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Automatic Extraction Method of 3D Feature Guidelines for Complex Cultural Relic Surfaces Based on Point Cloud 被引量:1
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作者 GENG Yuxin ZHONG Ruofei +1 位作者 HUANG Yuqin SUN Haili 《Journal of Geodesy and Geoinformation Science》 CSCD 2024年第1期16-41,共26页
Cultural relics line graphic serves as a crucial form of traditional artifact information documentation,which is a simple and intuitive product with low cost of displaying compared with 3D models.Dimensionality reduct... Cultural relics line graphic serves as a crucial form of traditional artifact information documentation,which is a simple and intuitive product with low cost of displaying compared with 3D models.Dimensionality reduction is undoubtedly necessary for line drawings.However,most existing methods for artifact drawing rely on the principles of orthographic projection that always cannot avoid angle occlusion and data overlapping while the surface of cultural relics is complex.Therefore,conformal mapping was introduced as a dimensionality reduction way to compensate for the limitation of orthographic projection.Based on the given criteria for assessing surface complexity,this paper proposed a three-dimensional feature guideline extraction method for complex cultural relic surfaces.A 2D and 3D combined factor that measured the importance of points on describing surface features,vertex weight,was designed.Then the selection threshold for feature guideline extraction was determined based on the differences between vertex weight and shape index distributions.The feasibility and stability were verified through experiments conducted on real cultural relic surface data.Results demonstrated the ability of the method to address the challenges associated with the automatic generation of line drawings for complex surfaces.The extraction method and the obtained results will be useful for line graphic drawing,displaying and propaganda of cultural relics. 展开更多
关键词 point cloud conformal parameterization vertex weight surface mesh cultural relics feature extraction
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Intelligent extraction of road cracks based on vehicle laser point cloud and panoramic sequence images
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作者 Ming Guo Li Zhu +4 位作者 Ming Huang Jie Ji Xian Ren Yaxuan Wei Chutian Gao 《Journal of Road Engineering》 2024年第1期69-79,共11页
In light of the limited efficacy of conventional methods for identifying pavement cracks and the absence of comprehensive depth and location data in two-dimensional photographs,this study presents an intelligent strat... In light of the limited efficacy of conventional methods for identifying pavement cracks and the absence of comprehensive depth and location data in two-dimensional photographs,this study presents an intelligent strategy for extracting road cracks.This methodology involves the integration of laser point cloud data obtained from a vehicle-mounted system and a panoramic sequence of images.The study employs a vehicle-mounted LiDAR measurement system to acquire laser point cloud and panoramic sequence image data simultaneously.A convolutional neural network is utilized to extract cracks from the panoramic sequence image.The extracted sequence image is then aligned with the laser point cloud,enabling the assignment of RGB information to the vehicle-mounted three dimensional(3D)point cloud and location information to the two dimensional(2D)panoramic image.Additionally,a threshold value is set based on the crack elevation change to extract the aligned roadway point cloud.The three-dimensional data pertaining to the cracks can be acquired.The experimental findings demonstrate that the use of convolutional neural networks has yielded noteworthy outcomes in the extraction of road cracks.The utilization of point cloud and image alignment techniques enables the extraction of precise location data pertaining to road cracks.This approach exhibits superior accuracy when compared to conventional methods.Moreover,it facilitates rapid and accurate identification and localization of road cracks,thereby playing a crucial role in ensuring road maintenance and traffic safety.Consequently,this technique finds extensive application in the domains of intelligent transportation and urbanization development.The technology exhibits significant promise for use in the domains of intelligent transportation and city development. 展开更多
关键词 Road crack extraction Vehicle laser point cloud Panoramic sequence images Convolutional neural network
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基于PointNet++的邻域特征增强点云语义分割方法
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作者 李松 张安思 +1 位作者 伍婕 张保 《激光杂志》 CAS 北大核心 2024年第7期174-179,共6页
随着智能驾驶、机器人导航等以点云为基础的应用蓬勃发展,点云语义分割逐渐成为研究热点。然而,现有的点云语义分割方法存在局部特征提取不充分、特征融合不完整的缺陷。针对这些不足,提出了对应的解决方案。对于局部特征提取不充分的现... 随着智能驾驶、机器人导航等以点云为基础的应用蓬勃发展,点云语义分割逐渐成为研究热点。然而,现有的点云语义分割方法存在局部特征提取不充分、特征融合不完整的缺陷。针对这些不足,提出了对应的解决方案。对于局部特征提取不充分的现象,通过嵌入邻域点的坐标、方向、距离等相关信息去关联邻域点的显式特征。对于特征融合不完整的现象,提出了一种最大池化与自注意力池化相结合的混合池化方法。网络架构基于PointNet++,并结合提出的局部特征提取和融合方法,在S3DIS数据集上的实验结果表明,与基线方法PointNet++相比,各评价指标都有不同程度的提高,证实了新方法的有效性和优越性。 展开更多
关键词 三维点云 语义分割 特征提取 深度学习
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Robust Radiometric Normalization of the near Equatorial Satellite Images Using Feature Extraction and Remote Sensing Analysis 被引量:1
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作者 Hayder Dibs Shattri Mansor +1 位作者 Noordin Ahmad Nadhir Al-Ansari 《Engineering(科研)》 CAS 2023年第2期75-89,共15页
Relative radiometric normalization (RRN) minimizes radiometric differences among images caused by inconsistencies of acquisition conditions rather than changes in surface. Scale invariant feature transform (SIFT) has ... Relative radiometric normalization (RRN) minimizes radiometric differences among images caused by inconsistencies of acquisition conditions rather than changes in surface. Scale invariant feature transform (SIFT) has the ability to automatically extract control points (CPs) and is commonly used for remote sensing images. However, its results are mostly inaccurate and sometimes contain incorrect matching caused by generating a small number of false CP pairs. These CP pairs have high false alarm matching. This paper presents a modified method to improve the performance of SIFT CPs matching by applying sum of absolute difference (SAD) in a different manner for the new optical satellite generation called near-equatorial orbit satellite and multi-sensor images. The proposed method, which has a significantly high rate of correct matches, improves CP matching. The data in this study were obtained from the RazakSAT satellite a new near equatorial satellite system. The proposed method involves six steps: 1) data reduction, 2) applying the SIFT to automatically extract CPs, 3) refining CPs matching by using SAD algorithm with empirical threshold, and 4) calculation of true CPs intensity values over all image’ bands, 5) preforming a linear regression model between the intensity values of CPs locate in reverence and sensed image’ bands, 6) Relative radiometric normalization conducting using regression transformation functions. Different thresholds have experimentally tested and used in conducting this study (50 and 70), by followed the proposed method, and it removed the false extracted SIFT CPs to be from 775, 1125, 883, 804, 883 and 681 false pairs to 342, 424, 547, 706, 547, and 469 corrected and matched pairs, respectively. 展开更多
关键词 Relative Radiometric Normalization Scale Invariant Feature Transform Automatically extraction Control points Sum of Absolute Difference
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Cloud point extraction coupled with HPLC-UV for the determination of phthalate esters in environmental water samples 被引量:24
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作者 WANG Ling JIANG Gui-bin +3 位作者 CAI Ya-qi HE Bin WANG Ya-wei SHEN Da-zhong 《Journal of Environmental Sciences》 SCIE EI CAS CSCD 2007年第7期874-878,共5页
A method based on cloud point extraction was developed to determine phthalate esters including di-ethyl-phthalate (DEP), di- (2-ethylhexyl)-phthalate (DEHP) and di-cyclohexyl-phthalate (DCP) in environmental w... A method based on cloud point extraction was developed to determine phthalate esters including di-ethyl-phthalate (DEP), di- (2-ethylhexyl)-phthalate (DEHP) and di-cyclohexyl-phthalate (DCP) in environmental water samples using high-performance liquid chromatography separation and ultraviolet detection (HPLC-UV). The non-ionic surfactant Triton X-114 was chosen as extraction solvent. The parameters affecting extraction efficiency, such as concentrations of Triton X-114 and Na2SO4, equilibration temperature, equilibration time and centrifugation time were evaluated and optimized. Under the optimum conditions, the method can achieve preconcentration factors of 35, 88, 111 and detection of limits of 2.0, 3.8, 1.0 ng/ml for DEP, DEHP and DCP in 10-ml water sample, respectively. The proposed method was successfully applied to the determination of trace amount of phathalate esters in effluent water of the wastewater treatment plant and the lixivium of plastic fragments. 展开更多
关键词 phthalate esters cloud point extraction Triton X-114 non-ionic surfactant HPLC-UV
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Determination of Ultratrace Amounts of Copper(Ⅱ) in Water Samples by Electrothermal Atomic Absorption Spectrometry After Cloud Point Extraction 被引量:10
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作者 CHEN Jian-guo CHEN neng-wu +2 位作者 CHEN Shao-hong LIN Li ZHONG Ying-ying 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 2007年第2期143-147,共5页
A novel approach was developed for the determination of ultratrace amounts of copper in water samples by using electrothermal atomic absorption spectrometry (ETAAS) after cloud point extraction ( CPE ). 1-( 2-Pyr... A novel approach was developed for the determination of ultratrace amounts of copper in water samples by using electrothermal atomic absorption spectrometry (ETAAS) after cloud point extraction ( CPE ). 1-( 2-Pyridylazo ) -2- naphthol was used as the chelating reagent and Triton X-114 as the mieellar-forming surfactant. CPE was conducted in a pH 8. 0 medium at 40 ℃ for 10 rain. After the separation of the phases by contrifugafion, the surfactant-rieh phase was diluted with 1 mL of a methanol solution of 0. 1 mol/L HNO3. Then 20μL of the diluted surfactant-rieh phase was injected into the graphite furnace for atomization in the absence of any matrix modifier. Various experimental conditions that affect the extraction and atomization processes were optimized. A detection limit of 5 ng/L was obtained after preconeentration. The linear dynamic range of the copper mass concentration was found to be 0-2.0 ng/mL, and the relative standard deviation was found to be less than 3. 1% for a sample containing 1.0 ng/mL Cu ( Ⅱ ). This developed method was successfully applied to the determination of uhratraee amounts of Cu in drinking water, tap water, and seawater samples. 展开更多
关键词 Cloud point extraction Preconeentration Electrothermal atomic absorption spectrometry Copper( Ⅱ) Water analysis
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Cloud point extraction and flame atomic absorption spectrometry analysis of palladium, platinum, and gold ions from industrial polluted soil 被引量:5
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作者 LIAN Yuanpei ZHEN Wei +3 位作者 TAI Zhigang YANG Yaling SONG Jun LI Zonghao 《Rare Metals》 SCIE EI CAS CSCD 2012年第5期512-516,共5页
Cloud point extraction (CPE) with Tergitol TMN-6 was applied for the extraction of trace amounts of palladium (Pd(Ⅱ)), platinum (Pt(Ⅳ)), and gold (Au(Ⅲ)) in the soil of industrial sewage. Ammonium pyrolysine dithio... Cloud point extraction (CPE) with Tergitol TMN-6 was applied for the extraction of trace amounts of palladium (Pd(Ⅱ)), platinum (Pt(Ⅳ)), and gold (Au(Ⅲ)) in the soil of industrial sewage. Ammonium pyrolysine dithiocarbamate (APDC) was adopted as the chelating agent prior to CPE and then was detected by atomic absorption spectrometry (AAS). Different parameters such as the concentration of surfactants, chelating agent and salt, sample pH, equilibration temperature and time, centrifugation time and rates, and the effect of foreign ions were studied. Under optimum conditions, the low limits of detections are 1.4, 2.8 and 1.2 ng·ml^-1 and the enrichment factors are 21, 12, and 24 for Pd(Ⅱ), Pt(Ⅳ), and Au(Ⅲ, respectively. The relative standard deviations vary from 0.6% to 1.0% (n=11). All correlation coefficients of the calibration curves are >0.9960. The proposed method was successfully applied for the determination of Pd(Ⅱ), Pt(Ⅳ), and Au(Ⅲ) in the real soil of industrial sewage samples. 展开更多
关键词 cloud point extraction ammonium pyrolysine dithiocarbamate Tergitol TMN-6 Pd Pt AU atomic absorption spectrometry
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Cloud Point Extraction of Polycyclic Aromatic Hydrocarbons in Aqueous Solution with Silicone Surfactants 被引量:7
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作者 姚炳佳 杨立 +1 位作者 胡琼 Shigendo Akita 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2007年第4期468-473,共6页
Cloud point extraction (CPE) processes with two silicone surfactants, Dow Coming DC-190 and DC-193, were studied as preconcentration and treatment for the water polluted by three trace polycyclic aromatic hydrocarbo... Cloud point extraction (CPE) processes with two silicone surfactants, Dow Coming DC-190 and DC-193, were studied as preconcentration and treatment for the water polluted by three trace polycyclic aromatic hydrocarbons (PAHs): anthracene, phenanthrene and pyrene. For all cases, the volumes of surfactant-rich phase obtained by two silicone surfactants were very small, i.e. a lower water content in the surfactant-rich phase was obtained. For example, less than 3% of the initial solution was obtained in a 1% (by mass) surfactant solution, which was much smaller than that of TX-114 in the same surfactant concentration. And TX-114 is known as a high compact surfactant-rich phase among most nonionic surfactants, thus the comparison showed that an excellent enrichment was ensured in the analysis application by the CPE process with the silicone surfactants, and the lower water content obtained in the surfactant-rich phase is also important in the large scale water treatment. The influences of additives and phase separation methodology on the recovery of PAHs were discussed. Comparing with DC-193, DC-190 has a lower cloud point and a higher recovery (near 100%) of all the three PAHs in same surfactant concentration, which was required for application as a preconcentration process prior to HPLC system. However the DC-190 solution is hard to be phase separated only by heating, whereas DC-193 has a relative higher phase separating speed by heating, but a high cloud point (around 360K) limits its application. Due to the phase separation by heating is the only method of CPE suitable to the large scale water treatment, the mixtures of two silicone surfacrants solutions were investigated in this study. A solution containing 1% of mixed DC-190 and DC-193 (in the ratio of 90 : 10) removed anthracene, phenanthrene and pyrene near 100% with a relative low cloud point and quick phase separating speed. 展开更多
关键词 cloud point extraction silicone surfactant ultraviolet absorbance polycyclic aromatic hydrocarbon water treatment
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Determination of Trace Amounts of Nickel (Ⅱ) by Graphite Furnace Atomic Absorption Spectrometry Coupled with Cloud Point Extraction 被引量:3
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作者 SHAH Syed Mazhar WANG Hao-nan SU Xing-guang 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 2011年第3期366-370,共5页
A new method based on the cloud point extraction(CPE) for separation and preconcentration of nickel(Ⅱ) and its subsequent determination by graphite furnace atomic absorption spectrometry(GFAAS) was proposed, 8-... A new method based on the cloud point extraction(CPE) for separation and preconcentration of nickel(Ⅱ) and its subsequent determination by graphite furnace atomic absorption spectrometry(GFAAS) was proposed, 8-hydroxyquinoline and Triton X-100 were used as the ligand and surfactant respectively. Nickel(Ⅱ) can form a hy-drophobic complex with 8-hydroxyquinoline, the complex can be extracted into the small volume surfactant rich phase at the cloud point temperature(CPT) for GFAAS determination. The factors affecting the cloud point extraction, such as pH, ligand concentration, surfactant concentration, and the incubation time were optimized. Under the optimal conditions, a detection limit of 12 ng/L and a relative standard deviation(RSD) of 2.9% were obtained for Ni(Ⅱ) determination. The enrichment factor was found to be 25. The proposed method was successfully applied to the determination of nickel(Ⅱ) in certified reference material and different types of water samples and the recovery was in a range of 95%―103%. 展开更多
关键词 Cloud point extraction Phase separation Graphite furnace atomic absorption spectrometry Nickel(Ⅱ)
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Determination of Mecruy at Trace Level in Natural Water Samples by Hydride Generation Atomic Absorption Spectrophotometry after Cloud Point Extraction Preconcentration 被引量:2
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作者 Ji Ying SONG Ming HOU Li Xiang ZHANG 《Chinese Chemical Letters》 SCIE CAS CSCD 2006年第9期1217-1220,共4页
A method for the determination of trace mercury in water samples by hydride generation atomic absorption spectrophotometry after cloud point extraction was proposed in the present work. The effects of pH, concentratio... A method for the determination of trace mercury in water samples by hydride generation atomic absorption spectrophotometry after cloud point extraction was proposed in the present work. The effects of pH, concentration of surfactant, and equilibration time on cloud point extraction were discussed. The enhancement factor of 20 and the detection limit of 0.039 μg/L were obtained for mercury with relative standard deviation of 4.8% (n = 11). 展开更多
关键词 Cloud point extraction MERCURY hydride generation atomic absorption spectrophotometry.
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Fingerprint singular points extraction based on orientation tensor field and Laurent series 被引量:3
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作者 刘琴 彭可 +4 位作者 刘巍 谢琴 李仲阳 兰浩 金耀 《Journal of Central South University》 SCIE EI CAS 2014年第5期1927-1934,共8页
Singular point(SP)extraction is a key component in automatic fingerprint identification system(AFIS).A new method was proposed for fingerprint singular points extraction,based on orientation tensor field and Laurent s... Singular point(SP)extraction is a key component in automatic fingerprint identification system(AFIS).A new method was proposed for fingerprint singular points extraction,based on orientation tensor field and Laurent series.First,fingerprint orientation flow field was obtained,using the gradient of fingerprint image.With these gradients,fingerprint orientation tensor field was calculated.Then,candidate SPs were detected by the cross-correlation energy in multi-scale Gaussian space.The energy was calculated between fingerprint orientation tensor field and Laurent polynomial model.As a global descriptor,the Laurent polynomial coefficients were allowed for rotational invariance.Furthermore,a support vector machine(SVM)classifier was trained to remove spurious SPs,using cross-correlation coefficient as a feature vector.Finally,experiments were performed on Singular Point Detection Competition 2010(SPD2010)database.Compared to the winner algorithm of SPD2010 which has best accuracy of 31.90%,the accuracy of proposed algorithm is 45.34%.The results show that the proposed method outperforms the state-of-the-art detection algorithms by large margin,and the detection is invariant to rotational transformations. 展开更多
关键词 fingerprint extraction singular point fingerprint orientation tensor field Laurent series rotational invariance supportvector machine (SVM)
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Image Feature Extraction and Matching of Augmented Solar Images in Space Weather
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作者 WANG Rui BAO Lili CAI Yanxia 《空间科学学报》 CAS CSCD 北大核心 2023年第5期840-852,共13页
Augmented solar images were used to research the adaptability of four representative image extraction and matching algorithms in space weather domain.These include the scale-invariant feature transform algorithm,speed... Augmented solar images were used to research the adaptability of four representative image extraction and matching algorithms in space weather domain.These include the scale-invariant feature transform algorithm,speeded-up robust features algorithm,binary robust invariant scalable keypoints algorithm,and oriented fast and rotated brief algorithm.The performance of these algorithms was estimated in terms of matching accuracy,feature point richness,and running time.The experiment result showed that no algorithm achieved high accuracy while keeping low running time,and all algorithms are not suitable for image feature extraction and matching of augmented solar images.To solve this problem,an improved method was proposed by using two-frame matching to utilize the accuracy advantage of the scale-invariant feature transform algorithm and the speed advantage of the oriented fast and rotated brief algorithm.Furthermore,our method and the four representative algorithms were applied to augmented solar images.Our application experiments proved that our method achieved a similar high recognition rate to the scale-invariant feature transform algorithm which is significantly higher than other algorithms.Our method also obtained a similar low running time to the oriented fast and rotated brief algorithm,which is significantly lower than other algorithms. 展开更多
关键词 Augmented reality Augmented image Image feature point extraction and matching Space weather Solar image
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Preconcentration of Cadmium in Environmental Samples by Cloud Point Extraction and Determination by FAAS 被引量:2
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作者 C. Bosch Ojeda F. Sánchez Rojas J. M. Cano Pavón 《American Journal of Analytical Chemistry》 2010年第3期127-134,共8页
Cloud point extraction (CPE) has been used for the preconcentration of cadmium, after the formation of a complex with 1, 5-bis(di-2-pyridylmethylene) thiocarbonohydrazide (DPTH), and further determination by flame ato... Cloud point extraction (CPE) has been used for the preconcentration of cadmium, after the formation of a complex with 1, 5-bis(di-2-pyridylmethylene) thiocarbonohydrazide (DPTH), and further determination by flame atomic absorption spectrometry (FAAS) using Triton X-114 as surfactant. The main factors affecting the CPE, such as concentration of Triton X-114 and DPTH, pH, equilibration temperature and incubation time, were optimized for the best extract efficiency. Under the optimum conditions i.e., pH 5.4, [DPTH] = 6x10-3%, [Triton X-114] = 0.25% (v/v), an enhancement factor of 10.5 fold was reached. The lower limit of detection (LOD) obtained under the optimal conditions was 0.95 μg L?1. The precision for 8 replicate deter- minations at 20 and 100 μgL?1 Cd were 2.4 % and 2 % relative standard deviation (R.S.D.). The calibration graph using the preconcentration method was linear with a correlation coefficient of 0,998 at levels close to the detection limit up to at least 200 μgL?1. The method was successfully applied to the determination of cadmium in water, environmental and food samples and in a BCR-176 standard reference material. 展开更多
关键词 CADMIUM Flame Atomic Absorption SPECTROMETRY Cloud point extraction TRITON X-114 Water SAMPLES Food SAMPLES
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Boiling Point Distribution of Hydrocarbon Types in Diesel Using Solid-Phase Extraction Followed by GC/FID-EIMS 被引量:1
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作者 Li Chengwei Tian Songbai Liu Zelong Zhu Xinyi 《China Petroleum Processing & Petrochemical Technology》 SCIE CAS 2008年第3期13-21,共9页
In this paper, a method was established to determine the boiling point distribution of hydrocarbon types in diesel. The diesel sample was separated into the saturate and aromatic fractions by means of solid-phase extr... In this paper, a method was established to determine the boiling point distribution of hydrocarbon types in diesel. The diesel sample was separated into the saturate and aromatic fractions by means of solid-phase extraction (SPE), and each fraction was analyzed by GC/FID-EIMS. According to the relationship between boiling point and retention time of n-paraffins in the chromatogram, the percentages of saturates and aromatics at each temperature interval were calculated. According to the average mass spectra of the saturate and aromatic fractions at each temperature interval, the hydrocarbon types of the sample were identified through summation of characteristic mass fragments. Using this method, the changes in composition of diesel during hydrotreating process were studied. The results showed that hydrogenation of aromatics is the main reaction during the hydrotreating process. The more rings the aromatics have, the easier the hydrogenation reactions would take place. The aromatics were converted into cycloparaffins via the hydrogenation and saturation process, leading to an increase in low boiling point fractions in the hydrotreated oil. 展开更多
关键词 boiling point distribution hydrocarbon type DIESEL GC/FID-EIMS solid-phase extraction
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A New Thioamide Derivative for Separation and Preconcentration of Multi Elements in Aquatic Environment by Cloud Point Extraction 被引量:1
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作者 Mohamed M. Hassanien Ali M. Hassan +1 位作者 Wael I. Mortada Ahmed A. El-Asmy 《American Journal of Analytical Chemistry》 2011年第6期697-709,共13页
2-(pyridine-2-yl)-N-p-chlorohydrazinecarbothioamide (HCPTS) was synthesized, characterized and successfully applied for the preconcentration of Cu(II), Ni(II), Zn(II), Cd(II), Co(II), Pb(II), Fe(II), and Hg(II) in wat... 2-(pyridine-2-yl)-N-p-chlorohydrazinecarbothioamide (HCPTS) was synthesized, characterized and successfully applied for the preconcentration of Cu(II), Ni(II), Zn(II), Cd(II), Co(II), Pb(II), Fe(II), and Hg(II) in water, blood, and urine samples prior to graphite furnace atomic absorption determination (GFAAS);Hg was determined by cold vapor technique. Under the optimum experimental conditions (i.e. pH = 8, 10–4 M of HCPTS, 0.05% w/v of Triton X-114), calibration graphs were linear in the range of 0.02 to 200 ng?mL–1 for Co(II), Cd(II), Pb(II) and Ni(II);0.03 to 200 ng?mL–1 for Cu(II);0.07 to 200 ng?mL–1 for Fe(II) and Zn(II) and 0.02 to 150 ng?mL–1 for Hg(II). The enrichment factors were 43, 51, 41, 46, 54, 40, 45 and 52 for Cu(II), Ni(II),Zn (II), Cd(II), Co(II), Pb(II), Fe(II), and Hg(II), respectively. The limit of detection were found to be 0.019, 0.094, 0.0514, 0.052, 0.0165, 0.047, 0.068 and 0.041 ng?mL–1 for Cu(II), Ni(II), Zn(II), Cd(II), Co(II), Pb(II), Fe(II), and Hg(II), respectively. The developed method was applied to the determination of these metal ions in water, blood and urine samples with satisfactory results. 展开更多
关键词 HEAVY Metals PRECONCENTRATION Cloud point extraction 2-(Pyridine-2-Yl)-N-P-Chlorohydrazinecarbothioamide
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Extraction of Sodium Copper Chlorophyll in Food Samples Based on Cloud Point Extraction with a Nonionic Surfactant 被引量:1
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作者 SUN Chen LIU Guangyu ZHAO Peixia 《Grain & Oil Science and Technology》 2018年第1期59-62,共4页
A new method was developed for the determination of sodium copper chlorophyll(SCC) by cloud point extraction preconcentration and spectrophotometry, for which Triton X-114 was selected as a nonionic surfactant. Severa... A new method was developed for the determination of sodium copper chlorophyll(SCC) by cloud point extraction preconcentration and spectrophotometry, for which Triton X-114 was selected as a nonionic surfactant. Several factors affecting the extraction efficiency of SCC and its subsequent determination, including the p H of the sample solution, salt and surfactant concentrations, and equilibration temperature and time, were studied and optimized. The extraction efficiency approached 99.4%.The calibration graph under the optimum conditions was linear in the concentration range of 3–220 mg/L with correlation coefficients> 0.9997(n = 8). The limit of detection for the analytes was 0.6 mg/L(S/N = 3). The proposed method is inexpensive, simple, and accurate for the extraction and determination of SCC in food samples. 展开更多
关键词 Cloud point extraction Sodium copper chlorophyll Triton X-114
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Recovery of polyphenols from camu-camu(Myrciaria dubia H.B.K.McVaugh)depulping residue by cloud point extraction
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作者 Carlos Eduardo de Araujo Padilha Juliana Chris Silva de Azevedo +5 位作者 Francisco Caninde de Sousa Junior Sergio Dantas de Oliveira Junior Domingos Fabiano de Santana Souza Jackson Araujo de Oliveira Gorete Ribeiro de Macedo Everaldo Silvino dos Santos 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2018年第12期2471-2476,共6页
In this study the potential of cloud point extraction formed by a non-ionic surfactant was used in order to separate polyphenols from industrial residues of camu-camu. The effects of operational conditions of the clou... In this study the potential of cloud point extraction formed by a non-ionic surfactant was used in order to separate polyphenols from industrial residues of camu-camu. The effects of operational conditions of the cloud point extraction(CPE) on the polyphenol recovery and volumetric ratio were investigated. The results showed a maximum recovery of 95.71% that was obtained using 7.0 wt% Triton X-114, native pH(3.25), and 80 wt%polyphenol extract at 30 °C. The use of cloud point extraction was successful to recover the polyphenols from agroindustrial residue since it is a simple as well as of low-cost technique. 展开更多
关键词 CLOUD point extraction RECOVERY POLYPHENOLS Camu-camu Depulping RESIDUE
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OPERATING POINT AND STRIPPING EXTRACTION CALCULATIONS FOR CYCLONE 10/5
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作者 王良明 S.Zaremba 《Nuclear Science and Techniques》 SCIE CAS CSCD 1992年第1期30-35,共6页
By using the magnetic field map, equilibrium orbit, operating point of v r and v z and beam trajectories after stripper for Cyclone 10/5 have been calculated. The positions of two strippers and two targets have been d... By using the magnetic field map, equilibrium orbit, operating point of v r and v z and beam trajectories after stripper for Cyclone 10/5 have been calculated. The positions of two strippers and two targets have been determined. The numerical simulation is consistent with experimental tests. 展开更多
关键词 Isochronous CYCLOTRON Operating point REVOLUTION FREQUENCY Betatron Oscillation FREQUENCY Equilibrium ORBIT STRIPPING extraction
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Parameters of Exterior Ballistic Feature Points Extraction in Radar Measurement Data by EMD
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作者 Wanjun Zhang Kailin Wang +2 位作者 Xiaoying Wu Guohui Li Hongtian Liu 《Journal of Beijing Institute of Technology》 EI CAS 2018年第4期503-509,共7页
The problem of measuring exterior ballistic feature points is always difficult to solve and it is essentiale on exterior ballistic measurement.By analysis of radar reflection characteristics and non-stationary echo si... The problem of measuring exterior ballistic feature points is always difficult to solve and it is essentiale on exterior ballistic measurement.By analysis of radar reflection characteristics and non-stationary echo signals of exterior ballistic feature points,the echo data of exterior ballistic feature points is measured by using the continuous wave radar.The parameters of feature points are extracted by the empirical mode decomposition method(EMD)of Hilbert-Huang transform(HHT)spectrum analysis technique.The radar echo signal model and EMD extraction model are established to analyze the exterior ballistic mutation point detection and EMD extraction method of aliasing echo signal.Typical feature point parameters of exterior ballistic in rocket flight tests are carried out and the effectiveness of the method is verified.A new method of measuring the parameters of exterior ballistic feature point is therefore presented. 展开更多
关键词 exterior ballistic characteristic points empirical mode decomposition method(EMD) continuous wave radar information extraction
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Determination of Selenium in Water by Vortex-Assisted Cloud-Point Extraction Combination with Fluorescence Detection
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作者 JIAO Yurong LI Haifang 《Journal of Donghua University(English Edition)》 EI CAS 2019年第5期487-492,共6页
A simple vortex-assisted cloud-point extraction(VA-CPE)method combined with the fluorescence(FL)strategy was developed to extract and determine inorganic Se(IV)in environmental water.Toluene was used as an extraction ... A simple vortex-assisted cloud-point extraction(VA-CPE)method combined with the fluorescence(FL)strategy was developed to extract and determine inorganic Se(IV)in environmental water.Toluene was used as an extraction reagent,and Se(VI)was reduced to Se(IV)by subjecting its solution in 4 mol/L HCl to microwave heating for generating a yellow piazselenol complex using 3,3'-diaminobenzidine(DAB)and Se(IV).The concentration of the complex exhibited an excellent linear relation with the FL at 560 nm with an excitation wavelength of 420 nm.In addition,the effects of the toluene volume,pH,and VA-CPE parameters were investigated and the interference from coexisting ions was also studied.This method was successfully applied to determine the concentration selenium in environmental water samples with a detection limit of 0.05μg/L in the line range from 0.50μg/L to 50.00μg/L. 展开更多
关键词 SELENIUM CLOUD-point extraction fluorescence(FL)derivatization 3 3'-diaminobenzidine(DAB)
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