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Microstructures,corrosion behavior and mechanical properties of as-cast Mg-6Zn-2X(Fe/Cu/Ni)alloys for plugging tool applications 被引量:1
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作者 Baosheng Liu Jiali Wei +4 位作者 Shaohua Zhang Yuezhong Zhang Pengpeng Wu Daqing Fang Guorui Ma 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第4期697-711,共15页
Mg-6Zn-2X(Fe/Cu/Ni)alloys were prepared through semi-continuous casting,with the aim of identifying a degradable magnesium(Mg)alloy suitable for use in fracturing balls.A comparative analysis was conducted to assess t... Mg-6Zn-2X(Fe/Cu/Ni)alloys were prepared through semi-continuous casting,with the aim of identifying a degradable magnesium(Mg)alloy suitable for use in fracturing balls.A comparative analysis was conducted to assess the impacts of adding Cu and Ni,which result in finer grains and the formation of galvanic corrosion sites.Scanner electronic microscopy examination revealed that precipitated phases concentrated at grain boundaries,forming a semi-continuous network structure that facilitated corrosion penetration in Mg-6Zn-2Cu and Mg-6Zn-2Ni alloys.Pitting corrosion was observed in Mg-6Zn-2Fe,while galvanic corrosion was identified as the primary mechanism in Mg-6Zn-2Cu and Mg-6Zn-2Ni alloys.Among the tests,the Mg-6Zn-2Ni alloy exhibited the highest corrosion rate(approximately 932.9 mm/a)due to its significant potential difference.Mechanical testing showed that Mg-6Zn-2Ni alloy possessed suitable ultimate compressive strength,making it a potential candidate material for degradable fracturing balls,effectively addressing the challenges of balancing strength and degradation rate in fracturing applications. 展开更多
关键词 magnesium alloys microstructure micro-galvanic corrosion mechanical properties
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Microstructure and mechanical properties stability of pre-hardening treatment in Al-Cu alloys for pre-hardening forming process
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作者 Liping Tang Pengfei Wei +1 位作者 Zhili Hu Qiu Pang 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第3期539-551,共13页
The stability of the microstructure and mechanical properties of the pre-hardened sheets during the pre-hardening forming(PHF)process directly determines the quality of the formed components.The microstructure stabili... The stability of the microstructure and mechanical properties of the pre-hardened sheets during the pre-hardening forming(PHF)process directly determines the quality of the formed components.The microstructure stability of the pre-hardened sheets was in-vestigated by differential scanning calorimetry(DSC),transmission electron microscopy(TEM),and small angle X-ray scattering(SAXS),while the mechanical properties and formability were analyzed through uniaxial tensile tests and formability tests.The results in-dicate that the mechanical properties of the pre-hardened alloys exhibited negligible changes after experiencing 1-month natural aging(NA).The deviations of ultimate tensile strength(UTS),yield strength(YS),and sheet formability(Erichsen value)are all less than 2%.Also,after different NA time(from 48 h to 1 month)is applied to alloys before pre-hardening treatment,the pre-hardened alloys possess stable microstructure and mechanical properties as well.Interestingly,with the extension of NA time before pre-hardening treatment from 48 h to 1 month,the contribution of NA to the pre-hardening treatment is limited.Only a yield strength increment of 20 MPa is achieved,with no loss in elongation.The limited enhancement is mainly attributed to the fact that only a limited number of clusters are transformed into Guinier-Preston(GP)zones at the early stage of pre-hardening treatment,and the formation ofθ''phase inhibits the nucleation and growth of GP zones as the precipitated phase evolves. 展开更多
关键词 Al-Cu alloy pre-hardened alloy natural aging mechanical properties microstructure
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Effect of annealing treatment on the microstructure and mechanical properties of warm-rolled Mg-Zn-Gd-Ca-Mn alloys
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作者 Yifan Song Xihai Li +5 位作者 Jinliang Xu Kai Zhang Yaozong Mao Hong Yan Huiping Li Rongshi Chen 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第10期2208-2220,共13页
The basal texture of traditional magnesium alloy AZ31 is easy to form and exhibits poor plasticity at room temperature.To address these problems,a multi-micro-alloyed high-plasticity Mg-1.8Zn-0.8Gd-0.1Ca-0.2Mn(wt%)all... The basal texture of traditional magnesium alloy AZ31 is easy to form and exhibits poor plasticity at room temperature.To address these problems,a multi-micro-alloyed high-plasticity Mg-1.8Zn-0.8Gd-0.1Ca-0.2Mn(wt%)alloy was developed using the unique role of rare earth and Ca solute atoms.In addition,the influence of the annealing process on the grain size,second phase,texture,and mechanical properties of the warm-rolled sheet at room temperature was analyzed with the goal of developing high-plasticity mag-nesium alloy sheets and obtaining optimal thermal-mechanical treatment parameters.The results show that the annealing temperature has a significant effect on the microstructure and properties due to the low alloying content:there are small amounts of larger-sized block and long string phases along the rolling direction(RD),as well as several spherical and rodlike particle phases inside the grains.With increas-ing annealing temperature,the grain size decreases and then increases,and the morphology,number,and size of the second phase also change correspondingly.The particle phase within the grains vanishes at 450℃,and the grain size increases sharply.In the full recrystal-lization stage at 300-350℃,the optimum strength-plasticity comprehensive mechanical properties are presented,with yield strengths of 182.1 and 176.9 MPa,tensile strengths of 271.1 and 275.8 MPa in the RD and transverse direction(TD),and elongation values of 27.4%and 32.3%,respectively.Moreover,there are still some larger-sized phases in the alloy that influence its mechanical properties,which offers room for improvement. 展开更多
关键词 Mg-Zn-Gd-Ca-Mn alloy annealing treatment microstructure TEXTURE dynamic recrystallization mechanical properties
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Role of alloying and heat treatment on microstructure and mechanical properties of cast Al-Li alloys:A review
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作者 Guo-hua Wu You-jie Guo +4 位作者 Fang-zhou Qi Shen Zhang Yi-xiao Wang Xin Tong Liang Zhang 《China Foundry》 SCIE EI CAS CSCD 2024年第5期445-460,共16页
Due to the prominent advantages of low density,high elastic modulus,high specific strength and specific stiffness,cast Al-Li alloys are suitable metallic materials for manufacturing complex large-sized components and ... Due to the prominent advantages of low density,high elastic modulus,high specific strength and specific stiffness,cast Al-Li alloys are suitable metallic materials for manufacturing complex large-sized components and are ideal structural materials for aerospace,defense and military industries.On the basis of the microstructural characteristics of cast Al-Li alloys,exploring the role of alloying and micro-alloying can stabilize their dominant position and further expand their application scope.In this review,the development progress of cast Al-Li alloys was summarized comprehensively.According to the latest research highlights,the influence of alloying and heat treatment on the microstructure and mechanical properties was systematically analyzed.The potential methods to improve the alloy performance were concluded.In response to the practical engineering requirements of cast Al-Li alloys,the scientific challenges and future research directions were discussed and prospected. 展开更多
关键词 cast Al-Li alloy ALLOYING microstructure mechanical properties heat treatment
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Microstructure and mechanical properties of new Mg-Zn-Y-Zr alloys with high castability and ignition resistance
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作者 T.A.Koltygina V.E.Bazhenov +5 位作者 A.V.Koltygin A.S.Prosviryakov N.Y.Tabachkova I.I.Baranov A.A.Komissarov A.I.Bazlov 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第12期2714-2726,共13页
Complex studies of new Mg-Zn-Y-Zr system alloys have been carried out.The content range for the formation of the two-phase structure MgSS(Mg solid solution)+LPSO(long-period stacking ordered)in alloys of the Mg-Zn-Y-Z... Complex studies of new Mg-Zn-Y-Zr system alloys have been carried out.The content range for the formation of the two-phase structure MgSS(Mg solid solution)+LPSO(long-period stacking ordered)in alloys of the Mg-Zn-Y-Zr system was determined by thermodynamic calculations.The effect of heat treatment regimes on microstructure,mechanical,and corrosion properties was invest-igated.The fluidity,hot tearing tendency,and ignition temperature of the alloys were determined.The best combination of castability,mechanical,and corrosion properties was found for the Mg-2.4Zn-4Y-0.8Zr alloy.The alloys studied are superior to their industrial counterparts in terms of technological properties,while maintain high corrosion and mechanical properties.The increased level of pro-perties is achieved by a suitable heat treatment regime that provides a complete transformation of the 18R to 14H modification of the LPSO phase. 展开更多
关键词 metals and alloys liquid-solid reactions microstructure FLUIDITY mechanical properties corrosion transmission electron mi-croscopy
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Effect of cold rolling deformation on microstructure evolution and mechanical properties of spray formed Al−Zn−Mg−Cu−Cr alloys
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作者 Cai-he FAN Yi-hui LI +4 位作者 Qin WU Ling OU Ze-yi HU Yu-meng NI Jian-jun YANG 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2024年第8期2442-2454,共13页
The impact of cold rolling deformation,which was introduced after solid solution and before aging treatment,on microstructure evolution and mechanical properties of the as-extruded spray formed Al−9.8Zn−2.3Mg−1.73Cu−0... The impact of cold rolling deformation,which was introduced after solid solution and before aging treatment,on microstructure evolution and mechanical properties of the as-extruded spray formed Al−9.8Zn−2.3Mg−1.73Cu−0.13Cr(wt.%)alloy,was investigated.SEM,TEM,and EBSD were used to analyze the microstructures,and tensile tests were conducted to assess mechanical properties.The results indicate that the D1-T6 sample,subjected to 25%cold rolling deformation,exhibits finer grains(3.35μm)compared to the D0-T6 sample(grain size of 4.23μm)without cold rolling.Cold rolling refines the grains that grow in solution treatment.Due to the combined effects of finer and more dispersed precipitates,higher dislocation density and smaller grains,the yield strength and ultimate tensile strength of the D1-T6 sample can reach 663 and 737 MPa,respectively.In comparison to the as-extruded and D0-T6 samples,the yield strength of the D1-T6 sample increases by 415 and 92 MPa,respectively. 展开更多
关键词 Al−Zn−Mg−Cu alloy spray forming microstructure evolution mechanical properties strengthening mechanism
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Evolution of mechanical properties,localized corrosion resistance and microstructure of a high purity Al-Zn-Mg-Cu alloy during non-isothermal aging
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作者 DAI Xuan-xuan LI Yu-zhang +2 位作者 LIU Sheng-dan YE Ling-ying BAO Chong-jun 《Journal of Central South University》 SCIE EI CAS CSCD 2024年第6期1790-1807,共18页
The evolution of mechanical properties,localized corrosion resistance of a high purity Al-Zn-Mg-Cu alloy during non-isothermal aging(NIA)was investigated by hardness test,electrical conductivity test,tensile test,inte... The evolution of mechanical properties,localized corrosion resistance of a high purity Al-Zn-Mg-Cu alloy during non-isothermal aging(NIA)was investigated by hardness test,electrical conductivity test,tensile test,intergranular corrosion test,exfoliation corrosion test,slow strain rate tensile test and electrochemical test,and the mechanism has been discussed based on microstructure examination by optical microscopy,electron back scattered diffraction,scanning electron microscopy and scanning transmission electron microscopy.The NIA treatment includes a heating stage from 40℃to 180℃with a rate of 20℃/h and a cooling stage from 180℃to 40℃with a rate of 10℃/h.The results show that the hardness and strength increase rapidly during the heating stage of NIA since the increasing temperature favors the nucleation and the growth of strengthening precipitates and promotes the transformation of Guinier-Preston(GPI)zones toη'phase.During the cooling stage,the sizes ofη'phase increase with a little change in the number density,leading to a further slight increase of the hardness and strength.As NIA proceeds,the corroded morphology in the alloy changes from a layering feature to a wavy feature,the maximum corrosion depth decreases,and the reason has been analyzed based on the microstructural and microchemical feature of precipitates at grain boundaries and subgrain boundaries. 展开更多
关键词 Al-Zn-Mg-Cu alloy non-isothermal aging mechanical properties localized corrosion resistance microstructure
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Effect of annealing temperature on microstructure and mechanical properties of Mg-Zn-Zr-Nd alloy with large final rolling deformation
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作者 ZHANG Jin-hai NIE Kai-bo +2 位作者 ZHANG Jin-hua DENG Kun-kun LIU Zhi-long 《Journal of Central South University》 SCIE EI CAS CSCD 2024年第6期1774-1789,共16页
In this study,the Mg-3Zn-0.5Zr-χNd(χ=0,0.6)alloys were subjected to final rolling treatment with large deformation of 50%.The impact of annealing temperatures on the microstructure and mechanical properties was inve... In this study,the Mg-3Zn-0.5Zr-χNd(χ=0,0.6)alloys were subjected to final rolling treatment with large deformation of 50%.The impact of annealing temperatures on the microstructure and mechanical properties was investigated.The rolled Mg-3Zn-0.5Zr-0.6Nd alloy exhibited an ultimate tensile strength of 386 MPa,a yield strength of 361 MPa,and an elongation of 7.1%.Annealing at different temperatures resulted in reduced strength and obviously increased elongation for both alloys.Optimal mechanical properties for the Mg-3Zn-0.5Zr-0.6Nd alloy were achieved after annealing at 200℃,with an ultimate tensile strength of 287 MPa,a yield strength of 235 MPa,and an elongation of 26.1%.The numerous deformed microstructures,twins,and precipitated phases in the rolled alloy could impede the deformation at room temperature and increase the work hardening rate.After annealing,a decrease in the work hardening effect and an increase in the dynamic recovery effect were obtained due to the formation of fine equiaxed grains,and the increased volume fraction of precipitated phases,which significantly improved the elongation of the alloy.Additionally,the addition of Nd element could enhance the annealing recrystallization rate,reduce the Schmid factor difference between basal and prismatic slip systems,facilitate multi-system slip initiation and improve the alloy plasticity. 展开更多
关键词 Mg-Zn-Zr-Nd alloy large final rolling deformation annealing temperatures microstructures mechanical properties
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Microstructure homogeneity and mechanical properties of laser-arc hybrid welded AZ31B magnesium alloy
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作者 Yongkang Gao Kangda Hao +4 位作者 Lianyong Xu Yongdian Han Lei Zhao Wenjing Ren Hongyang Jing 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2024年第5期1986-1995,共10页
Laser-arc hybrid welding of AZ31B magnesium alloy was carried out,the effects of welding parameters on weld formation,microstructure homogeneity and mechanical properties were investigated.The results showed that lase... Laser-arc hybrid welding of AZ31B magnesium alloy was carried out,the effects of welding parameters on weld formation,microstructure homogeneity and mechanical properties were investigated.The results showed that laser-arc hybrid welding was beneficial to improve the weld formation of magnesium alloy by inhibiting the defect of undercut and pores.The weld microstructure was mainly columnar grains neighboring the fusion line and equiaxed grains at the weld center.It was interesting that the grain size at the upper arc zone was smaller than that at the lower laser zone,with the difference mainly affected by laser power rather than welding current and welding speed.The welding parameters were optimized as laser power of 3.5 kW,welding current of 100 A and welding speed of 1.5 m/min.In this case,the weld was free of undercut and pores,and the tensile strength and elongation rate reached 252 MPa and 11.2%,respectively.Finally,the microstructure homogeneity was illustrated according to the heat distribution,and the evolution law of tensile properties was discussed basing on the weld formation and microstructure characteristics. 展开更多
关键词 Magnesium alloy Laser-arc hybrid welding microstructure homogeneity mechanical properties
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Microstructure and mechanical properties of stationary shoulder friction stir welding joint of 2A14-T62 aluminum alloy
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作者 邓建峰 王博 +3 位作者 王生希 郭伟强 黄智恒 费文潘 《China Welding》 CAS 2024年第2期31-38,共8页
2A14-T62 butt joint was successfully welded by stationary shoulder friction stir welding(SSFSW)method.The results showed that using a pin with small shoulder could broaden the process window,and under a rotation speed... 2A14-T62 butt joint was successfully welded by stationary shoulder friction stir welding(SSFSW)method.The results showed that using a pin with small shoulder could broaden the process window,and under a rotation speed of 2000 r/min and welding speed of 30 mm/min,joint with smooth surface,small reduction in thickness and little inner defects was obtained.The weld nugget zone was approx-imately circular,which was a unique morphology for SSFSW.The heat-affected zone(HAZ)and thermo-mechanically affected zone(TMAZ)were both quite narrow due to the lower heat input and slight mechanical action of the stationary shoulder.The fraction of high angle grain boundaries(HAGBs)exhibited a“W”shape along horizontal direction(from advancing side to retreating side),and the minim-um value located at HAZ.The average ultimate tensile strength and elongation of the joint were 325 MPa and 4.5%,respectively,with the joint efficiency of 68.3%.The joint was ductile fractured and the fracture surface contained two types of dimples morphology in different re-gions of the joint.Microhardness distribution in the joint exhibited a“W”shape,and the difference along the thickness direction was negli-gible.The joint had strong stress corrosion cracking susceptibility,and the slow stain rate tensile strength was 139 MPa.Microcrack and Al2O3 particulates were observed at the fracture surface. 展开更多
关键词 2A14-T62 aluminum alloy stationary shoulder friction stir welding microstructure mechanical property stress corrosion cracking
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Microstructure Characteristics and Elevated Temperature Mechanical Properties of a B Containedβ-solidifiedγ-TiAl Alloy
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作者 王秀琦 GUO Ruiqi +5 位作者 刘国怀 LI Tianrui YANG Yuxuan CHEN Yang XIN Meiling WANG Zhaodong 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS CSCD 2024年第3期738-746,共9页
The improved microstructure and enhanced elevated temperature mechanical properties of Ti-44Al-5Nb-(Mo,V,B)alloys were obtained by vacuum arc re-melting(VAR)and primary annealing heat treatment(HT)of 1260℃/6 h/Furnac... The improved microstructure and enhanced elevated temperature mechanical properties of Ti-44Al-5Nb-(Mo,V,B)alloys were obtained by vacuum arc re-melting(VAR)and primary annealing heat treatment(HT)of 1260℃/6 h/Furnace cooling(FC).The phase transformation,microstructure evolution and tensile properties for as-cast and HTed alloys were investigated.Results indicate that three main phase transformation points are determined,T_(eut)=1164.3℃,T_(γsolv)=1268.3℃and T_(βtrans)=1382.8℃.There are coarse lamellar colonies(300μm in length)and neighbor reticular B2 andγgrain(3-5μm)in as-cast alloy,while lamellar colonies are markedly refined and multi-oriented(20-50μm)as well as the volume fraction and grain sizes of equiaxedγand B2 phases(about 15μm)significantly increase in as-HTed alloy.Phase transformations involvingα+γ→α+γ+β/B2 and discontinuousγcoarsening contribute to the above characteristics.Borides(1-3μm)act as nucleation sites forβ_(eutectic) and produce massiveβgrains with different orientations,thus effectively refining the lamellar colonies and forming homogeneous multi-phase microstructure.Tensile curves show both the alloys exhibit suitable performance at 800℃.As-cast alloy shows a higher ultimate tensile stress of 647 MPa,while a better total elongation of more than 41%is obtained for as-HTed alloy.The mechanical properties improvement is mainly attributed to fine,multi-oriented lamellar colonies,coordinated deformation of homogeneous multi-phase microstructure and borides within lamellar interface preventing crack propagation. 展开更多
关键词 TiAl alloy phase transformation heat treatment BORIDE microstructure mechanical properties
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Improvement of Microstructure and Mechanical Properties of Rapid Cooling Friction Stir-welded A1050 Pure Aluminum
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作者 许楠 LIU Lutao +2 位作者 SONG Qining ZHAO Jianhua BAO Yefeng 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS CSCD 2024年第1期134-141,共8页
Two-mm thick A1050 pure aluminum plates were successfully joined by conventional and rapid cooling friction stir welding(FSW), respectively. The microstructure and mechanical properties of the welded joints were inves... Two-mm thick A1050 pure aluminum plates were successfully joined by conventional and rapid cooling friction stir welding(FSW), respectively. The microstructure and mechanical properties of the welded joints were investigated by electron backscatter diffraction characterization, Vickers hardness measurements, and tensile testing. The results showed that liquid CO_(2) coolant significantly reduced the peak temperature and increased the cooling rate, so the rapidly cooled FSW joint exhibited fine grains with a large number of dislocations. The grain refinement mechanism of the FSW A1050 pure aluminum joint was primarily attributed to the combined effects of continuous dynamic recrystallization, grain subdivision, and geometric dynamic recrystallization. Compared with conventional FSW, the yield strength, ultimate tensile strength, and fracture elongation of rapidly cooled FSW joint were significantly enhanced, and the welding efficiency was increased from 80% to 93%. The enhanced mechanical properties and improved synergy of strength and ductility were obtained due to the increased dislocation density and remarkable grain refinement. The wear of the tool can produce several WC particles retained in the joint, and the contribution of second phase strengthening to the enhanced strength should not be ignored. 展开更多
关键词 aluminum alloy friction stir welding RECRYSTALLIZATION microstructure mechanical properties
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Enhancing the mechanical properties of casting eutectic high -entropy alloys via W addition
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作者 Xu Yang Dezhi Chen +3 位作者 Li Feng Gang Qin Shiping Wu Ruirun Chen 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第6期1364-1372,共9页
The effect of W element on the microstructure evolution and mechanical properties of Al_(1.25)CoCrFeNi3 eutectic high-entropy alloy and Al_(1.25)CoCrFeNi_(3-x)W_(x)(x=0,0.05,0.1,0.3,and 0.5;atomic ratio)high-entropy a... The effect of W element on the microstructure evolution and mechanical properties of Al_(1.25)CoCrFeNi3 eutectic high-entropy alloy and Al_(1.25)CoCrFeNi_(3-x)W_(x)(x=0,0.05,0.1,0.3,and 0.5;atomic ratio)high-entropy alloys(HEAs)were explored.Results show that the Al_(1.25)CoCrFeNi_(3-x)W_(x) HEAs are composed of face-centered cubic and body-centered cubic(BCC)phases.As W content increases,the microstructure changes from eutectic to dendritic.The addition of W lowers the nucleation barrier of the BCC phase,decreases the valence electron concentration of the HEAs,and replaces Al in the BCC phase,thus facilitating the nucleation of the BCC phase.Tensile results show that the addition of W greatly improves the mechanical properties,and solid-solution,heterogeneous-interface,and second-phase strengthening are the main strengthening mechanisms.The yield strength,tensile strength,and elongation of the Al_(1.25)CoCrFeNi2.95W0.05 HEA are 601.44 MPa,1132.26 MPa,and 15.94%,respectively,realizing a balance between strength and plasti-city.The fracture mode of the Al_(1.25)CoCrFeNi_(3-x)W_(x) HEAs is ductile–brittle mixed fracture,and the crack propagates and initiates in the BCC phase.The eutectic lamellar structure impedes crack propagation and maintains plasticity. 展开更多
关键词 high-entropy alloy microstructure mechanical property fracture behavior
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Microstructure and mechanical properties of Co-28Cr-6Mo-0.22C investment castings by current solution treatment
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作者 Ze-yu Dan Jun Liu +4 位作者 Jian-lei Zhang Yan-hua Li Yuan-xin Deng Yun-hu Zhang Chang-jiang Song 《China Foundry》 SCIE EI CAS CSCD 2024年第4期369-378,共10页
This study examined the impact of current solution treatment on the microstructure and mechanical properties of the Co-28Cr-6Mo-0.22C alloy investment castings.The findings reveal that the current solution treatment s... This study examined the impact of current solution treatment on the microstructure and mechanical properties of the Co-28Cr-6Mo-0.22C alloy investment castings.The findings reveal that the current solution treatment significantly promotes the dissolution of carbides at a lower temperature.The optimal conditions for solution treatment are determined as a solution temperature of 1,125°C and a holding time of 5.0 min.Under these parameters,the size and volume fraction of precipitated phases in the investment castings are measured as6.2μm and 1.1vol.%.The yield strength,ultimate tensile strength,and total elongation of the Co-28Cr-6Mo-0.22C investment castings are 535 MPa,760 MPa,and 12.6%,respectively.These values exceed those obtained with the conventional solution treatment at 1,200°C for 4.0 h.The findings suggest a phase transformation of M_(23)C_(6)→σ+C following the current solution treatment at 1,125°C for 5.0 min.In comparison,the traditional solution treatment at 1,200°C for 4.0 h leads to the formation of M_(23)C_(6)and M_(6)C carbides.It is noteworthy that the non-thermal effect of the current during the solution treatment modifies the free energy of both the matrix and precipitation phase.This modification lowers the phase transition temperature of the M_(23)C_(6)→σ+C reaction,thereby facilitating the dissolution of carbides.As a result,the current solution treatment approach achieves carbide dissolution at a lower temperature and within a significantly shorter time when compared to the traditional solution treatment methods. 展开更多
关键词 CoCrMo alloy investment castings current solution treatment microstructure mechanical property CARBIDE
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A critical review on solid-state welding of high entropy alloys-processing,microstructural characteristics and mechanical properties of joints
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作者 Tushar Sonar Mikhail Ivanov +2 位作者 Evgeny Trofimov Aleksandr Tingaev Ilsiya Suleymanova 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第4期78-133,共56页
The high entropy alloys(HEAs)are the newly developed high-performance materials that have gained significant importance in defence,nuclear and aerospace sector due to their superior mechanical properties,heat resistan... The high entropy alloys(HEAs)are the newly developed high-performance materials that have gained significant importance in defence,nuclear and aerospace sector due to their superior mechanical properties,heat resistance,high temperature strength and corrosion resistance.These alloys are manufactured by the equal mixing or larger proportions of five or more alloying elements.HEAs exhibit superior mechanical performance compared to traditional engineering alloys because of the extensive alloying composition and higher entropy of mixing.Solid state welding(SSW)techniques such as friction stir welding(FSW),rotary friction welding(RFW),diffusion bonding(DB)and explosive welding(EW)have been efficiently deployed for improving the microstructural integrity and mechanical properties of welded HEA joints.The HEA interlayers revealed greater potential in supressing the formation of deleterious intermetallic phases and maximizing the mechanical properties of HEAs joints.The similar and dissimilar joining of HEAs has been manifested to be viable for HEA systems which further expands their industrial applications.Thus,the main objective of this review paper is to present a critical review of current state of research,challenges and opportunities and main directions in SSW of HEAs mainly CoCrFeNiMn and Al_xCoCrFeNi alloys.The state of the art of problems,progress and future outlook in SSW of HEAs are critically reviewed by considering the formation of phases,microstructural evolution and mechanical properties of HEAs joints. 展开更多
关键词 High entropy alloys Solid state welding microstructure mechanical properties
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Effect of Ti,Sc and Zr additions on microstructure and mechanical properties of rheo-diecasting Al-6Zn-2Mg-2Cu alloys 被引量:2
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作者 Sai-heng Hou Jian Feng +2 位作者 Song Chen Fan Zhang Da-quan Li 《China Foundry》 SCIE CAS CSCD 2023年第2期125-133,共9页
The microstructure and mechanical properties of rheo-diecasting Al-6Zn-2Mg-2Cu alloys microalloyed with Ti,Sc and Sc+Zr were studied by optical microscopy(OM),scanning electron microscopy(SEM),X-ray diffraction(XRD),h... The microstructure and mechanical properties of rheo-diecasting Al-6Zn-2Mg-2Cu alloys microalloyed with Ti,Sc and Sc+Zr were studied by optical microscopy(OM),scanning electron microscopy(SEM),X-ray diffraction(XRD),hardness testing,and tensile testing.The swirled equilibrium enthalpy device(SEED)process was introduced to prepare the semisolid slurry.Results show that the addition of Ti,Sc,and Sc+Zr refines the grain size and improves the uniformity of the semisolid slurry and then suppresses the growth of theα-Al grain during solution heat treatment.The microstructure of the four alloys in as-cast state mainly consists of sphericalα-Al and the Mg(Al,Cu,Zn)_(2)(η)eutectic phase.Moreover,primary Al_(3)Sc,Al_(3)(Sc,Zr)and Al_(3)Zr are also found in the micro-alloying alloys.After solution and aging heat treatment,most of the Mg(Al,Cu,Zn)_(2) phases dissolve into theα-Al matrix,while part of Mg(Al,Cu,Zn)_(2) phases transform to Al_(2)CuMg(S)phases.However,the coarse primary Al_(3)Sc and Al_(3)(Sc,Zr)still remain in the matrix,and promote crack initiation and propagation.With the tensile strength of 553 MPa,yield strength of 463 MPa and elongation of 13.4%at T6 state,trace Ti addition generates more attractive mechanical properties than the other three alloys. 展开更多
关键词 Al-Zn-Mg-Cu alloys RHEO-DIECASTING microstructure mechanical properties micro-alloying
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Effect of Ce on microstructure and mechanical properties of Mg-Zn-Ce magnesium alloys 被引量:1
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作者 Hong-fei Wu Wen-xin Hu +4 位作者 Shao-bo Ma Zheng-hua Yang Wei Wang Feng Liu Wei He 《China Foundry》 SCIE CAS CSCD 2023年第4期271-279,共9页
The Mg-6Zn alloy with different contents of Ce was prepared by the gravity casting method,and then the Mg-6Zn-xCe(x=0,0.5,1.0,1.5,wt.%)alloys were extruded at 300℃and 350℃ after solution treatment.The phase constitu... The Mg-6Zn alloy with different contents of Ce was prepared by the gravity casting method,and then the Mg-6Zn-xCe(x=0,0.5,1.0,1.5,wt.%)alloys were extruded at 300℃and 350℃ after solution treatment.The phase constitution and microstructure evolution of Mg-Zn-xCe alloys were analyzed by X-ray diffraction(XRD),scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS)and electron backscattering diffraction(EBSD).Meanwhile,the mechanical properties of the alloy were tested at room temperature.For as-cast alloys,the results show that the main compound in Mg-6Zn alloy is Mg4Zn7 phase,and the main compound is T-(MgZn)12Ce phase after the addition of different amounts of Ce.The microstructure and distribution of second phases are greatly improved after extrusion at 300℃and 350℃.Compared with initial mechanical properties,the strength and elongation increase obviously by means of extrusion at different temperatures.In addition,the microstructure after extrusion at 350℃is further analyzed according to EBSD data.The results show that rare earth element Ce probably promotes the activation of non-basal slip during the deformation process with the increase of Ce,which reduces the strength of basal texture and thus improves the plasticity of the alloy.Meanwhile,the increase of grain boundary migration ability leads to the gradual increase of recrystallization grain size and decreases the strength. 展开更多
关键词 Mg-Zn-Ce EXTRUSION microstructure mechanical properties magnesium alloys
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Synergistically Improved Mechanical Properties and Thermal Conductivity of Hypoeutectic AlSiNiFeMg Alloy Prepared by Ultrasonic-assisted Casting
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作者 ZHANG Wenda YUAN Xuan +4 位作者 ZHOU Yuli ZHONG Gu BAI Peikang WANG Hongfu LIU Jun 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS CSCD 2024年第6期1565-1568,共4页
We employed a melt ultrasonic treatment near the liquidus to prepare a high-thermal-conductivity Al-4Si-2Ni-0.8Fe-0.4Mg alloy.The influences of various ultrasonic powers on its microstructure,mechanical properties,and... We employed a melt ultrasonic treatment near the liquidus to prepare a high-thermal-conductivity Al-4Si-2Ni-0.8Fe-0.4Mg alloy.The influences of various ultrasonic powers on its microstructure,mechanical properties,and thermal conductivity were investigated.It is shown that near-liquidus ultrasonication significantly refines the alloy grains and eutectic structure,synergistically improving the alloy’s mechanical properties and thermal conductivity.Specifically,the grain size decreased by 84.5%from 941.4 to 186.2μm.Increasing the ultrasonic power improved the thermal conductivity of the alloy slightly and significantly enhanced its mechanical properties.At an ultrasonic power of 2100 W,the tensile strength,yield strength,elongation rate,and thermal conductivity were 216 MPa,142 MPa,6.3%,and 169 W/(m·k),respectively. 展开更多
关键词 Al-Si alloy mechanical property thermal conductivity ultrasonic treatment SOLIDIFICATION microstructure
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Microstructures and mechanical properties of Mg-Al-Sm series heat-resistant magnesium alloys 被引量:7
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作者 黄正华 戚文军 +1 位作者 徐静 蔡畅 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2015年第1期22-29,共8页
The microstructures and phase compositions of the as-cast and die-cast Mg-6.02Al-1.03 Sm, Mg-6.05Al-0.98Sm-0.56 Bi and Mg-5.95Al-1.01Sm-0.57 Zn alloys were investigated. Meanwhile, the tensile mechanical and flow prop... The microstructures and phase compositions of the as-cast and die-cast Mg-6.02Al-1.03 Sm, Mg-6.05Al-0.98Sm-0.56 Bi and Mg-5.95Al-1.01Sm-0.57 Zn alloys were investigated. Meanwhile, the tensile mechanical and flow properties were tested. The results show that the as-cast microstructure of Mg-6.02Al-1.03 Sm alloy is composed of δ-Mg matrix, discontinuous δ-Mg17Al12 phase and small block Al2 Sm phase with high thermal stability. Rod Mg3Bi2 phase precipitates when Bi is added, while the added metal Zn dissolves into δ-Mg matrix and δ-Mg17Al12 phase. The as-cast alloys exhibit the excellent tensile mechanical property. The tensile strength(δb) and elongation(δ) can reach 205-235 MPa and 8.5%-16.0% at ambient temperature, respectively. Meanwhile, they can also exceed 160 MPa and 14.0% at 423 K, respectively. The die-cast microstructures are refined obviously, and meanwhile the broken second phases distribute dispersedly. The die-cast alloys exhibit better tensile mechanical properties with the values of δb and δ of 240-285 MPa and 8.5%-16.5% at ambient temperature, respectively, and excellent flow property with the flow length of 1870-2420 mm. The die-cast tensile fractures at ambient temperature exhibit a typical character of ductile fracture. 展开更多
关键词 heat-resistant magnesium alloy Mg-Al-Sm alloy microstructure mechanical property flow property fracture morphology
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Effect of spark plasma sintering temperature on microstructure and mechanical properties of melt-spun TiAl alloys 被引量:1
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作者 柴丽华 陈玉勇 +1 位作者 张来启 林均品 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2012年第3期528-533,共6页
A TiAl alloy from pulverized rapidly solidified ribbons with the composition of Ti-46Al-2Cr-4Nb-0.3Y(mole fraction,%) was processed by spark plasma sintering(SPS).The effects of sintering temperature on the micros... A TiAl alloy from pulverized rapidly solidified ribbons with the composition of Ti-46Al-2Cr-4Nb-0.3Y(mole fraction,%) was processed by spark plasma sintering(SPS).The effects of sintering temperature on the microstructure and mechanical properties were studied.The results show that the microstructure and phase constitution vary with sintering temperature.Sintering the milled powders at 1200 ℃ produces fully dense compact.Higher sintering temperature does not improve the densification evidently.The dominant phases are γ and α2 in the bulk alloys sintered at 1200 ℃.With higher sintering temperature,the fraction of α2 phase decreases and the microstructure changes from equiaxed near γ grain to near lamellar structure,together with a slight coarsening.The bulk alloy sintered at 1260 ℃ with refined and homogeneous near lamellar structure reveals the best overall mechanical properties.The compressional fracture stress and compression ratio are 2984 MPa and 41.5%,respectively,at room temperature.The tensile fracture stress and ductility are 527.5 MPa and 5.9%,respectively,at 800 ℃. 展开更多
关键词 TiAl alloy rapid solidification spark plasma sintering microstructure mechanical properties
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