Research on the Performance of New Weighted Slippery Water Fracturing Fluid System

Deep and ultra-deep reservoirs have dense matrix and high fracture pressure, which leads to high pressure and difficulty in fracturing construction. Conventional aggravated fracturing fluids have the problems of low aggravation efficiency, high friction resistance, etc., and the reduction of construction pressure cannot reach the theoretical effect. In view of the above problems, this paper adopts the weighting agent HD160 and the drag reducing agent JHFR-2 to form a new type of weighted slippery water fracturing fluid system. And the weighting performance, drag reduction performance, corrosion performance, anti-expansion performance and reservoir damage of this system were studied. The results show that the density of the system is adjustable within 1.1 - 1.6 g·cm−3, and the drag reduction rate can be up to 68% at 1.5 g·cm−3, with low corrosion rate, surface tension less than 28 mN·m−1, anti-expansion rate as high as 94.5%, and the damage rate of the reservoir permeability is less than 10%, which is of good application prospect.

Numerical Modelling of Ore-forming Dynamics of Fractal Dispersive Fluid Systems

Based on an analysis of the fractal structures and mass transport mechanism of typical shear-fluid-ore formation system, the fractal dispersion theory of the fluid system was used in the dynamic study of the ore formation system. The model of point-source diffusive illuviation of the shear-fluid-ore formation system was constructed, and the numerical simulation of dynamics of the ore formation system was finished. The result shows that: (1) The metallogenic system have nested fractal structure. Different fractal dimension values in different systems show unbalance and inhomogeneity of ore-forming processes in the geohistory. It is an important parameter to symbolize the process of remobilization and accumulation of ore-forming materials. Also it can indicate the dynamics of the metallogenic system quantitatively to some extent. (2) In essence, the fractal dispersive ore-forming dynamics is a combination of multi-processes dominated by fluid dynamics and supplemented by molecule dispersion in fluids and fluid-rock interaction. It changes components and physico-chemical properties of primary rocks and fluids, favouring deposition and mineralization of ore-forming materials. (3) Gold ore-forming processes in different types of shear zones are quite different. (1) In a metallogenic system with inhomogeneous volumetric change and inhomogeneous shear, mineralization occurs in structural barriers in the centre of a shear zone and in geochemical barriers in the shear zone near its boundaries. But there is little possibility of mineralization out of the shear zone. (2) As to a metallogenic system with inhomogeneous volumetric change and simple shear, mineralization may occur only in structural barriers near the centre of the shear zone. (3) In a metallogenic system with homogeneous volumetric change and inhomogeneous shear, mineralization may occur in geochemical barriers both within and out of the shear zone.

Late Paleozoic Fluid Systems and Their Ore-forming Effects in the Yuebei Basin,Northern Guangdong,China

Based on detailed and systematic researches of the geology of ore deposits, fluid inclusions and isotope geochemistry etc., and regarding the Late Paleozoic fluid system of the Yuebei Basin as an integrated object in this paper, we have revealed the temporo-spatial evolution law of the basin＇s fluid system and discussed its ore-forming effects by simulating and analyzing the distribution of ore-forming elements, the fluid thermodynamics and dynamics of evolution processes of this basin. The results show that Late Paleozoic ore-forming fluid systems of the Yuebei Basin include four basic types as follows. （1） The sea floor volcanic-exhalation system developed during the rapid basin slip-extension stage in the Mid-Late Devonian, which affected the Dabaoshan region. It thus formed the Dabaoshan-type Cu-Pb-Zn-Fe sea floor volcanic-exhalation sedimentary deposits. （2） The compaction fluid system developed during the stable spreading and thermal subsidence-compression stage of the basin in the Mid-Late Devonian. The range of its effects extended all over the whole basin. It resulted in filling-metasomatic deposits, such as the Hongyan-type pyrite deposits and pyrite sheet within the Fankou-type Cu-Pb-Zn-S deposits. （3） The hot water circulation system of sea floor developed during the stage of basin uplifting and micro-aulacogen from the late Late Carboniferous to Middle Carboniferous. The range of its effects covered the Fankou region. It thus formed MVT deposits, such as the main orebody of the Fankou-type Pb-Zn-S deposits. （4） The gravity fluid system developed during the stage of fold uplifting and the basin closed from Middle Triassic to Jurassic, forming groundwater hydrothermal deposits, e.g. the veinlet Pb-Zn-calcite orebodies of the Fankou-type Pb-Zn- S deposits. Migration and concentration of the ore-forming fluids were constrained by the state of temporo-spatial distribution of its fluid potential. Growth faults not only converged the fluids and drove them to move upwards, but also the fluids often crossed the faults to the edges of the basin at the bottom of these faults and the lithologic interfaces, and even migrated to the basin＇s edges from top to bottom along the faults, which may be one of the basic reasons for the stratabound deposits to cluster mainly along the contemporaneous faults on the inner border of the basin. The superposed mineralization resulting from the multi-stage activity of contemporaneous faults and ore-forming fluid systems in the basin may be one of the key factors for forming superlarge ore deposits.

Ore-forming Fluid Systems and Mineralization in the Eastern Jiangnan Uplift in the Border Area of Anhui and Jiangxi Provinces, China

Obvious differences in mineralization characteristics exist between the southern and northern parts of the eastern part of the Jiangnan Uplift in northern Jiangxi Province and southern Anhui Province. The regional metallogeny is discussed, and the ore-forming fluid systems are classified in this article. It is proposed that the fluid ore-forming activities in the Jiangnan Uplift both in northern Jiangxi and southern Anhui have close relationships with the crust-mantle interaction and magmatic-tectonic activities. The types and scales of the mineralization on the both sides of the eastern Jiangnan Uplift were determined by fluid ore-forming systems and geological backgrounds.

Laboratory Research on the Performance of Fracturing Fluid System for Unconventional Oil and Gas Reservoir Transformation

Fracturing fluid is the blood of fracturing construction, which is very important for fracturing, which requires that fracturing fluid needs to have good performance. The three commonly used fracturing fluids for unconventional oil and gas reservoir transformation are: 1) Guar gum fracturing fluid;2) Water-based emulsion slippery water fracturing fluid;3) Oil-based emulsion slippery water fracturing fluid. In this paper, water samples and other experimental data provided by Mahu Oilfield are used to evaluate three different fracturing fluid systems in laboratory. The formulas of the three different fracturing fluid systems are: 1) Water-based emulsion slippery water fracturing fluid is clean slippery water fracturing fluid 0.1% JHFR-2D drag reducer + 0.2% JHFD-2 multifunctional additive;2) Oil-based emulsion slippery water fracturing fluid 0.1% A agent + 0.2% B agent;3) Guar gum fracturing fluid 0.1% guanidine gum + 0.5% drainage aid + 0.3% demulsifier. The compatibility, drag reduction performance, reservoir damage, residue content, anti-swelling performance, surface interfacial tension, viscosity and other properties of three different slippery water fracturing fluid systems were studied. Through laboratory experiments, the comprehensive indicators show that clean slippery water fracturing fluid has obvious advantages.

A kind of extended Korteweg-de Vries equation and solitary wave solutions for interfacial waves in a two-fluid system

This paper considers interfacial waves propagating along the interface between a two-dimensional two-fluid with a flat bottom and a rigid upper boundary. There is a light fluid layer overlying a heavier one in the system, and a small density difference exists between the two layers. It just focuses on the weakly non-linear small amplitude waves by introducing two small independent parameters： the nonlinearity ratio ε, represented by the ratio of amplitude to depth, and the dispersion ratio μ, represented by the square of the ratio of depth to wave length, which quantify the relative importance of nonlinearity and dispersion. It derives an extended KdV equation of the interfacial waves using the method adopted by Dullin et al in the study of the surface waves when considering the order up to O（μ^2）. As expected, the equation derived from the present work includes, as special cases, those obtained by Dullin et al for surface waves when the surface tension is neglected. The equation derived using an alternative method here is the same as the equation presented by Choi and Camassa. Also it solves the equation by borrowing the method presented by Marchant used for surface waves, and obtains its asymptotic solitary wave solutions when the weakly nonlinear and weakly dispersive terms are balanced in the extended KdV equation.

Validity ranges of interfacial wave theories in a two-layer fluid system

In the present paper, we endeavor to accomplish a diagram, which demarcates the validity ranges for interfacial wave theories in a two-layer system, to meet the needs of design in ocean engineering. On the basis of the available solutions of periodic and solitary waves, we propose a guideline as principle to identify the validity regions of the interfacial wave theories in terms of wave period T, wave height H, upper layer thickness dl, and lower layer thick-ness d2, instead of only one parameter-water depth d as in the water surface wave circumstance. The diagram proposed here happens to be Le Mehaute＇s plot for free surface waves if water depth ratio r= d1/d2 approaches to infinity and the upper layer water density p1 to zero. On the contrary, the diagram for water surface waves can be used for two-layer interfacial waves if gravity acceleration g in it is replaced by the reduced gravity defined in this study under the condition of σ=（P2 - Pl）/P2 → 1.0 and r 〉 1.0. In the end, several figures of the validity ranges for various interfacial wavetheories in the two-layer fluid are given and compared with the results for surface waves.

A Coupled Variable Coefficient Modified KdV Equation Arising from a Two-Layer Fluid System

A quite general coupled variable coefficient modified KdV (VCmKdV) equation in a two-layer fluid systemis derived by means of the reductive perturbation method.Making use of the CK's direct method,some similarityreductions of the coupled VCmKdV equation are obtained and their corresponding group explanations are discussed.Some exact solutions of the coupled equations are also presented.

The study of formulation and performance of formate drilling and completion fluid system

Formate drilling and completion fluid system is a new type of clean organic salt brine system which has been developed from inorganic salt brine drilling fluid system. It is beneficial to protecte and find hydrocarbon reservoir. Due to the solid free system, the damage of solid phase particles on reservoir, especially low permeability oil and gas layer, can be greatly eliminated, at the same time, drilling fluid and completion fluid have greater compatibility. It will avoid that precipitation which is not compatible with drilling and completion fluid and generates damages on reservoir. And because mud cake of the solid free system is thin and resilient, it is conductive to improve cementing quality greatly. Experiments show that the formate drilling and completion system has good rheological property, strong inhibition ability, good lubricating performance, good compatibility with reservoir rocks and formation water at high temperature.

Higher-order Boussinesq-type equations for interfacial waves in a two-fluid system

Interracial waves propagating along the interface between a three-dimensional two-fluid system with a rigid upper boundary and an uneven bottom are considered. There is a light fluid layer overlying a heavier one in the system, and a small density difference exists between the two layers. A set of higher-order Boussinesq-type equations in terms of the depth-averaged velocities accounting for stronger nonlinearity are derived. When the small parameter measuring frequency dispersion keeping up to lower-order and full nonlinearity are considered, the equations include the Choi and Camassa＇s results （1999）. The enhanced equations in terms of the depth-averaged velocities are obtained by applying the enhancement technique introduced by Madsen et al. （1991） and Schaffer and Madsen （1995a）. It is noted that the equations derived from the present study include, as special cases, those obtained by Madsen and Schaffer （1998）. By comparison with the dispersion relation of the linear Stokes waves, we found that the dispersion relation is more improved than Choi and Camassa＇s （1999） results, and the applicable scope of water depth is deeper.

Influence of the earth rotation on the interfacial wave solutions and wave-induced tangential stress in a two-layer fluid system

Interfacial waves and wave-induced tangential stress are studied for geostrophic small amplitude waves of two-layer fluid with a top free surface and a fiat bottom. The solutions were deduced from the general form of linear fluid dynamic equations of two-layer fluid under the f-plane approximation, and wave-induced tangential stress were estimated based on the solutions obtained. As expected, the solutions derived from the present work include as special cases those obtained by Sun et al. （2004. Science in China, Ser. D, 47（12）： 1147-1154） for geostrophic small amplitude surface wave solutions and wave-induced tangential stress if the density of the upper layer is much smaller than that of the lower layer. The results show that the interface and the surface will oscillate synchronously, and the influence of the earth＇s rotation both on the surface wave solutions and the interfacial wave solutions should be considered.

A solids-free brine drilling fluid system for coiled tubing drilling

There are many problems associated with coiled tubing drilling operations, such as great circulation pressure loss inside pipe, difficulties in weight on bit(WOB) transferring, and high probability of differential sticking. Aiming at these problems, solids-free brine drilling fluid system was developed on the basis of formulation optimization with brine base fluid experiment, which was evaluated and applied to field drilling. Based on the optimization of flow pattern regulator, salt-resisting filtrate reducer, high performance lubricant and bit cleaner, the basic formula of the solids-free brine drilling fluid system was formed: brine +(0.1%-0.2%) Na OH +(0.2%-0.4%) HT-XC +(2.0%-3.0%) YLJ-1 +(0.5%-2.0%) SDNR +(1.0%-2.5%) FT-1 A +(1.0%-5.0%) SD-505 + compound salt density regulator. Lab evaluation showed that the fluid had satisfactory temperature resistance(up to 150 ℃), excellent cuttings tolerance(up to 25%), and strong inhibition(92.7% cuttings recovery); Moreover, its lubrication performance was similar to that of all oil-based drilling fluid. The wellbore could be fairly cleaned at annular up-flow velocity of more than 0.8 m/s if the ratio of yield point to plastic viscosity was kept above 0.5. This fluid system has been applied in the drilling of three coiled tubing sidetracking wells in the Liaohe Oilfield, during which the system was stable and easy to adjust, resulting in excellent cuttings transportation, high ROP, regular hole size, and no down hole accidents. In summary, the solids-free brine drilling fluid system can meet the technical requirements of coiled tubing drilling.

Research and Application of Fuling Shale Gas Anti-Collapse and Anti-Leakage Drilling Fluid System

Aiming at the problems of microfracture development in hard brittle shale gas layer in Fuling block, Chongqing, such as collapse of borehole wall and the existence of permeability loss of microfracture during drilling, and serious pollution of drilling environment with oil-based drilling fluid, a water-based drilling fluid system for anti-collapse and anti-leakage was studied. A water-based drilling fluid system with anti-collapse and anti-leakage was formed by introducing functional treatment agents, such as polypolysaccharide MEG, polymer emulsion film forming wall cementing agent LFGB, polyamine inhibitor LCFA and deformable particle plugging agent BXLZ, into the conventional water-based drilling fluid. After rolling at 130°C for 16 h, the system has good rheological properties, low filtration loss, good inhibition, lubrication and plugging properties. It has good plugging properties for 0.12 mm, 0.24 mm, 0.38 mm micro-cracks and 400 mD and 800 mD sand plates. The system was successfully tested on site in August 2019 in Fuling Reef Block, showing good rheological properties, solid wall plugging, and strong ability to seal and inhibit fracture expansion. There was no block falling in the drilling process, and the tripping, casing running and well cementing operations were all smooth, which provided a new technical idea and scheme for environmental protection and green drilling in Fuling shale gas exploitation.

GLOBAL EXISTENCE AND OPTIMAL CONVERGENCE RATES OF SOLUTIONS FOR THREE-DIMENSIONAL ELECTROMAGNETIC FLUID SYSTEM

In this article, we study the electromagnetic fluid system in three-dimensional whole space R^3. Under assumption of small initial data, we establish the unique global solution by energy method. Moreover, we obtain the time decay rates of the higher-order spatial derivatives of the solution by combining the L^p-L^q estimates for the linearized equations and an elaborate energy method when the L^1-norm of the perturbation is bounded.

LARGE TIME BEHAVIOR OF A THIRD GRADE FLUID SYSTEM

We consider the large time behavior of a non-autonomous third grade fluid sys- tem, which could be viewed as a perturbation of the classical Navier-Stokes system. Under proper assumptions, we firstly prove that the family of processes generated by the problem ad- mits a uniform attractor in the natural phase space. Then we prove the upper-semicontinuity of the uniform attractor when the perturbation tends to zero.

Ore-Fluid Systems of Fine Disseminated Gold Deposits Along the Southeastern Margin of the Yangtze Plate

Fine disseminated gold deposits occurring along the southeastern margin ofthe Yangtze Plate belong to the epithermal type resulting from different systems of oreforming fluids. According to their sources, the ore-forming fluids can be divided intofour systems: a) meteoric water system; b) oil-brine system; c) basin-brine system; andd) magmatic-formation water system. The four hydrothermal systems are responsiblefor four types of gold deposits, respectively The meteoric water system produces hotspring gold deposits. The basin-brines, which are derived from fissure water, structuralwater and absorbed water sealed up in strata, are responsible for the basin-brine-typedeposits. The oil-brine system, having the same source as the basin-brines, is characterizedby the involvment of organic matter and is responsible for the oil-brine-type deposits.Inclusion fluld data show that there are obvious differences in chemical compesition andcarbon, oxygen, hydrogen and sulfur isotopes for these hydrothermal systems. Differentmetalloenic provinces, in which one of the four systems is dominant, can be recognizedin the region.

The biodiesel-based flat-rheology drilling fluid system

As the base oil of the current flat-rheology synthetic drilling fluid is high in cost and not renewable, the biodiesel-based flat-rheology drilling fluid with low-cost, environmental protection and renewable advantage was studied. Based on the optimization of raw materials, a cheap, environment-friendly biodiesel of soybean oil ethyl ester with good fluidity at low temperature was selected as the base oil. By selecting high oil-water ratio and introducing cationic surfactant into the auxiliary emulsifier, the thickening of biodiesel-based emulsion caused by hydrolysis and saponification after high-temperature aging was effectively eliminated. The organoclay prepared with cationic modifier of hexadecyl trimethyl ammonium chloride was used to improve the rheologic properties, stability and fluid loss of the drilling fluid while preventing low-temperature thickening. A flat-rheology modifier was synthesized with dimer fatty acid and cocoanut fatty acid diethanolamide, which could form strong network structure in the biodiesel-based drilling fluid to adjust effectively rheological properties of the drilling fluid. A biodiesel-based flat-rheology drilling fluid system with the density of 1.2 g/cm^(3) has been formulated which has constant rheology in the temperature range of 2-90 ℃, temperature tolerance of 160 ℃, seawater salinity tolerance of 5%, shale cuttings tolerance of 10%, and is environmentally friendly.

The Research of Anti-Swelling and Low Damage Killing Fluid System

In this paper, we introduced reservoir characteristics in Block Xiao-he-long and evaluate the performance of the existing killing fluid system. According to the production requirements, a anti-swelling and low damaging system of chemical agents suitable for this block was optimized, including anti-swelling agent, water lock inhibitor, fluid-loss agent additives, plus a corrosion inhibitor HS-1 developed by in the lab. The system is composed by base liquid (0.7%X + 2.0%KCl +0.05%SY-1+ 0.05%HS-1+2.0% DST-1 dissolved in water) and weighting material (NaCl) with its density adjustable range between 1.0g/ml and 1.2g/ml. Its anti-swelling ratio achieves 53.80%, and the reservoir permeability recovery ratio reaches more than 95.0%.

Optimization of Anti-Collapse Drilling Fluid Systems with High Potassium Content

The ash mudstone in some oil formations is highly water-sensitive.The oil formation is fractured,and the risk of well leakage and collapse is not negligible.This study presents a countermeasure for well collapse prevention,based on a“force-chemistry synergistic balance”approach and the utilization of environmentally friendly and efficient hydration inhibitors.The relevance of this approach is demonstrated considering a drilling fluid system with the high potassium content.The analysis shows that the system can maintain good rheological properties,filtration loss and suspension stability even after aging at 130℃ for 16 h.The primary roll recovery of rock chips is better than 98%.The secondary rolling recovery rate is 89%.The rapid water loss is close to zero.The effects of carrying rock,sand,hydration inhibition and dispersion of drill chips are all noticeable.

EXPERIMENTAL GEOCHEMISTRY STUDY ON GOLD IN WATER-ROCK REACTION UNDER THERMAL FLUID SYSTEM AT MESO-LOW TEMPERATURE

Based on the knowing geochemical characteristics of wall rock in the Mobin gold deposit and composition of fluid inclusion in ore,water rock experiments were carried out, important achievements are acquired as following: Gold is mainly derived from the ore bearing wall rock,i.e., a series of epimetamorphic clastic gritstone, sandy slate, and tuffaceous slate in the Wuqiang Banxi Formation, Wuqiangxi Group. In thermal system with middle low temperature chlorine gold may be derived form stable complex ions, so it is quite important in gold metallogenic process. Sulphur and chlorine perform as the major negative ions throughout the gold activation and migration movement. The concentration of sulphur and chlorine ions, pH value and temperature are of deciding significance for gold activation, migration and precipitation.