Surface modification of Cu-25Cr alloy induced by high current pulsed electron beam

A Cu-25Cr alloy prepared by vacuum induction melting method was treated by the high current pulsed electron beam （HCPEB） with pulse numbers ranging from 1 to 100. Surface morphologies and microstructures of the alloy before and after the treatment were investigated by scanning electron microscopy and X-ray diffraction. The results show that significant surface modification can be induced by HCPEB with the pulse number reaching 10. Craters with typical morphologies on the Cu-25Cr alloy surface are formed due to the dynamic thermal field induced by the HCPEB. Micro-cracks, as a unique feature, are well revealed in the irradiated Cu-25Cr specimens and attributed to quasi-static thermal stresses accumulated along the specimen surface. The amount of cracks is found to increase with the pulse number and a preference of these cracks to Cr phases rather than Cu phases is also noted. Another characteristic produced by the HCPEB is the fine Cr spheroids, which are determined to be due to occurrence of liquid phase separation in the Cu-25Cr alloy. In addition, an examination on surface roughness of all specimens reveals that more pulses will produce a roughened surface, as a result of compromising the above features.

Compounded Surface Modification of ZK60 Mg Alloy by High Current Pulsed Electron Beam+Micro-plasma Oxidation

In this study, compounded surface modification technology-high current pulsed electron beam （HCPEB） ＋ micro-plasma oxidation （MPO） was applied to treat ZK60 Mg alloys. The characteristics of the microstructure of ZK60 Mg alloy after single MPO and HCPEB＋MPO compounded treatment were investigated by SEM. The results showed that the density of the ceramic layer of HCPEB＋MPO-treated ZK60 Mg alloy was improved and defects were reduced compared to that under MPO treatment alone. Surface modified layer of ZK60 Mg alloys treated by HCPEB＋MPO was divided into three zones, namely the top loose ceramic zone, middle compact zone and inside HCPEB-induced melted zone. Corrosion resistance of ZK60 Mg alloy before and after the compounded surface modification was measured in a solution of 3.5% NaCl by potentiodynamic polarization curves. It was found that the corrosion current density of ZK60 Mg alloys could be reduced by about three orders of magnitude, from 311μA/cm^2 of the original sample to 0.2μA/cm^2 of the HCPEB＋MPO-treated sample. This indicates the great application potential of the HCPEB＋MPO compounded surface modification technology in improving the corrosion resistance of ZK60 Mg alloys in the future.

Characterizing modified surface layer of 316L stainless steel treated by high current pulsed electron beam

High current pulsed electron beam(HCPEB) is now developing as a useful tool for surface modification of materials.When concentrated electron flux transferring its energy into the surface layer of target material within a short pulse time,coupled thermal and stress processes would lead to the formation of metastalbe microstructure with improved properties.In the present work,HCPEB treatment of 316L stainless steel(SS) was carried out and the microstructural changes in modified surface layer were characterized with optical microscopy,X-ray diffractometry and electron backscatter diffractometry(EBSD) techniques.The corrosion resistance of modified surface was measured in a 5wt.% salt solution.The evolution regularity of surface craters and grain refinement effect,as well as the preferred orientation of(111) crystal plane occurring in the HCPEB treatment under different working parameters were discussed along with their influence on corrosion resistance.

Microstructure and properties of Nb/Ta multilayer films irradiated by a high current pulse electron beam

Nb/Ta multilayer films deposited on Ti6A14V substrate with Nb and Ta monolayer thicknesses of 30 nm, 120 nm, and 240 nm were irradiated by a high current pulse electron beam （HCPEB） to prepare Nb-Ta alloyed layers. The mi- crostructure and the composition of the outmost surface of melted alloyed layers were investigated using a transmission electron microscope （TEM） equipped with an X-ray energy dispersive spectrometer （EDS） attachment. The Ta content of the alloyed surface layer prepared from the monolayer of thickness 30 nm, 120 nm, and 240 nm was- 27.7 at.%, 6.37 at.%, and 0 at.%, respectively. It was found that the Ta content in the alloyed layer plays a dominant role in the microstructure of the films. The hardness and the wear rate of the alloyed layers decrease with the increasing content of Ta in the surface laver.

Ultra Fast Shutter Driven by Pulsed High Current

Radiation simulation utilizing plasma radiation sources (PRS) generates a large number of undesirable debris, which may damage the expensive diagnosing detectors. An ultra fast shutter (UFS) driven by pulsed high current can erect a physical barrier to the slowly moving debris after allowing the passage of X-ray photons. The UFS consists of a pair of thin metal foils twisting the parallel axes in a Nylon cassette, compressed with an outer magnetic field, generated from a fast capacitor bank, discharging into a single turn loop. A typical capacitor bank is of 7.5μF charging voltages varying from 30 kV to 45 kV, with corresponding currents of approximately 90 kA to140 kA and discharging current periods of approximately 13.1μs. A shutter closing time as fast as 38 microseconds has been obtained with an aluminium foil thickness of 100 micrometers and a cross-sectional area of 15 mm by 20 mm. The design, construction and the expressions of the valve-closing time of the UFS are presented along with the measured results of valve-closing velocities.

Numerical Calculation and Experimental Research on Crack Arrest by Detour Effect and Joule Heating of High Pulsed Current in Remanufacturing

The remanufacturing blanks with cracks were considered as irreparable. With utilization of detour effect and Joule heating of pulsed current, a technique to arrest the crack in martensitic stainless steel FV520B is developed. According to finite element theory, the finite element（FE） model of the cracked rectangular specimen is established firstly. Then, based on electro-thermo-structure coupled theory, the distributions of current density, temperature field, and stress field are calculated for the instant of energizing. Furthermore, the simulation results are verified by some corresponding experiments performed on high pulsed current discharge device of type HCPD-I. Morphology and microstructure around the crack tip before and after electro pulsing treatment are observed by optical microscope（OM） and scanning electron microscope（SEM）, and then the diameters of fusion zone and heat affected zone（HAZ） are measured in order to contrast with numerical calculation results. Element distribution, nano-indentation hardness and residual stress in the vicinity of the crack tip are surveyed by energy dispersive spectrometer（EDS）, scanning probe microscopy（SPM） and X-ray stress gauge, respectively. The results show that the obvious partition and refined grain around the crack tip can be observed due to the violent temperature change. The contents of carbon and oxygen in fusion zone and HAZ are higher than those in matrix, and however the hardness around the crack tip decreases. Large residual compressive stress is induced in the vicinity of the crack tip and it has the same order of magnitude for measured results and numerical calculation results that is 100 MPa. The relational curves between discharge energies and diameters of the fusion zone and HAZ are obtained by experiments. The difference of diameter of fusion zone between measured and calculated results is less than 18.3%. Numerical calculation is very useful to define the experimental parameters. An effective method to prevent further extension of the crack is presented and can provide a reference for the compressor rotor blade remanufacturing.

Microstructure and property modifications in surface layers of a Mg-4Sm-2Al-0.5Mn alloy induced by pulsed electron beam treatments

In this work,surface modification of a Mg-4Sm-2Al-0.5Mn alloy with high current pulse electron beam(HCPEB)under different number of pulses were investigated.The evolution in microstructure,composition and phase components and properties in the surface layer before and after HCPEB treatment were characterized.It was found that the Al 11 Sm 3 and Al 2 Sm phases in the surface layer were gradually dissolved during HCPEB treatment,leading to the formation of a chemical homogeneous melted layers.Besides,deformation bands were formed in the treated layer due to the thermal stress generated during treatment.After 15 pulses treatment,the surface hardness increases to the maximum value of about 62.2 HV,about 61.2%higher than that of the untreated state.Electrochemical results show that the 15 pulses treated sample presents the best corrosion resistance in the 3.5wt%NaCl water solution by showing the highest corrosion potential(E_(corr))of-1.339V SEC and the lowest corrosion current density(I_(corr))of 1.48×10^(-6)A·cm^(-2).The results prove that the surface properties of the Mg-4Sm-2Al-0.5Mn alloy can be significantly improved by the HCPEB treatments under proper conditions.

Effect of pulse frequency on hardness characteristics of Al-Cu alloy HPVP-GTAW joints

AA 2219-0 Al-Cu alloy single bead welds were obtained by hybrid ultrahigh frequency pulse variable polarity gas tungsten arc welding （HPVP-GTAW） process with pulse frequency varying from 25 kHz to 70 kHz. Weld hardness characteristics which mainly depicted by microhardness and its gradient were investigated systematically. The results show that pulse frequency has a great effect on the hardness characteristics. The weld zone microhardness and its gradient with different pulse frequency present an evident fluctuant trend. The fluctuation of gradient is slight, illustrating that the mierostructure is uniform with pulse frequcncy varied from 35 kHz to 60 kHz. The fusion zone microhardness and its gradient foUow the similar trends but fluetuate greatly. Maximum value of gradient appears around the fusion boundary due to the coarse and non- uniform microstrueture. The maximum gradient at 60 kHz is only 25.5 % of that at 45 kHz. According to the study, the best hardness characteristics are achieved at 60 kHz frequency.

A Control System Design to Establish Dose-Response Relationships in Wound Healing Therapy

Advanced biophysical wound healing therapies can apply mechanical, electrical, or light energy to re-stimulate healing processes in chronic wounds. Despite the growing evidence of the clinical efficacy of these therapies, the optimal treatment stimulation parameters remain unknown and there are no standard treatment protocols. We introduce a closed-loop control design as an experimental system to study the dose-response of wound healing therapy treatment within a prescribed multidimensional and multimodal stimulation parameter space. Systems engineering approaches are applied to the control problem for estimation of a transfer function and model equations derived for use in optimal model-based control. The experimental control system design consisted of simultaneous application of biophysical energies inputted into a wound system. A study design set up including the use of negative pressure wound therapy, electrical stimulation therapy, and photobiomodulation device systems was described. Treatment stimulation parameters were selected from experimental ranges used in the scientific literature. Classical control methods and model-based control were suggested for model selection and evaluation and design of the overall control system. An experimental design for multimodal biophysical wound healing therapy control system is introduced to establish the dose-response interactions for development of therapeutic applications and device design.

Measurement of emittance at CSNS ion source without analyzing magnet

Purpose High current beam is required for CSNS update in future.Over 50 mA H-will be designed to deliver to the linac in CSNSⅡ.For the present state of CSNS ion source,the beam emittance cannot satisfy the requirement of RFQ entrance at the 50 mA H-beam.In order to improve the beam quality,CSNS ion source is required further improvement.Methods Simulation shows emittance growth due to the space charge force in the intense H-beam when the beam transports through the analyzing magnet.After considering the neutralization of space charge,the emittance growth could be suppressed.The analyzing magnet thus is considered to removed,which might destroy the neutralization of space charge.The beam emittance is measured at the revised CSNS ion source.Results Measured results show that beam emittance without the analyzing magnet becomes smaller than that of CSNS ion source.At the requirement of 0.2πmm mrad,beam current is larger than 30 mA.It reveals that analyzing magnet could destroy space charge neutralization and result in the significant increase of emittance.Conclusions Although the results presented are preliminary,it is important to improve the beam quality.This paper details the ion source improvement and measurement process.