An adaptive response compensation technique has been proposed to compensate for the response lag of the constant-current hot-wire anemometer (CCA) by taking advantage of digital signal processing technology. First, we...An adaptive response compensation technique has been proposed to compensate for the response lag of the constant-current hot-wire anemometer (CCA) by taking advantage of digital signal processing technology. First, we have developed a simple response compensation scheme based on a precise theoretical expression for the frequency response of the CCA (Kaifuku et al. 2010, 2011), and verified its effectiveness experimentally for hot-wires of 5 μm, 10 μm and 20 μm in diameter. Then, another novel technique based on a two-sensor probe technique—originally developed for the response compensation of fine-wire thermocouples (Tagawa and Ohta 1997;Tagawa et al. 1998)—has been proposed for estimating thermal time-constants of hot-wires to realize the in-situ response compensation of the CCA. To demonstrate the usefulness of the CCA, we have applied the response compensation schemes to multipoint velocity measure- ment of a turbulent wake flow formed behind a circular cylinder by using a CCA probe consisting of 16 hot-wires, which were driven simultaneously by a very simple constant-current circuit. As a result, the proposed response compensation techniques for the CCA work quite successfully and are capable of improving the response speed of the CCA to obtain reliable measurements comparable to those by the commercially-available constant-temperature hot-wire anemometer (CTA).展开更多
In this article, the block scheme and metrological characteristics of the State primary standard of the mass (molar) fraction and mass (molar) concentration of the component in the liquid and solid substances and mate...In this article, the block scheme and metrological characteristics of the State primary standard of the mass (molar) fraction and mass (molar) concentration of the component in the liquid and solid substances and materials based on coulometric titration GET 176-2010 are given. Primary reference materials certified by coulometric titration in the Ural Scientific and Research Institute for Metrology include eight certified reference materials (CRMs) of pure solid substances (mostly salts of sodium or potassium) and one hydrochloric acid solution CRM. The metrological characteristics of these reference materials and the scheme of their application in titrimetric analysis are shown. The expanded uncertainty of the certified value (mass fraction for the solid substances or molar concentration for the solution) is in the range from 0.018% to 0.05%. Information about two primary reference materials of high purity iron and lead nitrate certified by controlled-potential coulometry with expanded uncertainty from 0.04% to 0.07% is also given.展开更多
建立一种管式炉内燃烧石油焦样品前处理,然后用自动碘量库仑滴定法测定石油焦中总硫含量的方法。探讨了影响实验结果的因素,电解液采用10 m L冰乙酸溶解于250 m L蒸馏水中,避光保存,实验环境温度为20℃以上,电解液中搅拌转子的转速为500...建立一种管式炉内燃烧石油焦样品前处理,然后用自动碘量库仑滴定法测定石油焦中总硫含量的方法。探讨了影响实验结果的因素,电解液采用10 m L冰乙酸溶解于250 m L蒸馏水中,避光保存,实验环境温度为20℃以上,电解液中搅拌转子的转速为500 r/min。在优化的实验条件下,测定结果的相对标准偏差在2.36%~3.94%(n=6)之间,3种石油焦样品加标回收率在82.0%~101.5%之间。该方法可应用于石油焦中总硫含量的测定。展开更多
文摘An adaptive response compensation technique has been proposed to compensate for the response lag of the constant-current hot-wire anemometer (CCA) by taking advantage of digital signal processing technology. First, we have developed a simple response compensation scheme based on a precise theoretical expression for the frequency response of the CCA (Kaifuku et al. 2010, 2011), and verified its effectiveness experimentally for hot-wires of 5 μm, 10 μm and 20 μm in diameter. Then, another novel technique based on a two-sensor probe technique—originally developed for the response compensation of fine-wire thermocouples (Tagawa and Ohta 1997;Tagawa et al. 1998)—has been proposed for estimating thermal time-constants of hot-wires to realize the in-situ response compensation of the CCA. To demonstrate the usefulness of the CCA, we have applied the response compensation schemes to multipoint velocity measure- ment of a turbulent wake flow formed behind a circular cylinder by using a CCA probe consisting of 16 hot-wires, which were driven simultaneously by a very simple constant-current circuit. As a result, the proposed response compensation techniques for the CCA work quite successfully and are capable of improving the response speed of the CCA to obtain reliable measurements comparable to those by the commercially-available constant-temperature hot-wire anemometer (CTA).
文摘In this article, the block scheme and metrological characteristics of the State primary standard of the mass (molar) fraction and mass (molar) concentration of the component in the liquid and solid substances and materials based on coulometric titration GET 176-2010 are given. Primary reference materials certified by coulometric titration in the Ural Scientific and Research Institute for Metrology include eight certified reference materials (CRMs) of pure solid substances (mostly salts of sodium or potassium) and one hydrochloric acid solution CRM. The metrological characteristics of these reference materials and the scheme of their application in titrimetric analysis are shown. The expanded uncertainty of the certified value (mass fraction for the solid substances or molar concentration for the solution) is in the range from 0.018% to 0.05%. Information about two primary reference materials of high purity iron and lead nitrate certified by controlled-potential coulometry with expanded uncertainty from 0.04% to 0.07% is also given.
文摘建立一种管式炉内燃烧石油焦样品前处理,然后用自动碘量库仑滴定法测定石油焦中总硫含量的方法。探讨了影响实验结果的因素,电解液采用10 m L冰乙酸溶解于250 m L蒸馏水中,避光保存,实验环境温度为20℃以上,电解液中搅拌转子的转速为500 r/min。在优化的实验条件下,测定结果的相对标准偏差在2.36%~3.94%(n=6)之间,3种石油焦样品加标回收率在82.0%~101.5%之间。该方法可应用于石油焦中总硫含量的测定。