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Cu_(0.4)In(0.4)Zn_(1.2)S_2纳米线的催化生长
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作者 熊志勇 胡建力 +1 位作者 李振松 邹超 《材料科学与工程学报》 CAS CSCD 北大核心 2014年第5期682-685,700,共5页
采用液相法制备了Cu0.4In0.4Zn1.2S2固溶半导体纳米线。对纳米线生长过程的分析表明,纳米线生长遵循溶液-固态-固相机理。前驱体首先受热分解形成Cu1.75S纳米晶,利用其结构中存在的Cu+空位溶解In3+和Zn2+,达到饱和后析出晶体形成Cu0.4In... 采用液相法制备了Cu0.4In0.4Zn1.2S2固溶半导体纳米线。对纳米线生长过程的分析表明,纳米线生长遵循溶液-固态-固相机理。前驱体首先受热分解形成Cu1.75S纳米晶,利用其结构中存在的Cu+空位溶解In3+和Zn2+,达到饱和后析出晶体形成Cu0.4In0.4Zn1.2S2固溶半导体纳米线。X射线衍射(XRD)、扫描电镜(SEM)、透射电镜(TEM)分析表明,纳米线呈曲折Z形,长度为5μm,具有纤锌矿结构。 展开更多
关键词 纳米线 催化 cu0.4in0.4zn1.2s2 硫化亚铜
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Magnetic Properties of NiCuZn Ferrite Thin Films Prepared by the Sol-gel Method
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作者 刘锋 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2007年第3期506-509,共4页
Ni0.4Cu0.2Zn0.4Fe2O4 thin films were fabricated on Si substrates by using the sol-gel method and rapid thermal annealing (RTA), and their magnetic properties and crystalline structures were investigated. The samples... Ni0.4Cu0.2Zn0.4Fe2O4 thin films were fabricated on Si substrates by using the sol-gel method and rapid thermal annealing (RTA), and their magnetic properties and crystalline structures were investigated. The samples calcined at and above 600 ℃ have a single-phase spinel structure and the average grain size of the sample calcined at 600 ℃ is about 20 nm. The initial permeability μi, saturation magnetization M and coercivity H of the samples increase with the increasing calcination temperature. The sample calcined at 600 ℃ exhibits an excellent soft magnetic performance, which has μi=33.97 (10 MHz), Hc=15.62 Oe and Ms=228.877 emu/cm^3. Low-temperature annealing can enhance the magnetic properties of the samples. The work shows that using the sol-gel method in conjunction with RTA is a promising way to fabricate integrated thin-film devices. 展开更多
关键词 Ni0.4Cu0.2Zn0.4Fe2O4 thin films sol-gel-method rapid thermal processing magnetic properties
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Solvothermal Synthesis and Visible Photocatalytic Activity of Zn0.4Cd0.6S/TiO2/Reduced graphene oxide Nanocomposite
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作者 Yongji Shi Botao Sun +1 位作者 Xinwei Wang Deshuang Guo 《Research and Application of Materials Science》 2019年第1期35-38,共4页
Zn0.4Cd0.6S/TiO2/Reduced graphene oxide(Zn0.4Cd0.6S/TiO2/RGO)nano-photocatalyst was synthe-sized by a facile solvothermal method.During the reaction,TiO2 and Zn0.8Cd0.2S nanoparticles were evenly dispersed across the ... Zn0.4Cd0.6S/TiO2/Reduced graphene oxide(Zn0.4Cd0.6S/TiO2/RGO)nano-photocatalyst was synthe-sized by a facile solvothermal method.During the reaction,TiO2 and Zn0.8Cd0.2S nanoparticles were evenly dispersed across the surface of RGO,which enhanced response to visible light.The photocatalytic activity of as-synthesized Zn0.4Cd0.6S/TiO2/RGO nanocomposite was studied by means of degrading methylene blue(MB)through the irradiation of visible light.Compared with other nanocomposites,the Zn0.4Cd0.6S/TiO2/RGO nanocomposite showed the highest photocatalytic degradation efficiency(96%)and high stability,which was 5.4 times of photodegradation efficiency of pure TiO2. 展开更多
关键词 Zn0.4Cd0.6S/TiO2/RGO PHOTOCATALYTIC activity VISIBLE light irradiation
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