This work explores the methodology for micron-scale water droplet contact angle derivation for the warty surface of octocoral sclerites. The calcite-made sclerites of the Red Sea octocoral Dendronephthya hemprichi hav...This work explores the methodology for micron-scale water droplet contact angle derivation for the warty surface of octocoral sclerites. The calcite-made sclerites of the Red Sea octocoral Dendronephthya hemprichi have been chosen as a model for this study. Water droplet condensation on the sclerites has been in-situ investigated using Quanta 200 FEG (field emission gun) ESEM (environmental scanning electron microscope) under wet environmental conditions. Two different analysis methods of droplet top and side views have been applied to determine the contact angle based on the secondary electron images. The ESEM image analysis for the sclerites indicates that their surface is hydrophilic. The microscopic contact angle is measured to be 45.3°±6.3°. The macroscopic contact angle has been calculated by using the Wenzel model for the surface texturing of the sclerites.展开更多
The objective of this study is to find out, to what extent the geochemical characteristics of lapis lazuli can be utilized in respect to its provenance. A wide range of variables is taken into consideration depending ...The objective of this study is to find out, to what extent the geochemical characteristics of lapis lazuli can be utilized in respect to its provenance. A wide range of variables is taken into consideration depending on the quantity of samples analysed from a specific geological region and the methods applied. In order to provide evidence, a multi-technique analytical approach using μXRF, ESEM, PGAA and PIXE is applied to samples from the most famous deposits of lapis lazuli. Special elements determined as fingerprints are compared in relation to the forming conditions obvious in textural features. The results and statistical output allow a differentiation that enables an optimized local classification of the blue stone. An absolute requirement for all geo-tracing performed on blue colored cultural objects of unknown provenance is awareness of the limits of analysis. The possible sources of lapis lazuli are tested by analysing the blue pigment used as paint on murals and ink on manuscripts from the Silk Road.展开更多
文摘This work explores the methodology for micron-scale water droplet contact angle derivation for the warty surface of octocoral sclerites. The calcite-made sclerites of the Red Sea octocoral Dendronephthya hemprichi have been chosen as a model for this study. Water droplet condensation on the sclerites has been in-situ investigated using Quanta 200 FEG (field emission gun) ESEM (environmental scanning electron microscope) under wet environmental conditions. Two different analysis methods of droplet top and side views have been applied to determine the contact angle based on the secondary electron images. The ESEM image analysis for the sclerites indicates that their surface is hydrophilic. The microscopic contact angle is measured to be 45.3°±6.3°. The macroscopic contact angle has been calculated by using the Wenzel model for the surface texturing of the sclerites.
文摘The objective of this study is to find out, to what extent the geochemical characteristics of lapis lazuli can be utilized in respect to its provenance. A wide range of variables is taken into consideration depending on the quantity of samples analysed from a specific geological region and the methods applied. In order to provide evidence, a multi-technique analytical approach using μXRF, ESEM, PGAA and PIXE is applied to samples from the most famous deposits of lapis lazuli. Special elements determined as fingerprints are compared in relation to the forming conditions obvious in textural features. The results and statistical output allow a differentiation that enables an optimized local classification of the blue stone. An absolute requirement for all geo-tracing performed on blue colored cultural objects of unknown provenance is awareness of the limits of analysis. The possible sources of lapis lazuli are tested by analysing the blue pigment used as paint on murals and ink on manuscripts from the Silk Road.