Burning products of TA15 titanium alloy by friction oxygen concentration method

The microstructural characteristics, elemental distribution law and microscopic formation mechanism of the burning products of TA15 titanium alloy were investigated by friction oxygen concentration method, associated with in situ observation, X-ray diffraction(XRD),scanning electron microscopy(SEM) and energy-dispersive spectroscopy(EDS) analyses, providing the thoughts to improve fireproof property. The results show that, when the friction contact pressure(p) is 0.20 MPa and oxygen concentration of premixed air flow(c) is 60 vol%, TA15 titanium alloy produces violent sparks and presents dazzling white light during combustion. The generated products after burning are mainly TiOand small amount of AlOoxides. Four distinct zones form from the combustion surface to the alloy matrix, and they are in the sequence of combustion zone, fusion zone, heat-affected zone and transition zone. Further, combustion zone is composed of TiOand A1203 compounds, containing obvious cracks. In the fusion zone, discontinuous oxygenrich Al-based solid solution forms, and the elemental distribution has strong volatility. In the heat-affected zone,there are abundant of Ti-based solid solution and small amount of Al-and Mo-based solid solution. Transition zone is made of lamellar structure. Two technical approaches are given to prevent oxygen diffusion inside the reaction zone and reaction-affected zone. On the one hand,the content of Al is designed as the upper limit of alloy composition; on the other hand, fireproof coatings are deposited on the surface of the alloy.

Effect of Surface Topography on Stress Concentration Factor

Neuber rule and Arola-Ramulu model are widely used to predict the stress concentration factor of rough specimens. However, the height parameters and effective valley radius used in these two models depend strongly on the resolution of the roughness-measuring instruments and are easily introduce measuring errors. Besides, it is difficult to find a suitable parameter to characterize surface topography to quantitatively describe its effect on stress concentration factor. In order to overcome these disadvantages, profile moments are carried out to characterize surface topography, surface topography is simulated by superposing series of cosine components, the stress concentration factors of different micro cosine-shaped surface topographies are investigated by finite element analysis. In terms of micro cosine-shaped surface topography, an equation using the second profile moment to estimate the stress concentration factor is proposed, predictions for the stress concentration factor using the proposed expression are within 10% error compared with the results of finite element analysis, which are more accurate than other models. Moreover, the proposed equation is applied to the real surface topography machined by turning. Predictions for the stress concentration factor using the proposed expression are within 10% of the maximum stress concentration factors and about 5% of the effective stress concentration factors estimated from the finite element analysis for three levels of turning surface topographies under different simulated scales. The proposed model is feasible in predicting the stress concentration factors of real machined surface topographies.

Red Tide Information Extraction Based on Multi-source Remote Sensing Data in Haizhou Bay

[Objective] The aim was to extract red tide information in Haizhou Bay on the basis of multi-source remote sensing data.[Method] Red tide in Haizhou Bay was studied based on multi-source remote sensing data,such as IRS-P6 data on October 8,2005,Landsat 5-TM data on May 20,2006,MODIS 1B data on October 6,2006 and HY-1B second-grade data on April 22,2009,which were firstly preprocessed through geometric correction,atmospheric correction,image resizing and so on.At the same time,the synchronous environment monitoring data of red tide water were acquired.Then,band ratio method,chlorophyll-a concentration method and secondary filtering method were adopted to extract red tide information.[Result] On October 8,2005,the area of red tide was about 20.0 km2 in Haizhou Bay.There was no red tide in Haizhou bay on May 20,2006.On October 6,2006,large areas of red tide occurred in Haizhou bay,with area of 436.5 km2.On April 22,2009,red tide scattered in Haizhou bay,and its area was about 10.8 km2.[Conclusion] The research would provide technical ideas for the environmental monitoring department of Lianyungang to implement red tide forecast and warning effectively.

Comparative Study of Z N Staining vs. Flurochrome Staining and Impact of Sample Processing on Diagnosis of Tuberculosis from Various Clinical Samples

Background: Tuberculosis is a highly infectious disease and India has the highest burden with it. Diagnosis of tuberculosis in many countries is still dependent on microscopy. Although its sensitivity is low in comparison to culture and molecular methods, its sensitivity can still be improved by using fluorescence staining method and processing of samples by homogenization and concentration method. Material and methods: Samples were collected from all newly registered suspected cases of tuberculosis in tertiary care hospital from outward and indoor department during a period of one year. Smears were prepared for Ziehl Neelsen stain and fluorescence stain both before and after homogenization and concentration procedure by 4% NAOH-2.9% sodium citrate method and results of them were interpreted according to RNTCP criteria for grading of sputum samples. All the samples were cultured in liquid culture MGIT system (Mycobacterial Growth Indicator Tube) and results of microscopy were compared with liquid culture taken as gold standard. Data were analyzed by using SPSS software version 16. Result: 350 samples were collected during study period. Out of 350 samples, 48 samples were positive for M. tuberculosis by MGIT system. In comparison with MGIT system, sensitivity of Z N stain for detection of acid fast bacilli was 77% before decontamination procedure, which was increased up to 85.42% after decontamination and concentration process. Sensitivity of fluroscence stain was 85.42% before processing, which was increased up to 91.67% after processing of samples. Conclusion: Sensitivity of smear microscopy can be enhanced by use of fluroscence microscopy and concentration method.

Detecting sand-dust storms using a wind-profiling radar

Sand-dust storm is a type of disastrous weather, typically occurring in arid and semi-arid climates. This study selected a region in the hinterlands of the Taklimakan Desert, called the Tazhong region, as the experimental area to quantitatively estimate the particle concentrations of sand-dust storms using the boundary layer wind-profiling radar. We thoroughly studied the radar echo signals and reflectivity factor features during the sand-dust storms. The results indicate that（1） under sand-dust storm conditions, boundary layer wind-profiling radar cannot capture the complete information regarding horizontal wind velocity and direction, but it can obtain the backscattering intensity of sand-dust storms; and（2） during sand-dust storms particle size distributions in the surface layer closely resemble log-normal distributions, with sand-dust particles sizes of 90–100 μm accounting for the maximum particle probability. Retrieved particle size distributions at heights of 600, 800, and 1000 m follow log-normal distributions, and the expected value of particle diameter decreases gradually with increasing height. From the perspective of orders of magnitude, the retrieved results for particle number concentrations and mass concentrations are consistent with previous aircraft-detected results, indicating that it is basically feasible to use boundary layer wind-profiling radar to quantitatively detect the particle concentrations of dust storms.

Energy-Efficient Deployment of Water Quality Sensor Networks

Water quality sensor networks are promising tools for the exploration of oceans.Some key areas need to be monitored effectively.Water quality sensors are deployed randomly or uniformly,however,and understanding how to deploy sensor nodes reasonably and realize effective monitoring of key areas on the basis of monitoring the whole area is an urgent problem to be solved.Additionally,energy is limited in water quality sensor networks.When moving sensor nodes,we should extend the life cycle of the sensor networks as much as possible.In this study,sensor nodes in non-key monitored areas are moved to key areas.First,we used the concentric circle method to determine the mobile sensor nodes and the target locations.Then,we determined the relationship between the mobile sensor nodes and the target locations according to the energy matrix.Finally,we calculated the shortest moving path according to the Floyd algorithm,which realizes the redeployment of the key monitored area.The simulation results showed that,compared with the method of direct movement,the proposed method can effectively reduce the energy consumption and save the network adjustment time based on the effective coverage of key areas.

Optimization of two-factor(pH and ion concentration)simultaneous selection in HPLC using a statistical method

A computer-assisted method is presented for simultaneous optimization of pH and ion con- centration selection for the optimal separation in reversed-phase HPLC.The method is based on a polynomial estimation from nine preliminary experiments according to two-factor rectangular design. This is followed by a two-dimension computer scanning technique.Resolution is used as the selection criterion.Good agreement was obtained between predicted data and experimental results.

Minimizing stress concentrations around an elliptical hole by concentrated forces acting on the uniaxially loaded plate

When concentrated forces are applied at any points of the outer region of an ellipse in an infinite plate, the complex potentials are determined using the conformal mapping method and Cauchy＇s integral formula. And then, based on the superposition principle, the analyt- ical solutions for stress around an elliptical hole in an infinite plate subjected to a uniform far-field stress and concentrated forces, are obtained. Tangential stress concentration will occur on the hole boundary when only far-field uniform loads are applied. When concen- trated forces are applied in the reversed directions of the uniform loads, tangential stress concentration on the hole boundary can be released significantly. In order to minimize the tangential stress concentration, we need to determine the optimum positions and values of the concentrated forces. Three different optimization methods are applied to achieve this aim. The results show that the tangential stress can be released significantly when the op- timized concentrated forces are applied.

Investigation on the amounts of Na_2CO_3 and sulphur to obtain pure Y_2O_2S and up-conversion luminescence of Y_2O_2S:Er

The process to prepare pure phase of hexagonal Y2O2S was investigated. Effect of mixed flux of Na2CO3 and S amounts was studied. The phase composition and morphology were characterized by X-ray diffraction （XRD） and scanning electron microscopy （SEM）. The results showed that the single phase of Y2O2S with smooth morphology could not be obtained as the molar ratio of Y2O3, Na2CO3 and S was in the range of 1：（0.5-1）：（2-3） until the molar ratio was increased to 1：1.5：4. Different Er3＋ concentration doped Y2O2S：Er powders were prepared with molar ratio of the raw materials 1：1.5：4. The quenching concentration of Er3＋ in Y2O2S was more than 2 mol.%, which was due to the interaction of electric quadrupoles between Er3＋ ions.