Magnesium alloys were considered to be used as biodegradable implants due to their biocompatibility,biodegradability and nontoxicity.However,under the simultaneous action of corrosive environment and mechanical loadin...Magnesium alloys were considered to be used as biodegradable implants due to their biocompatibility,biodegradability and nontoxicity.However,under the simultaneous action of corrosive environment and mechanical loading in human body,magnesium alloys are easy to be affected by corrosion fatigue and stress corrosion cracking.In this work,the fatigue behavior of the extruded Mg-Zn-Y-Nd alloy used for vascular stents was studied both in air and in simulated body fluid(SBF).It was revealed that the fatigue limit of as-extruded Mg-Zn-Y-Nd alloy in air is about 65 MPa at 10^7 cycles,while there is no limit in SBF and shows a linear relationship between the fatigue life and stress amplitudes.The fatigue crack source in air was formed by the inclusions and defects.However,the stress corrosion and hydrogen embrittlement are the main reasons for the formation of the fatigue initial crack source in SBF.展开更多
The safety of rail is very important for the development of high speed railway, and it is necessary to investigate the features of inner cracks in rail. In order to obtain the features of Acoustic Emission (AE) sour...The safety of rail is very important for the development of high speed railway, and it is necessary to investigate the features of inner cracks in rail. In order to obtain the features of Acoustic Emission (AE) sources of inner cracks in rail, AE sources with different types, depths and propagation distances are examined for crack in rail. The finite element method is utilized to model the rail with cracks and the results of experiment demonstrate the effectiveness of this model. Wavelet transform and Rayleigh-Lamb equations are utilized to extract the features of crack AE sources. The results illustrate that the intensity ratio among AE modes can identify the AE source types and the AE sources with different frequencies in rail. There are uniform AE mode features existing in the AE signals from AE sources in rail web, however AE signals from AE sources in rail head and rail base have the complex and unstable AE modes. Different AE source types have the different propagation features in rail. It is helpful to understand the rail cracks and detect the rail cracks based on the AE technique.展开更多
Mg-Al-Zn-Ca-Y alloys with excellent ignition and corrosion resistances—termed SEN alloys(where the letters"S,""E,"and"N"stand for stainless,environmentally friendly,and non-flammable,res...Mg-Al-Zn-Ca-Y alloys with excellent ignition and corrosion resistances—termed SEN alloys(where the letters"S,""E,"and"N"stand for stainless,environmentally friendly,and non-flammable,respectively)—have been developed recently.In this study,the microstructure,tensile properties,and high-cycle fatigue properties of an extruded Mg-9.0Al-0.8Zn-0.1Mn-0.3Ca-0.2Y(SEN9)alloy are investigated and compared with those of a commercial Mg-9.0Al-0.8Zn-0.1Mn(AZ91)alloy extruded under the same conditions.Both the extruded SEN9 alloy and the extruded AZ91 alloy have a fully recrystallized structure comprising equiaxed grains,but the former has a smaller average grain size owing to the promoted dynamic recrystallization during extrusion.The extruded AZ91 alloy contains coarse Mg_(17)Al_(12) discontinuous precipitate(DP)bands parallel to the extrusion direction,which are formed during its cool down after extrusion.In contrast,the extruded SEN9 alloy contains relatively fine undissolved Al_(2)Ca,Al_(8)Mn_(4)Y,and Al_(2)Y second-phase particles,which are formed during the solidification stage of the casting process.The tensile strength of the extruded SEN9 alloy,which has finer grains and more abundant particles,is slightly higher than that of the extruded AZ91 alloy.However,the difference in their strengths is relatively small because the stronger solid-solution hardening and precipitation hardening effects in the extruded AZ91alloy offset the stronger grain-boundary hardening and dispersion hardening effects in the extruded SEN9alloy to some extent.The tensile elongation of the extruded AZ91 alloy is significantly lower than that of the extruded SEN9 alloy because the large cracks formed in the DP bands in the former cause its premature fracture.Although the extruded SEN9 alloy has higher tensile properties than the extruded AZ91alloy,the high-cycle fatigue life and fatigue strength of the former are shorter and lower,respectively,than those of the latter.The DP bands in the extruded AZ91 alloy do not act as fatigue crack initiation sites,and therefore,fatigue cracks initiate on the specimen surface at all stress amplitude levels.In contrast,in most of the fatigue-fractured specimens of the extruded SEN9 alloy,fatigue cracks initiate on the undissolved Al_(2)Ca and Al_(2)Y particles present on the surface or subsurface of the specimens because of the high local stress concentration on the particles during cyclic loading.This particle-initiated fatigue fracture eventually decreases the high-cycle fatigue resistance of the extruded SEN9 alloy.展开更多
基金The authors are grateful for the financial support of Key Projects of the Joint Fund of the National Natural Science Foundation of China(No.U1804251)the National Key Research and Development Program of China(No.2018YFC1106703,2017YFB0702504 and 2016YFC1102403).
文摘Magnesium alloys were considered to be used as biodegradable implants due to their biocompatibility,biodegradability and nontoxicity.However,under the simultaneous action of corrosive environment and mechanical loading in human body,magnesium alloys are easy to be affected by corrosion fatigue and stress corrosion cracking.In this work,the fatigue behavior of the extruded Mg-Zn-Y-Nd alloy used for vascular stents was studied both in air and in simulated body fluid(SBF).It was revealed that the fatigue limit of as-extruded Mg-Zn-Y-Nd alloy in air is about 65 MPa at 10^7 cycles,while there is no limit in SBF and shows a linear relationship between the fatigue life and stress amplitudes.The fatigue crack source in air was formed by the inclusions and defects.However,the stress corrosion and hydrogen embrittlement are the main reasons for the formation of the fatigue initial crack source in SBF.
基金supported by the China Scholarship Council,the National Natural Science Foundation of China(61171197,61201307,61371045)the Innovation Funds of Harbin Institute of Technology(Grant IDGA18102011)the Promotive Research Fund for Excellent Young and Middle-Aged Scientisits of Shandong Province(BS2010DX001)
文摘The safety of rail is very important for the development of high speed railway, and it is necessary to investigate the features of inner cracks in rail. In order to obtain the features of Acoustic Emission (AE) sources of inner cracks in rail, AE sources with different types, depths and propagation distances are examined for crack in rail. The finite element method is utilized to model the rail with cracks and the results of experiment demonstrate the effectiveness of this model. Wavelet transform and Rayleigh-Lamb equations are utilized to extract the features of crack AE sources. The results illustrate that the intensity ratio among AE modes can identify the AE source types and the AE sources with different frequencies in rail. There are uniform AE mode features existing in the AE signals from AE sources in rail web, however AE signals from AE sources in rail head and rail base have the complex and unstable AE modes. Different AE source types have the different propagation features in rail. It is helpful to understand the rail cracks and detect the rail cracks based on the AE technique.
基金supported by the National Research Council of Science&Technology(NST)grant(No.CRC-15-06-KIGAM)funded by the Korea government(MSIP)。
文摘Mg-Al-Zn-Ca-Y alloys with excellent ignition and corrosion resistances—termed SEN alloys(where the letters"S,""E,"and"N"stand for stainless,environmentally friendly,and non-flammable,respectively)—have been developed recently.In this study,the microstructure,tensile properties,and high-cycle fatigue properties of an extruded Mg-9.0Al-0.8Zn-0.1Mn-0.3Ca-0.2Y(SEN9)alloy are investigated and compared with those of a commercial Mg-9.0Al-0.8Zn-0.1Mn(AZ91)alloy extruded under the same conditions.Both the extruded SEN9 alloy and the extruded AZ91 alloy have a fully recrystallized structure comprising equiaxed grains,but the former has a smaller average grain size owing to the promoted dynamic recrystallization during extrusion.The extruded AZ91 alloy contains coarse Mg_(17)Al_(12) discontinuous precipitate(DP)bands parallel to the extrusion direction,which are formed during its cool down after extrusion.In contrast,the extruded SEN9 alloy contains relatively fine undissolved Al_(2)Ca,Al_(8)Mn_(4)Y,and Al_(2)Y second-phase particles,which are formed during the solidification stage of the casting process.The tensile strength of the extruded SEN9 alloy,which has finer grains and more abundant particles,is slightly higher than that of the extruded AZ91 alloy.However,the difference in their strengths is relatively small because the stronger solid-solution hardening and precipitation hardening effects in the extruded AZ91alloy offset the stronger grain-boundary hardening and dispersion hardening effects in the extruded SEN9alloy to some extent.The tensile elongation of the extruded AZ91 alloy is significantly lower than that of the extruded SEN9 alloy because the large cracks formed in the DP bands in the former cause its premature fracture.Although the extruded SEN9 alloy has higher tensile properties than the extruded AZ91alloy,the high-cycle fatigue life and fatigue strength of the former are shorter and lower,respectively,than those of the latter.The DP bands in the extruded AZ91 alloy do not act as fatigue crack initiation sites,and therefore,fatigue cracks initiate on the specimen surface at all stress amplitude levels.In contrast,in most of the fatigue-fractured specimens of the extruded SEN9 alloy,fatigue cracks initiate on the undissolved Al_(2)Ca and Al_(2)Y particles present on the surface or subsurface of the specimens because of the high local stress concentration on the particles during cyclic loading.This particle-initiated fatigue fracture eventually decreases the high-cycle fatigue resistance of the extruded SEN9 alloy.