Fe-6.5wt%Si composite compact was fabricated by spark plasma sintering(SPS).Mec hanical alloying(MA)was used to prepare Fe-Si composite powders.The composite p owders were sintered by SPS at elevsated temperature from...Fe-6.5wt%Si composite compact was fabricated by spark plasma sintering(SPS).Mec hanical alloying(MA)was used to prepare Fe-Si composite powders.The composite p owders were sintered by SPS at elevsated temperature from 500℃ to 700℃.The exp erimental results indicate that the non-equilibrium state of composite Fe-Si i s preserved in the compact.The density of the bulk rises with the increasing tem perature and there is no diffusion of silicon and iron in the interface.展开更多
Fe-6.5wt%Si alloy has excellent soft magnetic properties,but it is hard to be cold-rolled due to appearance of ordered phases in this alloy.In this paper we report that ultra thin Fe-6.5wt%Si sheet of 0.05 mm thick wa...Fe-6.5wt%Si alloy has excellent soft magnetic properties,but it is hard to be cold-rolled due to appearance of ordered phases in this alloy.In this paper we report that ultra thin Fe-6.5wt%Si sheet of 0.05 mm thick was obtained by heavily cold rolling.By means of optical microscope,micro-hardness indenter,instron,SEM and X-ray diffraction,the effect of heat treatment on mechanical properties of this alloy sheet was investigated.The heavily cold-rolled sheet exhibits some extent of ductility.The ultimate tensile strength reaches 1.93 GPa.After heat treatment,micro-hardness is decreased and the ductility is lost,especially at temperature above 650℃ when recrystallization takes place.The reason for decreasing the ductility lies in the ordered DO3 phase transformation.展开更多
基金Funded by the National Natural Science Foundation of China(No.50232020)and the State"863"H tech.Project(No.2002AA327080)
文摘Fe-6.5wt%Si composite compact was fabricated by spark plasma sintering(SPS).Mec hanical alloying(MA)was used to prepare Fe-Si composite powders.The composite p owders were sintered by SPS at elevsated temperature from 500℃ to 700℃.The exp erimental results indicate that the non-equilibrium state of composite Fe-Si i s preserved in the compact.The density of the bulk rises with the increasing tem perature and there is no diffusion of silicon and iron in the interface.
基金supported by the National Basic Research Program of China ("973" Project)(Grant No 2006CB605205-2)the National Natural Science Foundation of China (Grant No 50771018)
文摘Fe-6.5wt%Si alloy has excellent soft magnetic properties,but it is hard to be cold-rolled due to appearance of ordered phases in this alloy.In this paper we report that ultra thin Fe-6.5wt%Si sheet of 0.05 mm thick was obtained by heavily cold rolling.By means of optical microscope,micro-hardness indenter,instron,SEM and X-ray diffraction,the effect of heat treatment on mechanical properties of this alloy sheet was investigated.The heavily cold-rolled sheet exhibits some extent of ductility.The ultimate tensile strength reaches 1.93 GPa.After heat treatment,micro-hardness is decreased and the ductility is lost,especially at temperature above 650℃ when recrystallization takes place.The reason for decreasing the ductility lies in the ordered DO3 phase transformation.
