Ternary Pb-Sn-Cd alloy nanoparticles were prepared b y the sonochemical dispersion method. The nanoparticles were found to be about 40 —60 nm and coated with an amorphous layer of surfactant dioctadecyldithiophosph a...Ternary Pb-Sn-Cd alloy nanoparticles were prepared b y the sonochemical dispersion method. The nanoparticles were found to be about 40 —60 nm and coated with an amorphous layer of surfactant dioctadecyldithiophosph ate(DDP).The formation and constituent of the as-prepared nanoalloy were charac terized by transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), X-ray diffraction (XRD), differential thermal anal ysis and thermogravimetry (DTA-TG), and Fourier transform infrared (FT-IR) spe ctrophotometer.It was also found that the powder showed excellent antiwear prope rty by tribological test results.展开更多
研究了钨含量为36%,Ni与Fe质量比为7/3和9/1的两种W Ni Fe三元合金的预应变时效硬度变化规律,用X射线衍射鉴定了时效后两种合金的物相组成,并用透射电镜观察其微观结构。结果表明:Ni与Fe质量比为7/3的W Ni Fe三元合金在800℃下进行预应...研究了钨含量为36%,Ni与Fe质量比为7/3和9/1的两种W Ni Fe三元合金的预应变时效硬度变化规律,用X射线衍射鉴定了时效后两种合金的物相组成,并用透射电镜观察其微观结构。结果表明:Ni与Fe质量比为7/3的W Ni Fe三元合金在800℃下进行预应变时效时,硬度随时间增加而单调降低;相同条件下Ni与Fe质量比为9/1的W Ni Fe三元合金时效初期硬度下降,但随时间延长硬度又逐步提高。X射线衍射物相鉴定和透射电子显微分析发现:Ni与Fe质量比为7/3的合金在预应变时效过程中没有明显沉淀析出物,其时效硬度下降是固溶度降低、残余应力消除以及回复与再结晶的结果;而Ni与Fe质量比为9/1的合金经预应变时效后析出了细小弥散的β相,其硬度变化存在两种机制,一种是固溶度降低、残余应力消除和回复与再结晶引起软化,另一种是细小β相沉淀析出导致弥散强化。展开更多
文摘Ternary Pb-Sn-Cd alloy nanoparticles were prepared b y the sonochemical dispersion method. The nanoparticles were found to be about 40 —60 nm and coated with an amorphous layer of surfactant dioctadecyldithiophosph ate(DDP).The formation and constituent of the as-prepared nanoalloy were charac terized by transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), X-ray diffraction (XRD), differential thermal anal ysis and thermogravimetry (DTA-TG), and Fourier transform infrared (FT-IR) spe ctrophotometer.It was also found that the powder showed excellent antiwear prope rty by tribological test results.
文摘研究了钨含量为36%,Ni与Fe质量比为7/3和9/1的两种W Ni Fe三元合金的预应变时效硬度变化规律,用X射线衍射鉴定了时效后两种合金的物相组成,并用透射电镜观察其微观结构。结果表明:Ni与Fe质量比为7/3的W Ni Fe三元合金在800℃下进行预应变时效时,硬度随时间增加而单调降低;相同条件下Ni与Fe质量比为9/1的W Ni Fe三元合金时效初期硬度下降,但随时间延长硬度又逐步提高。X射线衍射物相鉴定和透射电子显微分析发现:Ni与Fe质量比为7/3的合金在预应变时效过程中没有明显沉淀析出物,其时效硬度下降是固溶度降低、残余应力消除以及回复与再结晶的结果;而Ni与Fe质量比为9/1的合金经预应变时效后析出了细小弥散的β相,其硬度变化存在两种机制,一种是固溶度降低、残余应力消除和回复与再结晶引起软化,另一种是细小β相沉淀析出导致弥散强化。
