UV Spectrophotometric Target Factor Analysis （TFA） was used for the simultaneous determination of four components （acetaminophen, guuaifenesin, caffeine, Chlorphenamine maleate） in cough syrup. The computer Frogra...UV Spectrophotometric Target Factor Analysis （TFA） was used for the simultaneous determination of four components （acetaminophen, guuaifenesin, caffeine, Chlorphenamine maleate） in cough syrup. The computer Frogram of TFA is based on VC＋＋ language. The difficulty of overlapping of absorption spectra of four compounds was overcome by this procedure. The experimental results show that the average recovery of each component is all in the range from 98.9% to 106.8% and each component obtains satisfactory results without any pre-separation.展开更多
The increasing importance of endothelium-derived relaxing factor(EDRF),which has now been identified as nitric oxide (NO),has been underscored by the eltlcidation of its role'in a growing number of normal and path...The increasing importance of endothelium-derived relaxing factor(EDRF),which has now been identified as nitric oxide (NO),has been underscored by the eltlcidation of its role'in a growing number of normal and pathophysiological processes. Therefore techniques for detection of nitric oxide should serve as useful tools in defining the role of nitric oxide to these processes.We have improved a simple, sensitive assay methods for determination of nitric oxide in blood, tissue, and other body fluids both by fluorometric and by ultraviolet-visible spectrophotometric measurements. Data obtained by floores cence and by UV-visible assay were correlated well (r=0. 9938, P<0. 0001 ).Linearity:0.1￣ 100μmol/L,r =0.9996,P<0.0001. The minimum detection limit were < 10pmol/L. Within-and between-run CVs were 2. 48%and 4. 62% (n = 10),respectively.Reference values for healthy adults(n=40) were(9.82 ± 1. 57) pmol/L. In conclusion:the methods is sensitive, specific,and precise. It is fairly rapid and simple to perform andrequires no pretreatment of sample, i. e., plasma and urine.The value can be obtained by fluorimeter and/or UV-visible spectrophotometer.The present method is sufficiently rapid and simple to make this a practical choice for many laboratories.展开更多
This paper used atomic absorption spectrophotometry to determine the content distribution of Cu and Cd in the soil of Duanzhou District,Zhaoqing City.The single factor index method,Nemerow comprehensive index method,p...This paper used atomic absorption spectrophotometry to determine the content distribution of Cu and Cd in the soil of Duanzhou District,Zhaoqing City.The single factor index method,Nemerow comprehensive index method,pollution load index method,geoaccumulation index method,and potential ecological hazard index method were used to analyze the content and pollution status of Cu and Cd in the soil of Duanzhou District,providing a basis for understanding the pollution status of Cu and Cd in the soil of Zhaoqing City.展开更多
基金the Science Foundation of Zhejiang Province(No.Y404082)the Science Foundation of Analysis Test of Zhejiang Province(No.03084)
文摘UV Spectrophotometric Target Factor Analysis （TFA） was used for the simultaneous determination of four components （acetaminophen, guuaifenesin, caffeine, Chlorphenamine maleate） in cough syrup. The computer Frogram of TFA is based on VC＋＋ language. The difficulty of overlapping of absorption spectra of four compounds was overcome by this procedure. The experimental results show that the average recovery of each component is all in the range from 98.9% to 106.8% and each component obtains satisfactory results without any pre-separation.
文摘The increasing importance of endothelium-derived relaxing factor(EDRF),which has now been identified as nitric oxide (NO),has been underscored by the eltlcidation of its role'in a growing number of normal and pathophysiological processes. Therefore techniques for detection of nitric oxide should serve as useful tools in defining the role of nitric oxide to these processes.We have improved a simple, sensitive assay methods for determination of nitric oxide in blood, tissue, and other body fluids both by fluorometric and by ultraviolet-visible spectrophotometric measurements. Data obtained by floores cence and by UV-visible assay were correlated well (r=0. 9938, P<0. 0001 ).Linearity:0.1￣ 100μmol/L,r =0.9996,P<0.0001. The minimum detection limit were < 10pmol/L. Within-and between-run CVs were 2. 48%and 4. 62% (n = 10),respectively.Reference values for healthy adults(n=40) were(9.82 ± 1. 57) pmol/L. In conclusion:the methods is sensitive, specific,and precise. It is fairly rapid and simple to perform andrequires no pretreatment of sample, i. e., plasma and urine.The value can be obtained by fluorimeter and/or UV-visible spectrophotometer.The present method is sufficiently rapid and simple to make this a practical choice for many laboratories.
基金Fourth Batch of Innovative Research Teams from Zhaoqing University(TD202408)Quality Engineering and Teaching Reform Project of Zhaoqing University in 2024(zlgc 2024002)+1 种基金2024 School-level Course Ideological and Political Reform Demonstration Project of Zhaoqing University(ZHAOXUEYUAN[2024]83)Notice on the List of Projects for the Construction of Teaching Quality and Teaching Reform in Undergraduate Universities in Guangdong Province in 2021(Yue Jiao Gao Han[2021]29).
文摘This paper used atomic absorption spectrophotometry to determine the content distribution of Cu and Cd in the soil of Duanzhou District,Zhaoqing City.The single factor index method,Nemerow comprehensive index method,pollution load index method,geoaccumulation index method,and potential ecological hazard index method were used to analyze the content and pollution status of Cu and Cd in the soil of Duanzhou District,providing a basis for understanding the pollution status of Cu and Cd in the soil of Zhaoqing City.
