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MoS_(2)上Cu_(2)O的担载及催化性能研究 被引量:1
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作者 陈晓伟 刘璐 《哈尔滨师范大学自然科学学报》 CAS 2021年第3期66-70,共5页
采用两步水热法制备了Cu_(2)O/MoS_(2)催化剂,首先,通过水热法获得层状的MoS_(2)纳米片,然后在MoS_(2)纳米片上合成Cu_(2)O纳米颗粒,形成负载型Cu_(2)O/MoS_(2)催化剂.通过X射线衍射(XRD)、扫描电子显微镜(SEM)、透射电子显微镜(TEM)等... 采用两步水热法制备了Cu_(2)O/MoS_(2)催化剂,首先,通过水热法获得层状的MoS_(2)纳米片,然后在MoS_(2)纳米片上合成Cu_(2)O纳米颗粒,形成负载型Cu_(2)O/MoS_(2)催化剂.通过X射线衍射(XRD)、扫描电子显微镜(SEM)、透射电子显微镜(TEM)等手段对催化剂的结构进行表征,并以NaBH4还原对硝基苯酚(4-NP)为探针反应评价其催化性能.研究表明,担载之后,Cu_(2)O纳米粒子均匀分散在MoS_(2)载体表面,粒子尺寸明显减少,由此催化NaBH4还原4-NP的性能也得到了显著改善. 展开更多
关键词 Cu2O/MoS2 复合催化剂 催化 4-NP
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Synthesis and opto-electrical properties of Cu2NiSnS4 nanoparticles using a facile solid-phase process at low temperature
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作者 李士娜 马瑞新 牛建文 《Optoelectronics Letters》 EI 2020年第6期401-404,共4页
Cu_2NiSnS_4 nanoparticles were prepared for the first time using a facile solid-phase process at a temperature of 180 °C. The crystalline structure, morphology and optical properties of the Cu_2NiSnS_4 nanopartic... Cu_2NiSnS_4 nanoparticles were prepared for the first time using a facile solid-phase process at a temperature of 180 °C. The crystalline structure, morphology and optical properties of the Cu_2NiSnS_4 nanoparticles were characterized by means of X-ray diffraction(XRD), field emission scanning electron microscopy(FESEM), transmission electron microscope(TEM) and ultraviolet-visible(UV-vis) spectrophotometer. The band gap and conversion efficiency of Cu_2NiSnS_4 nanoparticles were studied at various temperature. The results showed that the Cu_2NiSnS_4 nanoparticles exhibited an optimum band gap of 1.58 e V and a conversion efficiency of 0.64% at 180 °C, indicating that it maybe be useful in low-cost thin film solar cells. 展开更多
关键词 Synthesis and opto-electrical properties of Cu_2NiSnS_4 nanoparticles using a facile solid-phase process at low temperature
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