu-Mg alloy undergoes obvious re-dissolution and re-precipitation during the rapid cold-stamping deformation process.The plasticθ′phase has a slower re-dissolution rate than the brittle S′phase.The long strip-shaped S′phases and the acicularθ′phases in Al-Cu-Mg alloy after three passes of cold stamping basically re-dissolved to form a supersaturated solid solution.A large number of fine granular balanceθphases precipitate after four passes of rapid cold-stamping deformation.Rapid cold stamping deformation causes the S′phase andθ′phase to break and promote the nano-precipitate phases to re-dissolve.The high distortion free energy of the matrix promotes the precipitation of the equilibriumθphase,and the hardness of the alloy obviously increases from HB 55 to HB 125 after the rapid cold stamping process.展开更多
High-angle annular dark-field scanning transmission electron microscopy and selected area electron diffraction techniques were used to study the mechanism that underlies the influence of rapid cold-stamping deformatio...High-angle annular dark-field scanning transmission electron microscopy and selected area electron diffraction techniques were used to study the mechanism that underlies the influence of rapid cold-stamping deformation on the fracture behavior of the elongated nanoprecipitated phase in extruded Al−Cu−Mg alloy.Results show that the interface between the long strip-shaped S′phase and the aluminum matrix in the extruded Al−Cu−Mg alloy is flat and breaks during rapid cold-stamping deformation.The breaking mechanisms are distortion and brittle failure,redissolution,and necking.The breakage of the long strip S′phase increases the contact surface between the S′phase and the aluminum matrix and improves the interfacial distortion energy.This effect accounts for the higher free energy of the S′phase than that of the matrix and creates conditions for the redissolution of solute atoms back into the aluminum matrix.The brittle S′phase produces a resolved step during rapid cold-stamping deformation.This step further accelerates the diffusion of solute atoms and promotes the redissolution of the S′phase.Thus,the S′phase necks and separates,and the long strip-shaped S′phase in the extruded Al−Cu−Mg alloy is broken into a short and thin S′phase.展开更多
Electric product house of magnesium alloy sheet is usually obtained by warm stamping owing to its poor plasticity and formability at room temperature.The formability of AZ31B magnesium alloy sheet can be improved by r...Electric product house of magnesium alloy sheet is usually obtained by warm stamping owing to its poor plasticity and formability at room temperature.The formability of AZ31B magnesium alloy sheet can be improved by repeated unidirectional bending(RUB)process through control of(0002)basal texture.Compared with as-received sheet,the Erichsen value(IE)of the sheet underwent RUB process increases to 5.90 from 3.53 at room temperature.It is also confirmed that cell phone houses could be stamped successfully in crank press with AZ31B magnesium alloy sheets underwent RUB process.It provides an alternative to the electronics industry in the application of magnesium alloys.展开更多
基金Project(2019JJ60050) supported by the Natural Science Foundation of Hunan Province,China
文摘High-resolution transmission electron microscopy(TEM),X-ray diffractometry(XRD),energy dispersive spectroscopy(EDS)and hardness test were used to study the re-dissolution and re-precipitation behavior of nano-precipitates of the spray-formed fine-grained Al-Cu-Mg alloy during rapid cold stamping deformation.Results show that the extruded Al-Cu-Mg alloy undergoes obvious re-dissolution and re-precipitation during the rapid cold-stamping deformation process.The plasticθ′phase has a slower re-dissolution rate than the brittle S′phase.The long strip-shaped S′phases and the acicularθ′phases in Al-Cu-Mg alloy after three passes of cold stamping basically re-dissolved to form a supersaturated solid solution.A large number of fine granular balanceθphases precipitate after four passes of rapid cold-stamping deformation.Rapid cold stamping deformation causes the S′phase andθ′phase to break and promote the nano-precipitate phases to re-dissolve.The high distortion free energy of the matrix promotes the precipitation of the equilibriumθphase,and the hardness of the alloy obviously increases from HB 55 to HB 125 after the rapid cold stamping process.
基金Project(19A131)supported by Key Scientific Research Project of Hunan Province,ChinaProject(2019JJ60050)supported by the Natural Science Foundation of Hunan Province,China。
文摘High-angle annular dark-field scanning transmission electron microscopy and selected area electron diffraction techniques were used to study the mechanism that underlies the influence of rapid cold-stamping deformation on the fracture behavior of the elongated nanoprecipitated phase in extruded Al−Cu−Mg alloy.Results show that the interface between the long strip-shaped S′phase and the aluminum matrix in the extruded Al−Cu−Mg alloy is flat and breaks during rapid cold-stamping deformation.The breaking mechanisms are distortion and brittle failure,redissolution,and necking.The breakage of the long strip S′phase increases the contact surface between the S′phase and the aluminum matrix and improves the interfacial distortion energy.This effect accounts for the higher free energy of the S′phase than that of the matrix and creates conditions for the redissolution of solute atoms back into the aluminum matrix.The brittle S′phase produces a resolved step during rapid cold-stamping deformation.This step further accelerates the diffusion of solute atoms and promotes the redissolution of the S′phase.Thus,the S′phase necks and separates,and the long strip-shaped S′phase in the extruded Al−Cu−Mg alloy is broken into a short and thin S′phase.
基金Project(50504019)supported by the National Natural Science Foundation of ChinaProject(2008BB4040)supported by the Science Foundation of Chongqing,ChinaProject(2008AA4028)supported by Scientific and Technological Project of Chongqing Science and Technology Commission,China
文摘Electric product house of magnesium alloy sheet is usually obtained by warm stamping owing to its poor plasticity and formability at room temperature.The formability of AZ31B magnesium alloy sheet can be improved by repeated unidirectional bending(RUB)process through control of(0002)basal texture.Compared with as-received sheet,the Erichsen value(IE)of the sheet underwent RUB process increases to 5.90 from 3.53 at room temperature.It is also confirmed that cell phone houses could be stamped successfully in crank press with AZ31B magnesium alloy sheets underwent RUB process.It provides an alternative to the electronics industry in the application of magnesium alloys.