Dry wear tests under atmospheric conditions at 25-200 °C and loads of 12.5-300 N were performed for AM60B alloy. The wear rate increases with increasing the load; the mild-to-severe wear transitions occur under t...Dry wear tests under atmospheric conditions at 25-200 °C and loads of 12.5-300 N were performed for AM60B alloy. The wear rate increases with increasing the load; the mild-to-severe wear transitions occur under the loads of 275 N at 25 °C, 150 N at 100 °C and 75 N at 200 °C, respectively. However, as the load is less than 50 N, the wear rate at 200 °C is lower than that at 25 °C or 100 °C. In mild wear regimes, the wear mechanisms can be classified into abrasive wear, oxidation wear and delamination wear. Delamination wear prevailed as the mild-to-severe wear transition starts to occur; the delamination occurs from the inside of matrix. Subsequently, plastic-extrusion wear as severe wear prevails accompanied with the transition. The thick and hard tribo-layer postpones the mild-to-severe wear transition due to restricting the occurrence of massive plastic deformation of worn surfaces.展开更多
The effect of iron content on wear behavior of hypereutectic Al?17Si?2Cu?1Ni alloy produced by rheocasting process was investigated. The dry sliding wear tests were carried out with a pin-on-disk wear tester. The resu...The effect of iron content on wear behavior of hypereutectic Al?17Si?2Cu?1Ni alloy produced by rheocasting process was investigated. The dry sliding wear tests were carried out with a pin-on-disk wear tester. The results show that the wear rate of the rheocast alloy is lower than that of the alloy produced by conventional casting process under the same applied load. The fine particle-likeδ-Al4(Fe,Mn)Si2 and polygonalα-Al15(Fe,Mn)3Si2 phases help to improve the wear resistance of rheocast alloys. As the volume fraction of fine Fe-bearing compounds increases, the wear rate of the rheocast alloy decreases. Moreover, the wear rate of rheocast alloy increases with the increase of applied load from 50 to 200 N. For the rheocast alloy with 3% Fe, oxidation wear is the main mechanism at low applied load (50 N). At higher applied loads, a combination of delamination and oxidation wear is the dominant wear mechanism.展开更多
The microstructure and dry sliding wear behav- ior of cast Al-18 wt% MgaSi in-situ metal matrix com- posite modified by Nd were investigated. Experimental results show that, after introducing a proper amount of Nd, bo...The microstructure and dry sliding wear behav- ior of cast Al-18 wt% MgaSi in-situ metal matrix com- posite modified by Nd were investigated. Experimental results show that, after introducing a proper amount of Nd, both primary and eutectic Mg2Si in the Al-18 wt% Mg2Si composite are well modified. The morphology of primary Mg2Si is changed from irregular or dendritic to polyhedral shape, and its average particle size is signifi- cantly decreased. Moreover, the morphology of the eutectic MgzSi phase is altered from flake-like to very short fibrous or dot-like. The wear rates and friction coefficient of the composites with Nd are lower than those without Nd. Furthermore, the addition of 0.5 wt% Nd changes the wear mechanism of the composite from the combination of abrasive, adhesive, and delamination wear without Nd into a single mild abrasion wear with 0.5 wt% Nd.展开更多
The dry sliding wear behavior of AA6061/ZrB2 in-situ composite prepared by the reaction of inorganic salts K2ZrF6 and KBF4 with molten aluminum was investigated.An attempt was made to develop a mathematical model to p...The dry sliding wear behavior of AA6061/ZrB2 in-situ composite prepared by the reaction of inorganic salts K2ZrF6 and KBF4 with molten aluminum was investigated.An attempt was made to develop a mathematical model to predict the wear rate of AA6061/(0-10%) ZrB2 in-situ composites.Four-factor,five-level central composite rotatable design was used to minimize the number of experiments.The factors considered are sliding velocity,sliding distance,normal load and mass fraction of ZrB2 particles.The effect of these factors on the wear rate of the fabricated composite was analyzed and the predicted trends were discussed by observing the wear surface morphologies.The in-situ formed ZrB2 particles enhance the wear performance of the composite.The wear rate of the composite bears a proportional relationship with the sliding velocity,sliding distance and normal load.展开更多
Al-Si/15%SiCp(volume fraction) composites with different silicon contents were fabricated by spray deposition technique, and typical microstructures of these composites were studied by optical microscopy(OM). Dry slid...Al-Si/15%SiCp(volume fraction) composites with different silicon contents were fabricated by spray deposition technique, and typical microstructures of these composites were studied by optical microscopy(OM). Dry sliding wear tests were carried out using a block-on-ring wear machine to investigate the effect of applied load range of 10-220 N on the wear and friction behavior of these composites sliding against SAE 52100 grade bearing steel. Scanning electron microscopy(SEM) and energy-dispersive X-ray microanalysis(EDAX) were utilized to examine the morphologies of the worn surfaces in order to observe the wear characteristics and investigate the wear mechanism. The results show that the wear behavior of these composites is dependent on the silicon content in the matrix alloy and the applied load. Al-Si/15%SiCp composites with higher silicon content exhibit better wear resistance in the applied load range. Under lower loads, the major wear mechanisms are oxidation wear and abrasive wear for all tested composites. Under higher loads, severe adhesive wear becomes the main wear mechanisms for Al-7Si/15%SiCp and Al-13Si/15%SiCp composites, while Al-20Si/15%SiCp presents a compound wear mechanism, consisting of oxidation, abrasive wear and adhesion wear.展开更多
Al2O3 fiber (Al2O3f) and SiC particle (SiCp) hybrid metal matrix composites (MMCs) were fabricated by squeeze casting method.The tests were carried out using a pin-on-disk friction and wear tester by sliding the...Al2O3 fiber (Al2O3f) and SiC particle (SiCp) hybrid metal matrix composites (MMCs) were fabricated by squeeze casting method.The tests were carried out using a pin-on-disk friction and wear tester by sliding these pin specimens at a constant speed of 0.36 m/s (570 r/min) against a steel counter disk at room temperature,100 C and 150 C,respectively.To observe the wear characteristics and investigate the wear mechanism,the morphologies of the worn surfaces and specific wear rate were analyzed by using scanning electron microscope (SEM) and Arrhenius plots.Moreover,the effects of fiber orientation and hybrid ratio were discussed.展开更多
The corrosion, corrosive wear and dry sliding wear of nanocomposites, are extremely complicated and involve various chemical, physical anbd mechanical factors. The aim of this work is to investigate the effects of nan...The corrosion, corrosive wear and dry sliding wear of nanocomposites, are extremely complicated and involve various chemical, physical anbd mechanical factors. The aim of this work is to investigate the effects of nanosized SiC content on the hardness, dry sliding wear, corrosion and corrosive wear of Al/SiC nanocomposites synthesized by mechanical milling cold pressing and hot extrusion. The corrosion resistance of these composites in 3%NaCl solution was investigated by electrochemical polarization testing and their dry sliding as well as corrosive wear resistance in the same solution was evaluated using a pin-on-disc tester. The microstructures of the samples and their worn surfaces were examined using scanning electron microscopy. It was shown that the dry sliding wear and corrosion resistance of these nanocomposites were improved with the increase of SiC content. It was concluded that due to the lubrication effect of the solution, both the friction coefficient and frictional heat that might soften the material were reduced. In addition, the improved strength of the nanocomposites combined with their better corrosion resistance contributed to their increased corrosive wear resistance, compared with the base alloy. The prominent wear mechanism in the unreinforced alloy was adhesive wear, in the Al/SiC nanocomposites, the wear mechanism changed to abrasive.展开更多
The tribological properties of isostatic graphite and carbon graphite under dry sliding and water lubricated conditions were studied.The friction test was conducted by using a pin-on-disc tribometer.The friction coeff...The tribological properties of isostatic graphite and carbon graphite under dry sliding and water lubricated conditions were studied.The friction test was conducted by using a pin-on-disc tribometer.The friction coefficient and the wear rate were employed to evaluate the tribological performances of the two materials,and wear morphology was used to analyze the wear mechanism.The results show that the friction coefficient of the isostatic graphite is larger than that of the carbon graphite under the dry sliding condition,and the wear rate is lower than that of the carbon graphite.Under the water lubricated condition,the friction coefficients and the wear rates of the isostatic graphite decrease obviously.The main wear form of the isostatic graphite is abrasive wear,while the main wear form of the carbon graphite is spalling wear.Finally,the tribological mechanism of the isostatic graphite under dry sliding and water lubricated conditions were systematically analyzed.展开更多
As-cast samples of the Al-3wt.%Ni-lwt.%Bi alloy resulting from the horizontal directional solidification process were subjected to the micro-abrasive wear test.The effects of the solidification thermal and microstruct...As-cast samples of the Al-3wt.%Ni-lwt.%Bi alloy resulting from the horizontal directional solidification process were subjected to the micro-abrasive wear test.The effects of the solidification thermal and microstructural parameters,such as the growth and cooling rates and the cellular and primary dendritic spacings(VL and TR;λ1 and λc;respectively),were evaluated in the wear resistance of the investigated alloy.The tribological parameters analyzed were the wear volume and rate(Vw and Rw).The solidification experiments and the wear tests were carried out by means of a water-cooled horizontal directional solidification device and a rotary-fixed ball wear machine,respectively.The results show lower Vw and Rw values correspond to finer microstructures and the Vw dependence on λ1 is characterized by an experimental mathematical equation.A better distribution of Bi soft droplets and Al3Ni hard intermetallic particles is observed within the finer interdendritic region and,in consequence,the better wear resistance is achieved in as-cast samples with dendritic morphology rather than cellular morphology.A transition of wear mechanism from adhesive to abrasive is observed.展开更多
Friction and sliding wear behaviour of Ti-B-N coatings against AISI440C steel ba ll and WC-6wt%Co ball were studied by using pin-on-disk tribometer along with mi crostructure characterization using optical microscopy ...Friction and sliding wear behaviour of Ti-B-N coatings against AISI440C steel ba ll and WC-6wt%Co ball were studied by using pin-on-disk tribometer along with mi crostructure characterization using optical microscopy (OM), scanning electron m icroscopy (SEM) and X-ray photoelectron spectroscopy (XPS). It is shown that the wear resistance of film depended on the wear mechanism. In the case of AISI440C steel, adhesive wear were pre-dominant and the wear rate increased sharply to a maximum when N content reach ~38at.%. This might be related to the change of fi lm microstructure and phase configuration, so the least adhesive transfer of tri bo-film was observed. If WC-6wt%Co ball was used, less deformation wear debris w as observed, this was responsible for the rise of wear rate. Despite of differen t wear modes, friction coefficients in both cases were found to depend mainly on the formation and the amount of h-BN phase. Elemental analysis by energy disper sive spectroscopy (EDS) and X-ray photoelectron spectroscopy (XPS) revealed that oxygen participated in the wear behavior by reacting with films to form the deb ris comprised of various types of Ti oxide including TiO, TiO2 and Ti2O3 , which increased wear resistance.展开更多
Tribological behaviours of Ti-6Al-4V alloy pins sliding against GCr15 steel discs over a range of contact pressures (0.33-1.33 MPa) and sliding velocities (30-70 m/s) were investigated using a pin-on-disc tribomet...Tribological behaviours of Ti-6Al-4V alloy pins sliding against GCr15 steel discs over a range of contact pressures (0.33-1.33 MPa) and sliding velocities (30-70 m/s) were investigated using a pin-on-disc tribometer under unlubricated conditions. The wear mechanisms and the wear transition were analyzed based on examinations of worn surfaces using SEM, EDS and XRD. When the velocity increases, the friction coefficient and the wear rate of the Ti-6Al-4V alloy show typical transition features, namely, the critical values of sliding velocities for 0.33 and 0.67 MPa are 60 and 40 m/s, respectively. The experimental results reveal that the tribological behaviours of Ti-6Al-4V alloys are controlled by the thermal-mechanical effects, which connects with the friction heat and hard particles of the pairs. A tribolayer containing mainly Ti oxides and V oxides is formed on the worn surface of Ti-6Al-4V alloy.展开更多
The dry sliding wear and friction behaviors of compacted graphite cast iron (C. G. iron) were analyzed. The influence of the operating conditions (i.e. velocity,pressure), chemical composition and microstructure on th...The dry sliding wear and friction behaviors of compacted graphite cast iron (C. G. iron) were analyzed. The influence of the operating conditions (i.e. velocity,pressure), chemical composition and microstructure on the dry sliding tribological characteristics of the cast iron was studied. The 3-D topographical properties and wear surface temperature characteristics of C. G. iron were discussed. The results suggested that, compared with spheroidal graphite cast iron (S. G. iron) and grey cast iron, C. G. iron has the lowest wear rate,the highest friction coefficient, the lowest attenuation quantity in friction coefficient and is suitable for brake materials. The wear resistance and friction coefficient of C. G. iron can be substantially increased by introducing alloy elements such as phosphorus. The good tribological properties of C. G. iron under dry sliding condition have been further explained from mechanism by analyzing the 3-D surface topography and temperature field of dry sliding surface of specimen.展开更多
At room temperature,dry sliding wear tests were carried out using pin-on-disc test rig,in which the pin is made of vermicular iron and the disc is made of 40 Cr steel.The microstructures of the frictional surfaces for...At room temperature,dry sliding wear tests were carried out using pin-on-disc test rig,in which the pin is made of vermicular iron and the disc is made of 40 Cr steel.The microstructures of the frictional surfaces for the pin specimens were investigated.Under the action of both frictional heat and frictional shearing stress,aplastic deformation layer under the frictional surface is formed.The morphology and properties of the plastic deformation layer depend on specimen material,contact pressure and frictional shearing stress.In the plastic deformation layer,the phosphorous mass percent varies at different depth and results in different hardness.On the outer side of surface,the hardness is the biggest and the phosphorous mass percent is the highest.They become gradually small from outer side to inner side of the surface.展开更多
The effect of grain refiner, Mn and Sn additions on the sliding wear behavior of A356 aluminum alloys was investigated. The microstructure and worn surfaces of the studied alloys were characterized by optical microsc...The effect of grain refiner, Mn and Sn additions on the sliding wear behavior of A356 aluminum alloys was investigated. The microstructure and worn surfaces of the studied alloys were characterized by optical microscopy(OM), scanning electron microscopy(SEM), and transmission electron microscopy(TEM). The experimental results indicate that the alloy refined by Al-5Ti-B alloy exhibits equiaxed α(Al) dendrites and performs better wear resistance compared with the alloy without the grain refiner. Moreover, the addition of Mn can change the β-Al5 Fe Si phase to α-Al(Mn,Fe)Si phase and reduce the possibility of crack formation, thus improving the wear resistance. Sn added to A356 aluminum alloy forms Mg2 Sn precipitates after heat treatment. Therefore, the unrealizable precipitation hardening Mg2 Si phase and the softening β-Sn phase can reduce the hardness of the alloy, and finally reduce the wear resistance.展开更多
Titanium alloys are poor in wear resistance and it is not suitable under sliding conditions even with lubrication because ofits severe adhesive wear tendency.The surface modifications through texturing and surface coa...Titanium alloys are poor in wear resistance and it is not suitable under sliding conditions even with lubrication because ofits severe adhesive wear tendency.The surface modifications through texturing and surface coating were used to enhance the surfaceproperties of the titanium alloy substrate.Hard and wear resistant coatings such as TiAlN and AlCrN were applied over texturedtitanium alloy surfaces with chromium as interlayer.To improve the friction and wear resisting performance of hard coatings further,solid lubricant,molybdenum disulphide(MoS2),was deposited on dimples made over hard coatings.Unidirectional sliding weartests were performed with pin on disc contact geometry,to evaluate the tribological performance of coated substrates.The tests wereperformed under three different normal loads for a period of40min at sliding velocity of2m/s.The tribological behaviours ofmulti-layer coatings such as coating structure,friction coefficient and specific wear rate were investigated and analyzed.The lowerfriction coefficient of approximately0.1was found at the early sliding stage,which reduces the material transfer and increases thewear life.Although,the friction coefficient increased to high values after MoS2coating was partially removed,substrate was stillprotected against wear by underlying hard composite layer.展开更多
A specific revised HFCVD apparatus and a novel process combining HFCVD and polishing technique were presented to deposit the micro-and nano-crystalline multilayered ultra-smooth diamond(USCD) film on the interior-ho...A specific revised HFCVD apparatus and a novel process combining HFCVD and polishing technique were presented to deposit the micro-and nano-crystalline multilayered ultra-smooth diamond(USCD) film on the interior-hole surface of WC-Co drawing dies with aperture ranging from d1.0 mm to 60 mm.Characterization results indicate that the surface roughness values(Ra) in the entry zone,drawing zone and bearing zone of as-fabricated USCD coated drawing die were measured as low as 25.7,23.3 and 25.5 nm,respectively.Furthermore,the friction properties of USCD films were examined in both dry sliding and water-lubricating conditions,and the results show that the USCD film presents much superior friction properties.Its friction coefficients against ball-bearing steel,copper and silicon nitride balls(d4 mm),is always lower than that of microcrystalline diamond(MCD) or WC-Co sample,regardless of the lubricating condition.Meanwhile,it still presents competitive wear resistance with the MCD films.Finally,the working lifetime and performance of as-fabricated USCD coated drawing dies were examined under producing low-carbon steel pipes in dry-sliding and water-lubricating conditions.Under the water-lubricating drawing condition,its production significantly increases by about 20 times compared with the conventional WC-Co drawing dies.展开更多
Tribological behaviour of the die-cast AZ71E magnesium alloy was investigated in an applied load range of 10-50 N at high temperatures under dry sliding conditions using a pin-on-disc wear testing machine. The results...Tribological behaviour of the die-cast AZ71E magnesium alloy was investigated in an applied load range of 10-50 N at high temperatures under dry sliding conditions using a pin-on-disc wear testing machine. The results indicate that the wear rate increases with the increase of applied load and sliding distance, whereas the friction coefficient decreases with the increase of applied load. Scanning electron microscopy and optical microscopy studies on the worn surfaces and sub-surfaces show that the predominant wear mechanism is abrasion at low applied loads. The mild delamination wear accompanying with adhesion wear is the predominant wear mechanism under high applied loads at 150 ℃, whereas the severe delamination and melting wear are the predominant wear mechanisms under high applied load at 200 ℃. An investigation of the microstructure, thermal stability and tensile properties at high temperatures, using the optical microscopy, X-ray diffraction, differential scanning calorimetry, shows that the dominant secondary phase in AZ71E alloy, Al11Ce3, leads to the improvement in the tensile and elongation properties of alloy at high temperatures, which results in the improvement in the anti wear performance.展开更多
In order to improve the wear and corrosion resistance of AZ31 magnesium alloy,a magnetron-sputtered Al layer with a thickness of 11μm was firstly applied on the alloy,and then treated by plasma electrolytic oxidation...In order to improve the wear and corrosion resistance of AZ31 magnesium alloy,a magnetron-sputtered Al layer with a thickness of 11μm was firstly applied on the alloy,and then treated by plasma electrolytic oxidation(PEO)in an aluminate and silicate electrolytes,respectively.The performance of PEO coatings was investigated by dry sliding wear and electrochemical corrosion tests.The aluminate coating exhibits excellent wear resistance under both 10 and 20 N loads.The silicate coating only shows low wear rate under 10 N,but it was destroyed under 20 N.Corrosion tests show that the Al layer after magnetron sputtering treatment alone cannot afford good protection to the Mg substrate.However,the duplex layer of PEO/Al can significantly improve the corrosion resistance of AZ31 alloy.Electrochemical tests show that the aluminate and silicate coatings have corrosion current densities of-1.6×10^(-6) and-1.1×10^(-6) A/cm^(2),respectively,which are two orders lower than that of the un-coated AZ31 alloy.However,immersion tests and electrochemical impedance spectroscopy(EIS)show that the aluminate coating exhibits better long-term corrosion protection than silicate coating.展开更多
The microstructural features and the consequent mechanical properties were characterized in aluminium borate whisker(ABOw)(5, 10 and 15 wt.%) reinforced commercially-pure aluminium composites fabricated by conventiona...The microstructural features and the consequent mechanical properties were characterized in aluminium borate whisker(ABOw)(5, 10 and 15 wt.%) reinforced commercially-pure aluminium composites fabricated by conventional powder metallurgy technique. The aluminium powder and the whisker were effectively blended by a semi-powder metallurgy method. The blended powder mixtures were cold compacted and sintered at 600 ℃. The sintered composites were characterized for microstructural features by optical microscopy(OM), scanning electron microscopy(SEM), energy dispersive spectroscopy(EDS), transmission electron microscopy(TEM) and X-ray diffraction(XRD) analysis. Porosity in the composites with variation in ABOw contents was determined. The effect of variation in content of ABOw on mechanical properties, viz. hardness, bending strength and compressive strength of the composites was evaluated. The dry sliding wear behaviour was evaluated at varying sliding distance at constant loads. Maximum flexural strength of 172 MPa and compressive strength of 324 MPa with improved hardness around HV 40.2 are obtained in composite with 10 wt.% ABOw. Further increase in ABOw content deteriorates the properties. A substantial increase in wear resistance is also observed with 10 wt.% ABOw. The excellent combination of mechanical properties of Al-10 wt.%ABOw composites is attributed to good interfacial bonds, less porosity and uniformity in the microstructure.展开更多
In this study,CoCrFeNiTi0.5Alx high‐entropy alloys were produced by induction melting and their dry sliding wear behavior was examined at different temperatures.In addition to face‐centered cubic(FCC)phases,low amou...In this study,CoCrFeNiTi0.5Alx high‐entropy alloys were produced by induction melting and their dry sliding wear behavior was examined at different temperatures.In addition to face‐centered cubic(FCC)phases,low amounts of a tetragonal phase were detected in the microstructures of alloys without Al and microscratches were formed by wear particles on the worn surfaces of the alloy specimens.Two body‐centered cubic(BCC)phases were detected in the alloy with 0.5Al and a fatigue‐related extrusion wear mechanism was detected on the worn surface.The alloy specimen with a high Al content exhibited the best wear characteristics.No wear tracks were formed in single‐phase BCC intermetallic alloys at room temperature and they exhibited a higher wear strength at high temperatures when compared to other samples.展开更多
基金Project (51071078) supported by the National Natural Science Foundation of ChinaProject (AE201035) supported by the Research Fund of Key Laboratory for Advanced Technology in Environmental Protection of Jiangsu Province, China
文摘Dry wear tests under atmospheric conditions at 25-200 °C and loads of 12.5-300 N were performed for AM60B alloy. The wear rate increases with increasing the load; the mild-to-severe wear transitions occur under the loads of 275 N at 25 °C, 150 N at 100 °C and 75 N at 200 °C, respectively. However, as the load is less than 50 N, the wear rate at 200 °C is lower than that at 25 °C or 100 °C. In mild wear regimes, the wear mechanisms can be classified into abrasive wear, oxidation wear and delamination wear. Delamination wear prevailed as the mild-to-severe wear transition starts to occur; the delamination occurs from the inside of matrix. Subsequently, plastic-extrusion wear as severe wear prevails accompanied with the transition. The thick and hard tribo-layer postpones the mild-to-severe wear transition due to restricting the occurrence of massive plastic deformation of worn surfaces.
基金Project(2015M572135)supported by the China Postdoctoral Science FoundationProject(2012CB619600)supported by the National Basic Research Program of China
文摘The effect of iron content on wear behavior of hypereutectic Al?17Si?2Cu?1Ni alloy produced by rheocasting process was investigated. The dry sliding wear tests were carried out with a pin-on-disk wear tester. The results show that the wear rate of the rheocast alloy is lower than that of the alloy produced by conventional casting process under the same applied load. The fine particle-likeδ-Al4(Fe,Mn)Si2 and polygonalα-Al15(Fe,Mn)3Si2 phases help to improve the wear resistance of rheocast alloys. As the volume fraction of fine Fe-bearing compounds increases, the wear rate of the rheocast alloy decreases. Moreover, the wear rate of rheocast alloy increases with the increase of applied load from 50 to 200 N. For the rheocast alloy with 3% Fe, oxidation wear is the main mechanism at low applied load (50 N). At higher applied loads, a combination of delamination and oxidation wear is the dominant wear mechanism.
基金financially supported by the National Natural Youth Science Foundation of China (No. 50901038)the Key Laboratory Foundation of Liaoning Provincial Committee of Education (Nos. 20060394 and 2009S053)
文摘The microstructure and dry sliding wear behav- ior of cast Al-18 wt% MgaSi in-situ metal matrix com- posite modified by Nd were investigated. Experimental results show that, after introducing a proper amount of Nd, both primary and eutectic Mg2Si in the Al-18 wt% Mg2Si composite are well modified. The morphology of primary Mg2Si is changed from irregular or dendritic to polyhedral shape, and its average particle size is signifi- cantly decreased. Moreover, the morphology of the eutectic MgzSi phase is altered from flake-like to very short fibrous or dot-like. The wear rates and friction coefficient of the composites with Nd are lower than those without Nd. Furthermore, the addition of 0.5 wt% Nd changes the wear mechanism of the composite from the combination of abrasive, adhesive, and delamination wear without Nd into a single mild abrasion wear with 0.5 wt% Nd.
文摘The dry sliding wear behavior of AA6061/ZrB2 in-situ composite prepared by the reaction of inorganic salts K2ZrF6 and KBF4 with molten aluminum was investigated.An attempt was made to develop a mathematical model to predict the wear rate of AA6061/(0-10%) ZrB2 in-situ composites.Four-factor,five-level central composite rotatable design was used to minimize the number of experiments.The factors considered are sliding velocity,sliding distance,normal load and mass fraction of ZrB2 particles.The effect of these factors on the wear rate of the fabricated composite was analyzed and the predicted trends were discussed by observing the wear surface morphologies.The in-situ formed ZrB2 particles enhance the wear performance of the composite.The wear rate of the composite bears a proportional relationship with the sliding velocity,sliding distance and normal load.
基金Project(2013GK3021)supported by the Science and Technology Plan of Hunan Province,ChinaProject supported by Young Teacher Growth Plan of Hunan University,China
文摘Al-Si/15%SiCp(volume fraction) composites with different silicon contents were fabricated by spray deposition technique, and typical microstructures of these composites were studied by optical microscopy(OM). Dry sliding wear tests were carried out using a block-on-ring wear machine to investigate the effect of applied load range of 10-220 N on the wear and friction behavior of these composites sliding against SAE 52100 grade bearing steel. Scanning electron microscopy(SEM) and energy-dispersive X-ray microanalysis(EDAX) were utilized to examine the morphologies of the worn surfaces in order to observe the wear characteristics and investigate the wear mechanism. The results show that the wear behavior of these composites is dependent on the silicon content in the matrix alloy and the applied load. Al-Si/15%SiCp composites with higher silicon content exhibit better wear resistance in the applied load range. Under lower loads, the major wear mechanisms are oxidation wear and abrasive wear for all tested composites. Under higher loads, severe adhesive wear becomes the main wear mechanisms for Al-7Si/15%SiCp and Al-13Si/15%SiCp composites, while Al-20Si/15%SiCp presents a compound wear mechanism, consisting of oxidation, abrasive wear and adhesion wear.
基金supported by Changwon National University in 2010the Korea Research Foundation Grant (KRF-2008-D00005) funded by the Korean Government (MOEHRD Basic Research Promotion Fund)
文摘Al2O3 fiber (Al2O3f) and SiC particle (SiCp) hybrid metal matrix composites (MMCs) were fabricated by squeeze casting method.The tests were carried out using a pin-on-disk friction and wear tester by sliding these pin specimens at a constant speed of 0.36 m/s (570 r/min) against a steel counter disk at room temperature,100 C and 150 C,respectively.To observe the wear characteristics and investigate the wear mechanism,the morphologies of the worn surfaces and specific wear rate were analyzed by using scanning electron microscope (SEM) and Arrhenius plots.Moreover,the effects of fiber orientation and hybrid ratio were discussed.
基金Iranian Nanotechnology Initiative (INI) for finical support of the research work
文摘The corrosion, corrosive wear and dry sliding wear of nanocomposites, are extremely complicated and involve various chemical, physical anbd mechanical factors. The aim of this work is to investigate the effects of nanosized SiC content on the hardness, dry sliding wear, corrosion and corrosive wear of Al/SiC nanocomposites synthesized by mechanical milling cold pressing and hot extrusion. The corrosion resistance of these composites in 3%NaCl solution was investigated by electrochemical polarization testing and their dry sliding as well as corrosive wear resistance in the same solution was evaluated using a pin-on-disc tester. The microstructures of the samples and their worn surfaces were examined using scanning electron microscopy. It was shown that the dry sliding wear and corrosion resistance of these nanocomposites were improved with the increase of SiC content. It was concluded that due to the lubrication effect of the solution, both the friction coefficient and frictional heat that might soften the material were reduced. In addition, the improved strength of the nanocomposites combined with their better corrosion resistance contributed to their increased corrosive wear resistance, compared with the base alloy. The prominent wear mechanism in the unreinforced alloy was adhesive wear, in the Al/SiC nanocomposites, the wear mechanism changed to abrasive.
基金The National Natural Science Foundation of China(No.51635004,11472078)。
文摘The tribological properties of isostatic graphite and carbon graphite under dry sliding and water lubricated conditions were studied.The friction test was conducted by using a pin-on-disc tribometer.The friction coefficient and the wear rate were employed to evaluate the tribological performances of the two materials,and wear morphology was used to analyze the wear mechanism.The results show that the friction coefficient of the isostatic graphite is larger than that of the carbon graphite under the dry sliding condition,and the wear rate is lower than that of the carbon graphite.Under the water lubricated condition,the friction coefficients and the wear rates of the isostatic graphite decrease obviously.The main wear form of the isostatic graphite is abrasive wear,while the main wear form of the carbon graphite is spalling wear.Finally,the tribological mechanism of the isostatic graphite under dry sliding and water lubricated conditions were systematically analyzed.
基金financial support provided by IFPA-Federal Institute of Education, Science and Technology of Pará, UFPA-Federal University of Pará, and CNPq-The Brazilian Research Council (grants 302846/2017-4 and 400634/2016-3)CAPES-Coordenacao de Aperfeicoamento de Pessoal de Nível SuperiorBrasil-Finance Code 001
文摘As-cast samples of the Al-3wt.%Ni-lwt.%Bi alloy resulting from the horizontal directional solidification process were subjected to the micro-abrasive wear test.The effects of the solidification thermal and microstructural parameters,such as the growth and cooling rates and the cellular and primary dendritic spacings(VL and TR;λ1 and λc;respectively),were evaluated in the wear resistance of the investigated alloy.The tribological parameters analyzed were the wear volume and rate(Vw and Rw).The solidification experiments and the wear tests were carried out by means of a water-cooled horizontal directional solidification device and a rotary-fixed ball wear machine,respectively.The results show lower Vw and Rw values correspond to finer microstructures and the Vw dependence on λ1 is characterized by an experimental mathematical equation.A better distribution of Bi soft droplets and Al3Ni hard intermetallic particles is observed within the finer interdendritic region and,in consequence,the better wear resistance is achieved in as-cast samples with dendritic morphology rather than cellular morphology.A transition of wear mechanism from adhesive to abrasive is observed.
文摘Friction and sliding wear behaviour of Ti-B-N coatings against AISI440C steel ba ll and WC-6wt%Co ball were studied by using pin-on-disk tribometer along with mi crostructure characterization using optical microscopy (OM), scanning electron m icroscopy (SEM) and X-ray photoelectron spectroscopy (XPS). It is shown that the wear resistance of film depended on the wear mechanism. In the case of AISI440C steel, adhesive wear were pre-dominant and the wear rate increased sharply to a maximum when N content reach ~38at.%. This might be related to the change of fi lm microstructure and phase configuration, so the least adhesive transfer of tri bo-film was observed. If WC-6wt%Co ball was used, less deformation wear debris w as observed, this was responsible for the rise of wear rate. Despite of differen t wear modes, friction coefficients in both cases were found to depend mainly on the formation and the amount of h-BN phase. Elemental analysis by energy disper sive spectroscopy (EDS) and X-ray photoelectron spectroscopy (XPS) revealed that oxygen participated in the wear behavior by reacting with films to form the deb ris comprised of various types of Ti oxide including TiO, TiO2 and Ti2O3 , which increased wear resistance.
基金the National Natural Science Foundation of China(No.50375046 and No.50432020)
文摘Tribological behaviours of Ti-6Al-4V alloy pins sliding against GCr15 steel discs over a range of contact pressures (0.33-1.33 MPa) and sliding velocities (30-70 m/s) were investigated using a pin-on-disc tribometer under unlubricated conditions. The wear mechanisms and the wear transition were analyzed based on examinations of worn surfaces using SEM, EDS and XRD. When the velocity increases, the friction coefficient and the wear rate of the Ti-6Al-4V alloy show typical transition features, namely, the critical values of sliding velocities for 0.33 and 0.67 MPa are 60 and 40 m/s, respectively. The experimental results reveal that the tribological behaviours of Ti-6Al-4V alloys are controlled by the thermal-mechanical effects, which connects with the friction heat and hard particles of the pairs. A tribolayer containing mainly Ti oxides and V oxides is formed on the worn surface of Ti-6Al-4V alloy.
基金The subject is supported by National Natural Science Fundof China: 50432020 and The Innovation Fund forOutstanding Scholar of Henan Province: 0421000600
文摘The dry sliding wear and friction behaviors of compacted graphite cast iron (C. G. iron) were analyzed. The influence of the operating conditions (i.e. velocity,pressure), chemical composition and microstructure on the dry sliding tribological characteristics of the cast iron was studied. The 3-D topographical properties and wear surface temperature characteristics of C. G. iron were discussed. The results suggested that, compared with spheroidal graphite cast iron (S. G. iron) and grey cast iron, C. G. iron has the lowest wear rate,the highest friction coefficient, the lowest attenuation quantity in friction coefficient and is suitable for brake materials. The wear resistance and friction coefficient of C. G. iron can be substantially increased by introducing alloy elements such as phosphorus. The good tribological properties of C. G. iron under dry sliding condition have been further explained from mechanism by analyzing the 3-D surface topography and temperature field of dry sliding surface of specimen.
基金Item Sponsored by Provincial Outstanding Youth Science Foundation of Henan in China(04120002100)Opening Foundationof State Key Laboratory of Solid Lubrication
文摘At room temperature,dry sliding wear tests were carried out using pin-on-disc test rig,in which the pin is made of vermicular iron and the disc is made of 40 Cr steel.The microstructures of the frictional surfaces for the pin specimens were investigated.Under the action of both frictional heat and frictional shearing stress,aplastic deformation layer under the frictional surface is formed.The morphology and properties of the plastic deformation layer depend on specimen material,contact pressure and frictional shearing stress.In the plastic deformation layer,the phosphorous mass percent varies at different depth and results in different hardness.On the outer side of surface,the hardness is the biggest and the phosphorous mass percent is the highest.They become gradually small from outer side to inner side of the surface.
文摘The effect of grain refiner, Mn and Sn additions on the sliding wear behavior of A356 aluminum alloys was investigated. The microstructure and worn surfaces of the studied alloys were characterized by optical microscopy(OM), scanning electron microscopy(SEM), and transmission electron microscopy(TEM). The experimental results indicate that the alloy refined by Al-5Ti-B alloy exhibits equiaxed α(Al) dendrites and performs better wear resistance compared with the alloy without the grain refiner. Moreover, the addition of Mn can change the β-Al5 Fe Si phase to α-Al(Mn,Fe)Si phase and reduce the possibility of crack formation, thus improving the wear resistance. Sn added to A356 aluminum alloy forms Mg2 Sn precipitates after heat treatment. Therefore, the unrealizable precipitation hardening Mg2 Si phase and the softening β-Sn phase can reduce the hardness of the alloy, and finally reduce the wear resistance.
文摘Titanium alloys are poor in wear resistance and it is not suitable under sliding conditions even with lubrication because ofits severe adhesive wear tendency.The surface modifications through texturing and surface coating were used to enhance the surfaceproperties of the titanium alloy substrate.Hard and wear resistant coatings such as TiAlN and AlCrN were applied over texturedtitanium alloy surfaces with chromium as interlayer.To improve the friction and wear resisting performance of hard coatings further,solid lubricant,molybdenum disulphide(MoS2),was deposited on dimples made over hard coatings.Unidirectional sliding weartests were performed with pin on disc contact geometry,to evaluate the tribological performance of coated substrates.The tests wereperformed under three different normal loads for a period of40min at sliding velocity of2m/s.The tribological behaviours ofmulti-layer coatings such as coating structure,friction coefficient and specific wear rate were investigated and analyzed.The lowerfriction coefficient of approximately0.1was found at the early sliding stage,which reduces the material transfer and increases thewear life.Although,the friction coefficient increased to high values after MoS2coating was partially removed,substrate was stillprotected against wear by underlying hard composite layer.
基金Project(51005154) supported by the National Natural Science Foundation of ChinaProject(12CG11) supported by the Chenguang Program of Shanghai Municipal Education Commission,ChinaProject(201104271) supported by the China Postdoctoral Science Foundation Special Funded Project
文摘A specific revised HFCVD apparatus and a novel process combining HFCVD and polishing technique were presented to deposit the micro-and nano-crystalline multilayered ultra-smooth diamond(USCD) film on the interior-hole surface of WC-Co drawing dies with aperture ranging from d1.0 mm to 60 mm.Characterization results indicate that the surface roughness values(Ra) in the entry zone,drawing zone and bearing zone of as-fabricated USCD coated drawing die were measured as low as 25.7,23.3 and 25.5 nm,respectively.Furthermore,the friction properties of USCD films were examined in both dry sliding and water-lubricating conditions,and the results show that the USCD film presents much superior friction properties.Its friction coefficients against ball-bearing steel,copper and silicon nitride balls(d4 mm),is always lower than that of microcrystalline diamond(MCD) or WC-Co sample,regardless of the lubricating condition.Meanwhile,it still presents competitive wear resistance with the MCD films.Finally,the working lifetime and performance of as-fabricated USCD coated drawing dies were examined under producing low-carbon steel pipes in dry-sliding and water-lubricating conditions.Under the water-lubricating drawing condition,its production significantly increases by about 20 times compared with the conventional WC-Co drawing dies.
基金Project (KLMT201107) supported by the Key Laboratory of Manufacture and Test Techniques for Automobile Parts (Ministry of Education), China
文摘Tribological behaviour of the die-cast AZ71E magnesium alloy was investigated in an applied load range of 10-50 N at high temperatures under dry sliding conditions using a pin-on-disc wear testing machine. The results indicate that the wear rate increases with the increase of applied load and sliding distance, whereas the friction coefficient decreases with the increase of applied load. Scanning electron microscopy and optical microscopy studies on the worn surfaces and sub-surfaces show that the predominant wear mechanism is abrasion at low applied loads. The mild delamination wear accompanying with adhesion wear is the predominant wear mechanism under high applied loads at 150 ℃, whereas the severe delamination and melting wear are the predominant wear mechanisms under high applied load at 200 ℃. An investigation of the microstructure, thermal stability and tensile properties at high temperatures, using the optical microscopy, X-ray diffraction, differential scanning calorimetry, shows that the dominant secondary phase in AZ71E alloy, Al11Ce3, leads to the improvement in the tensile and elongation properties of alloy at high temperatures, which results in the improvement in the anti wear performance.
基金the National Natural Science Foundation of China(No.51671084)。
文摘In order to improve the wear and corrosion resistance of AZ31 magnesium alloy,a magnetron-sputtered Al layer with a thickness of 11μm was firstly applied on the alloy,and then treated by plasma electrolytic oxidation(PEO)in an aluminate and silicate electrolytes,respectively.The performance of PEO coatings was investigated by dry sliding wear and electrochemical corrosion tests.The aluminate coating exhibits excellent wear resistance under both 10 and 20 N loads.The silicate coating only shows low wear rate under 10 N,but it was destroyed under 20 N.Corrosion tests show that the Al layer after magnetron sputtering treatment alone cannot afford good protection to the Mg substrate.However,the duplex layer of PEO/Al can significantly improve the corrosion resistance of AZ31 alloy.Electrochemical tests show that the aluminate and silicate coatings have corrosion current densities of-1.6×10^(-6) and-1.1×10^(-6) A/cm^(2),respectively,which are two orders lower than that of the un-coated AZ31 alloy.However,immersion tests and electrochemical impedance spectroscopy(EIS)show that the aluminate coating exhibits better long-term corrosion protection than silicate coating.
基金support provided by the Central Instrument Facility Centre(CIFC)of IIT(BHU)the Department of Ceramic Engineering especially Advance Refractory Lab(ARL)of IIT(BHU)Varanasi。
文摘The microstructural features and the consequent mechanical properties were characterized in aluminium borate whisker(ABOw)(5, 10 and 15 wt.%) reinforced commercially-pure aluminium composites fabricated by conventional powder metallurgy technique. The aluminium powder and the whisker were effectively blended by a semi-powder metallurgy method. The blended powder mixtures were cold compacted and sintered at 600 ℃. The sintered composites were characterized for microstructural features by optical microscopy(OM), scanning electron microscopy(SEM), energy dispersive spectroscopy(EDS), transmission electron microscopy(TEM) and X-ray diffraction(XRD) analysis. Porosity in the composites with variation in ABOw contents was determined. The effect of variation in content of ABOw on mechanical properties, viz. hardness, bending strength and compressive strength of the composites was evaluated. The dry sliding wear behaviour was evaluated at varying sliding distance at constant loads. Maximum flexural strength of 172 MPa and compressive strength of 324 MPa with improved hardness around HV 40.2 are obtained in composite with 10 wt.% ABOw. Further increase in ABOw content deteriorates the properties. A substantial increase in wear resistance is also observed with 10 wt.% ABOw. The excellent combination of mechanical properties of Al-10 wt.%ABOw composites is attributed to good interfacial bonds, less porosity and uniformity in the microstructure.
文摘In this study,CoCrFeNiTi0.5Alx high‐entropy alloys were produced by induction melting and their dry sliding wear behavior was examined at different temperatures.In addition to face‐centered cubic(FCC)phases,low amounts of a tetragonal phase were detected in the microstructures of alloys without Al and microscratches were formed by wear particles on the worn surfaces of the alloy specimens.Two body‐centered cubic(BCC)phases were detected in the alloy with 0.5Al and a fatigue‐related extrusion wear mechanism was detected on the worn surface.The alloy specimen with a high Al content exhibited the best wear characteristics.No wear tracks were formed in single‐phase BCC intermetallic alloys at room temperature and they exhibited a higher wear strength at high temperatures when compared to other samples.