PT fuel injector is one of the most important parts of modern diesel engine.To satisfy the requirements of the rapid and accurate test of PT fuel injector,the self-adaptive floating clamping mechanism was developed an...PT fuel injector is one of the most important parts of modern diesel engine.To satisfy the requirements of the rapid and accurate test of PT fuel injector,the self-adaptive floating clamping mechanism was developed and used in the relevant bench.Its dynamic characteristics directly influence the test efficiency and accuracy.However,due to its special structure and complex oil pressure signal,related documents for evaluating dynamic characteristics of this mechanism are lack and some dynamic characteristics of this mechanism can't be extracted and recognized effectively by traditional methods.Aiming at the problem above-mentioned,a new method based on Hilbert-Huang transform(HHT) is presented.Firstly,combining with the actual working process,the dynamic liquid pressure signal of the mechanism is acquired.By analyzing the pressure fluctuation during the whole working process in time domain,oil leakage and hydraulic shock in the clamping chamber are discovered.Secondly,owing to the nonlinearity and nonstationarity of pressure signal,empirical mode decomposition is used,and the signal is decomposed and reconstructed into forced vibration,free vibration and noise.By analyzing forced vibration in the time domain,machining error and installation error of cam are revealed.Finally,free vibration component is analyzed in time-frequency domain with HHT,the traits of free vibration in the time-frequency domain are revealed.Compared with traditional methods,Hilbert spectrum has higher time-frequency resolutions and higher credibility.The improved mechanism based on the above analyses can guarantee the test accuracy of injector injection.This new method based on the analyses of the pressure signal and combined with HHT can provide scientific basis for evaluation,design improvement of the mechanism,and give references for dynamic characteristics analysis of the hydraulic system in the interrelated fields.展开更多
The preparation of dense Si_(3)N_(4)-based ceramics has attracted great attention because of the achievable improvements in their mechanical properties and high-temperature oxidation resistance.In this work,advanced d...The preparation of dense Si_(3)N_(4)-based ceramics has attracted great attention because of the achievable improvements in their mechanical properties and high-temperature oxidation resistance.In this work,advanced dense boron-containingα/β-Si_(3)N_(4)/Si monoliths were prepared via a high pressure‒high temperature technique in which polymer-derived amorphous SiBN powders were used as raw materials.The crystallization behavior and phase transformation of the polymer-derived amorphous samples were studied in the temperature range from 1400 to 1800℃.The results demonstrate that the incorporation of boron in the Si_(3)N_(4)matrix suppresses the phase transformation fromα-Si_(3)N_(4)toβ-Si_(3)N_(4).Furthermore,the mechanical properties of the as-prepared samples were measured,and the maximum hardness and fracture toughness of boron-rich SiBN samples reached 14.8 GPa and 7.96 MPa·m1/2,respectively.The hardness of the obtained boron-rich SiBN samples is stable up to 300℃.In addition,the oxidation behavior of the samples prepared at 1400 and 1600℃ was investigated at 1400℃ for 50 h.The results show that the incorporation of boron significantly improved the oxidation resistance of the samples because of the formation of borosilicate/cristobalite.This work provides guidance for the synthesis of boron-containingα/β-Si_(3)N_(4)-based ceramics with excellent mechanical properties and oxidation resistance.展开更多
Water injection for oil displacement is one of the most effective ways to develop fractured-vuggy carbonate reservoirs.With the increase in the number of rounds of water injection,the development effect gradually fail...Water injection for oil displacement is one of the most effective ways to develop fractured-vuggy carbonate reservoirs.With the increase in the number of rounds of water injection,the development effect gradually fails.The emergence of high-pressure capacity expansion and water injection technology allows increased production from old wells.Although high-pressure capacity expansion and water injection technology has been implemented in practice for nearly 10 years in fractured-vuggy reservoirs,its mechanism remains unclear,and the water injection curve is not apparent.In the past,evaluating its effect could only be done by measuring the injection-production volume.In this study,we analyze the mechanism of high-pressure capacity expansion and water injection.We propose a fluid exchange index for high-pressure capacity expansion and water injection and establish a discrete model suitable for high-pressure capacity expansion and water injection curves in fractured-vuggy reservoirs.We propose the following mechanisms:replenishing energy,increasing energy,replacing energy,and releasing energy.The above mechanisms can be identified by the high-pressure capacity expansion and water injection curve of the well HA6X in the Halahatang Oilfield in the Tarim Basin.By solving the basic model,the relative errors of Reservoirs I and II are found to be 1.9%and 1.5%,respectively,and the application of field examples demonstrates that our proposed high-pressure capacity expansion and water injection indicator curve is reasonable and reliable.This research can provide theoretical support for high-pressure capacity expansion and water injection technology in fracture-vuggy carbonate reservoirs.展开更多
A new high-pressure die-cast(HPDC) Mg–4 Al–3 La–1 Ca–0.3 Mn(ALaX431) alloy with high strength has successfully been fabricated. This HPDC alloy in peakaged state exhibits tensile yield strength(TYS) of 220 MPa at ...A new high-pressure die-cast(HPDC) Mg–4 Al–3 La–1 Ca–0.3 Mn(ALaX431) alloy with high strength has successfully been fabricated. This HPDC alloy in peakaged state exhibits tensile yield strength(TYS) of 220 MPa at room temperature and TYS of 145 MPa at 250 ℃,higher than the corresponding strength of HPDC Mg alloys reported so far. These high strengths are mainly due to the formation of fine grained structure, semi-continuous reticular structure consisting of stable Al_(3)La and(Mg,Al)2 Ca particles along grain boundaries and numerous nanoscale Al_(2)Ca precipitates within grains. Due to its higher strength than existing HPDC Mg alloys, the new developed alloy has great application potential.展开更多
In recent years,high-entropy alloys(HEAs) have developed a lot as the new style of materials,which have become a research focus in the materials fields.It breaks the normal procedure of traditional alloy design(based ...In recent years,high-entropy alloys(HEAs) have developed a lot as the new style of materials,which have become a research focus in the materials fields.It breaks the normal procedure of traditional alloy design(based on one/two elements as the main component,and adds some other elements to improve the micro structure and required related performance of the alloy),and consists of five or more equal or nearly equal elements,with multiple principal elements.Therefore,HEAs have many excellent mechanical properties compared with traditional alloys,which have aroused great research interest of researchers.The rapid development of high-pressure technology makes it a powerful tool to modulate the structures of HEAs,and brings new chance for the study and optimization of mechanical properties of HEAs.In this paper,the application of high-pressure technology in exploring and improving the mechanical properties of HEAs is reviewed,which could deepen the understanding of high-pressure technology and provide a new avenue for further exploration of HEAs’ mechanical properties.展开更多
A newly developed Mg-4Zn-2La-3Y alloy with high strength was fabricated by high-pressure die casting method,and its microstructures were thoroughly studied using transmission electron microscopy.The results demonstrat...A newly developed Mg-4Zn-2La-3Y alloy with high strength was fabricated by high-pressure die casting method,and its microstructures were thoroughly studied using transmission electron microscopy.The results demonstrate that it owns fine grains and approximately highly interconnected intermetallic phase skeletons,and exhibits ultra-high strength at both room and high temperatures.Interestingly,the eutectic intermetallic skeleton of this alloys is consisted of numerous fine particles,which are mainly consisted of two intermetallic phases,namely W and Mg12RE.Multiple{101}twins and SFs were found in the Mg12RE phase while a few of SFs in the W phase.Additionally,minor long-period stacking ordered phase was observed in the eutectoid phase,and it probably nucleated on the Mg12RE phase following a certain OR as(0002)14H//(110)Mg12REand[1120]14H//[111]Mg12RE,or(0002)14H//(211)Mg12REand[1120]14H//[111]Mg12RE.This special intermetallic skeleton with many interfaces and planar faults can efficiently transfer dislocations across grain boundaries,and this is the key factor for the outstanding mechanical properties of the studied alloy.展开更多
Deep oil and gas reservoirs are under high-temperature conditions,but traditional coring methods do not consider temperature-preserved measures and ignore the influence of temperature on rock porosity and permeability...Deep oil and gas reservoirs are under high-temperature conditions,but traditional coring methods do not consider temperature-preserved measures and ignore the influence of temperature on rock porosity and permeability,resulting in distorted resource assessments.The development of in situ temperaturepreserved coring(ITP-Coring)technology for deep reservoir rock is urgent,and thermal insulation materials are key.Therefore,hollow glass microsphere/epoxy resin thermal insulation materials(HGM/EP materials)were proposed as thermal insulation materials.The materials properties under coupled hightemperature and high-pressure(HTHP)conditions were tested.The results indicated that high pressures led to HGM destruction and that the materials water absorption significantly increased;additionally,increasing temperature accelerated the process.High temperatures directly caused the thermal conductivity of the materials to increase;additionally,the thermal conduction and convection of water caused by high pressures led to an exponential increase in the thermal conductivity.High temperatures weakened the matrix,and high pressures destroyed the HGM,which resulted in a decrease in the tensile mechanical properties of the materials.The materials entered the high elastic state at 150℃,and the mechanical properties were weakened more obviously,while the pressure led to a significant effect when the water absorption was above 10%.Meanwhile,the tensile strength/strain were 13.62 MPa/1.3%and 6.09 MPa/0.86%at 100℃ and 100 MPa,respectively,which meet the application requirements of the self-designed coring device.Finally,K46-f40 and K46-f50 HGM/EP materials were proven to be suitable for ITP-Coring under coupled conditions below 100℃ and 100 MPa.To further improve the materials properties,the interface layer and EP matrix should be optimized.The results can provide references for the optimization and engineering application of materials and thus technical support for deep oil and gas resource development.展开更多
Arsenic materials have attracted great attention due to their unique properties.However,research concerning iron-arsenic(Fe-As) alloys is very scarce due to the volatility of As at low temperature and the high melting...Arsenic materials have attracted great attention due to their unique properties.However,research concerning iron-arsenic(Fe-As) alloys is very scarce due to the volatility of As at low temperature and the high melting point of Fe.Herein,a new Fe-As alloy was obtained by mechanical alloying(MA) followed by vacuum hot-pressed sintering(VHPS).Moreover,a systematic study was carried out on the microstructural evolution,phase composition,leaching toxicity of As,and physical and mechanical properties of Fe-As alloys with varying weight fractions of As(20%,25%,30%,35%,45%,55%,65%,and 75%).The results showed that pre-alloyed metallic powders(PAMPs) have a fine grain size and specific supersaturated solid solution after MA,which could effectively improve the mechanical properties of Fe-As alloys by VHPS.A high density(> 7.350 g·cm^(-3)),low toxicity,and excellent mechanical properties could be obtained for FeAs alloys sintered via VHPS by adding an appropriate amount of As,which is more valuable than commercial Fe-As products.The Fe-25% As alloy with low toxicity and a relatively high density(7.635 g·cm^(-3)) provides an ultra-high compressive strength(1989.19 MPa),while the Fe-65% As alloy owns the maximum Vickers hardness(HVo.5 899.41).After leaching by the toxicity characteristic leaching procedure(TCLP),these alloys could still maintain good mechanical performance,and the strengthening mechanisms of Fe-As alloys before and after leaching were clarified.Changes in the grain size,micro structure,and phase distribution induced significant differences in the compressive strength and hardness.展开更多
文摘PT fuel injector is one of the most important parts of modern diesel engine.To satisfy the requirements of the rapid and accurate test of PT fuel injector,the self-adaptive floating clamping mechanism was developed and used in the relevant bench.Its dynamic characteristics directly influence the test efficiency and accuracy.However,due to its special structure and complex oil pressure signal,related documents for evaluating dynamic characteristics of this mechanism are lack and some dynamic characteristics of this mechanism can't be extracted and recognized effectively by traditional methods.Aiming at the problem above-mentioned,a new method based on Hilbert-Huang transform(HHT) is presented.Firstly,combining with the actual working process,the dynamic liquid pressure signal of the mechanism is acquired.By analyzing the pressure fluctuation during the whole working process in time domain,oil leakage and hydraulic shock in the clamping chamber are discovered.Secondly,owing to the nonlinearity and nonstationarity of pressure signal,empirical mode decomposition is used,and the signal is decomposed and reconstructed into forced vibration,free vibration and noise.By analyzing forced vibration in the time domain,machining error and installation error of cam are revealed.Finally,free vibration component is analyzed in time-frequency domain with HHT,the traits of free vibration in the time-frequency domain are revealed.Compared with traditional methods,Hilbert spectrum has higher time-frequency resolutions and higher credibility.The improved mechanism based on the above analyses can guarantee the test accuracy of injector injection.This new method based on the analyses of the pressure signal and combined with HHT can provide scientific basis for evaluation,design improvement of the mechanism,and give references for dynamic characteristics analysis of the hydraulic system in the interrelated fields.
基金support from the National Natural Science Foundation of China(No.12204254)the Natural Science Foundation of Zhejiang Province(No.LQ23A040005)+1 种基金the Program for Science and Technology Innovation Team in Zhejiang(No.2021R01004)support from the Technical University of Darmstadt,Germany.Zhaoju Yu thanks the Natural Science Foundation of China(Nos.51872246 and 52061135102)for financial support.
文摘The preparation of dense Si_(3)N_(4)-based ceramics has attracted great attention because of the achievable improvements in their mechanical properties and high-temperature oxidation resistance.In this work,advanced dense boron-containingα/β-Si_(3)N_(4)/Si monoliths were prepared via a high pressure‒high temperature technique in which polymer-derived amorphous SiBN powders were used as raw materials.The crystallization behavior and phase transformation of the polymer-derived amorphous samples were studied in the temperature range from 1400 to 1800℃.The results demonstrate that the incorporation of boron in the Si_(3)N_(4)matrix suppresses the phase transformation fromα-Si_(3)N_(4)toβ-Si_(3)N_(4).Furthermore,the mechanical properties of the as-prepared samples were measured,and the maximum hardness and fracture toughness of boron-rich SiBN samples reached 14.8 GPa and 7.96 MPa·m1/2,respectively.The hardness of the obtained boron-rich SiBN samples is stable up to 300℃.In addition,the oxidation behavior of the samples prepared at 1400 and 1600℃ was investigated at 1400℃ for 50 h.The results show that the incorporation of boron significantly improved the oxidation resistance of the samples because of the formation of borosilicate/cristobalite.This work provides guidance for the synthesis of boron-containingα/β-Si_(3)N_(4)-based ceramics with excellent mechanical properties and oxidation resistance.
基金supported by the China Postdoctoral Science Foundation(No.M2019650965)Major R&D Plan of Sichuan Province(No.2020YFQ0034)the National Natural Science Fund Projects(Grant No.51804253).
文摘Water injection for oil displacement is one of the most effective ways to develop fractured-vuggy carbonate reservoirs.With the increase in the number of rounds of water injection,the development effect gradually fails.The emergence of high-pressure capacity expansion and water injection technology allows increased production from old wells.Although high-pressure capacity expansion and water injection technology has been implemented in practice for nearly 10 years in fractured-vuggy reservoirs,its mechanism remains unclear,and the water injection curve is not apparent.In the past,evaluating its effect could only be done by measuring the injection-production volume.In this study,we analyze the mechanism of high-pressure capacity expansion and water injection.We propose a fluid exchange index for high-pressure capacity expansion and water injection and establish a discrete model suitable for high-pressure capacity expansion and water injection curves in fractured-vuggy reservoirs.We propose the following mechanisms:replenishing energy,increasing energy,replacing energy,and releasing energy.The above mechanisms can be identified by the high-pressure capacity expansion and water injection curve of the well HA6X in the Halahatang Oilfield in the Tarim Basin.By solving the basic model,the relative errors of Reservoirs I and II are found to be 1.9%and 1.5%,respectively,and the application of field examples demonstrates that our proposed high-pressure capacity expansion and water injection indicator curve is reasonable and reliable.This research can provide theoretical support for high-pressure capacity expansion and water injection technology in fracture-vuggy carbonate reservoirs.
基金financially supported by the National Natural Science Foundation of China (Nos.51701200 and 11804030)the Fundamental Research Funds for the Central Universities (No.3072020CF1009)+2 种基金the Open Funds of the State Key Laboratory of Rare Earth Resource Utilization (Nos.RERU2020008 and 2020012)the Scientific and Technological Developing Scheme of Jilin Province (No.20200801048GH)the Jilin Scientific and Technological Development Programs (No.20200201240JC)。
文摘A new high-pressure die-cast(HPDC) Mg–4 Al–3 La–1 Ca–0.3 Mn(ALaX431) alloy with high strength has successfully been fabricated. This HPDC alloy in peakaged state exhibits tensile yield strength(TYS) of 220 MPa at room temperature and TYS of 145 MPa at 250 ℃,higher than the corresponding strength of HPDC Mg alloys reported so far. These high strengths are mainly due to the formation of fine grained structure, semi-continuous reticular structure consisting of stable Al_(3)La and(Mg,Al)2 Ca particles along grain boundaries and numerous nanoscale Al_(2)Ca precipitates within grains. Due to its higher strength than existing HPDC Mg alloys, the new developed alloy has great application potential.
基金supported by the National Natural Science Foundation of China (Grant Nos. 62104090, 11604133, and 11874174)the Natural Science Foundation of Shandong Province(Grant Nos. ZR2017QA013, ZR2021QA087, and ZR2021QA092 )+3 种基金the Science and Technology Plan of Youth Innovation Team for Universities of Shandong Province (Grant No. 2019KJJ019)the Introduction and Cultivation Plan of Youth Innovation Talents for Universities of Shandong Province, Fundamental Research Funds for the Central Universities (buctrc 202122)the Research Funding of Liaocheng University (318012016, 318051610, and 318051612)the Special Construction Project Fund for Shandong Province Taishan Scholars。
文摘In recent years,high-entropy alloys(HEAs) have developed a lot as the new style of materials,which have become a research focus in the materials fields.It breaks the normal procedure of traditional alloy design(based on one/two elements as the main component,and adds some other elements to improve the micro structure and required related performance of the alloy),and consists of five or more equal or nearly equal elements,with multiple principal elements.Therefore,HEAs have many excellent mechanical properties compared with traditional alloys,which have aroused great research interest of researchers.The rapid development of high-pressure technology makes it a powerful tool to modulate the structures of HEAs,and brings new chance for the study and optimization of mechanical properties of HEAs.In this paper,the application of high-pressure technology in exploring and improving the mechanical properties of HEAs is reviewed,which could deepen the understanding of high-pressure technology and provide a new avenue for further exploration of HEAs’ mechanical properties.
基金supported by the National Natural Science Foundation of China under grants no.51701200 and 51871069the Scientific and Technological Developing Scheme of Jilin Province under grants no.20200801048GH。
文摘A newly developed Mg-4Zn-2La-3Y alloy with high strength was fabricated by high-pressure die casting method,and its microstructures were thoroughly studied using transmission electron microscopy.The results demonstrate that it owns fine grains and approximately highly interconnected intermetallic phase skeletons,and exhibits ultra-high strength at both room and high temperatures.Interestingly,the eutectic intermetallic skeleton of this alloys is consisted of numerous fine particles,which are mainly consisted of two intermetallic phases,namely W and Mg12RE.Multiple{101}twins and SFs were found in the Mg12RE phase while a few of SFs in the W phase.Additionally,minor long-period stacking ordered phase was observed in the eutectoid phase,and it probably nucleated on the Mg12RE phase following a certain OR as(0002)14H//(110)Mg12REand[1120]14H//[111]Mg12RE,or(0002)14H//(211)Mg12REand[1120]14H//[111]Mg12RE.This special intermetallic skeleton with many interfaces and planar faults can efficiently transfer dislocations across grain boundaries,and this is the key factor for the outstanding mechanical properties of the studied alloy.
基金supported by the Sichuan Science and Technology Program (Grant Nos.2023NSFSC0004,2023NSFSC0790)the National Natural Science Foundation of China (Grant Nos.51827901,52304033)the Sichuan University Postdoctoral Fund (Grant No.2024SCU12093)。
文摘Deep oil and gas reservoirs are under high-temperature conditions,but traditional coring methods do not consider temperature-preserved measures and ignore the influence of temperature on rock porosity and permeability,resulting in distorted resource assessments.The development of in situ temperaturepreserved coring(ITP-Coring)technology for deep reservoir rock is urgent,and thermal insulation materials are key.Therefore,hollow glass microsphere/epoxy resin thermal insulation materials(HGM/EP materials)were proposed as thermal insulation materials.The materials properties under coupled hightemperature and high-pressure(HTHP)conditions were tested.The results indicated that high pressures led to HGM destruction and that the materials water absorption significantly increased;additionally,increasing temperature accelerated the process.High temperatures directly caused the thermal conductivity of the materials to increase;additionally,the thermal conduction and convection of water caused by high pressures led to an exponential increase in the thermal conductivity.High temperatures weakened the matrix,and high pressures destroyed the HGM,which resulted in a decrease in the tensile mechanical properties of the materials.The materials entered the high elastic state at 150℃,and the mechanical properties were weakened more obviously,while the pressure led to a significant effect when the water absorption was above 10%.Meanwhile,the tensile strength/strain were 13.62 MPa/1.3%and 6.09 MPa/0.86%at 100℃ and 100 MPa,respectively,which meet the application requirements of the self-designed coring device.Finally,K46-f40 and K46-f50 HGM/EP materials were proven to be suitable for ITP-Coring under coupled conditions below 100℃ and 100 MPa.To further improve the materials properties,the interface layer and EP matrix should be optimized.The results can provide references for the optimization and engineering application of materials and thus technical support for deep oil and gas resource development.
基金financially supported by the National Natural Science Foundation of China (No.52104406)the Natural Science Foundation of Hunan Province (No.2022JJ20074)+1 种基金the Foundation for Innovative Research Groups of the National Natural Science Foundation of China (No.52121004)the National Natural Science Foundation of China for Distinguished Young Scholars (No.51825403)。
文摘Arsenic materials have attracted great attention due to their unique properties.However,research concerning iron-arsenic(Fe-As) alloys is very scarce due to the volatility of As at low temperature and the high melting point of Fe.Herein,a new Fe-As alloy was obtained by mechanical alloying(MA) followed by vacuum hot-pressed sintering(VHPS).Moreover,a systematic study was carried out on the microstructural evolution,phase composition,leaching toxicity of As,and physical and mechanical properties of Fe-As alloys with varying weight fractions of As(20%,25%,30%,35%,45%,55%,65%,and 75%).The results showed that pre-alloyed metallic powders(PAMPs) have a fine grain size and specific supersaturated solid solution after MA,which could effectively improve the mechanical properties of Fe-As alloys by VHPS.A high density(> 7.350 g·cm^(-3)),low toxicity,and excellent mechanical properties could be obtained for FeAs alloys sintered via VHPS by adding an appropriate amount of As,which is more valuable than commercial Fe-As products.The Fe-25% As alloy with low toxicity and a relatively high density(7.635 g·cm^(-3)) provides an ultra-high compressive strength(1989.19 MPa),while the Fe-65% As alloy owns the maximum Vickers hardness(HVo.5 899.41).After leaching by the toxicity characteristic leaching procedure(TCLP),these alloys could still maintain good mechanical performance,and the strengthening mechanisms of Fe-As alloys before and after leaching were clarified.Changes in the grain size,micro structure,and phase distribution induced significant differences in the compressive strength and hardness.