[Objectives]To establish a thin-layer chromatography(TLC)method for the determination of rubiadin-1-methyl ether in Yao Medicine Chuanlianzhu(Damnacanthus giganteus).[Methods]A silica gel G thin-layer plate was adopte...[Objectives]To establish a thin-layer chromatography(TLC)method for the determination of rubiadin-1-methyl ether in Yao Medicine Chuanlianzhu(Damnacanthus giganteus).[Methods]A silica gel G thin-layer plate was adopted for TLC.Petroleum ether(60-90℃)-chloroform-methanol-water(7:15:3:1)was used as the developing solvent and inspected under ultraviolet lamp(365 nm).The content was determined by Inertsil ODS-3 C 18 column(4.60 mm×250 mm,5μm),mobile phase:acetonitrile-0.2%phosphoric acid gradient elution,detection wavelength 277 nm,flow rate 1.0 mL/min,column temperature 30℃,injection volume 10μL.[Results]The spots of 10 Chuanlianzhu samples from different origins showed the same color at the same position as the control,and the spots were clear and specific.The injection volume of rubiadin-1-methyl ether showed a good linear relationship in the range of 2.90-145μg(R=0.9996).The average recovery rate of rubiadin-1-methyl ether in the low,medium and high dose groups of Yao Medicine Chuanlianzhu was 98.72%,and RSD=1.78%.[Conclusions]This method can effectively identify Yao Medicine Chuanlianzhu medicinal materials and accurately determine the content of rubiadin-1-methyl ether in the medicinal materials.It provides a scientific basis for the development and utilization of Yao Medicine Chuanlianzhu medicinal resources.展开更多
为利用干酪乳杆菌制备发酵菠萝果汁饮品,本研究对干酪乳杆菌LK-1(Lactobacillus casei LK-1,L. casei LK-1)的生长曲线、产酸、耐酸和耐糖等特性进行研究分析,并以活菌数和总酸为指标,通过单因素实验及响应面法考察L. casei LK-1发酵菠...为利用干酪乳杆菌制备发酵菠萝果汁饮品,本研究对干酪乳杆菌LK-1(Lactobacillus casei LK-1,L. casei LK-1)的生长曲线、产酸、耐酸和耐糖等特性进行研究分析,并以活菌数和总酸为指标,通过单因素实验及响应面法考察L. casei LK-1发酵菠萝果汁的最佳条件。结果表明,L. casei LK-1在pH5~7和0%~10%质量分数葡萄糖环境下,具备良好的生长繁殖能力;在酸性(pH3)和高糖(40%质量分数葡萄糖)环境中培养3 h,其存活率分别为76%和71%;在MRS培养基中培养48 h,产酸量为5.35 g/kg,产酸能力良好,适用于果汁的发酵。L. casei LK-1发酵菠萝果汁的最佳条件为:初始pH6.8,发酵温度37℃,接种量1%(v/v),发酵时间30 h,此条件下制备的发酵菠萝果汁饮品活菌数为8.99±0.04 lg CFU/mL,总酸含量为7.16±0.26 g/kg,且色泽鲜亮,酸甜适口,风味较好,为L. casei LK-1在发酵食品中的进一步应用提供了理论和技术依据。展开更多
Aluminum alloy thin-walled structures are widely used in the automotive industry due to their advantages related to light weight and crashworthiness.They can be produced at room temperature by the electrohydraulic for...Aluminum alloy thin-walled structures are widely used in the automotive industry due to their advantages related to light weight and crashworthiness.They can be produced at room temperature by the electrohydraulic forming process.In the present study,the influence of the related parameters on the forming quality of a 6063 aluminum alloy sinusoidal corrugation tube has been assessed.In particular,the orthogonal experimental design(OED)and central composite design(CCD)methods have been used.Through the range analysis and variance analysis of the experimental data,the influence degree of wire diameter(WD)and discharge energy(DE)on the forming quality was determined.Multiple regression analysis was performed using the response surface methodology.A prediction model for the attaching-die state coefficient was established accordingly.The following optimal arrangement of parameters was obtained(WD=0.759 mm,DE=2.926 kJ).The attaching-die state coefficient reached the peak value of 0.001.Better optimized wire diameter and discharge energy for a better attaching-die state could be screened by CCD compared with OED.The response surface method in CCD was more suitable for the design and optimization of the considered process parameters.展开更多
The Joint Conference Organizing Committee of The Chinese Society of Metals(CSM),The Japan Insti-tute of Metals(JIM),The Korean Institute of Metals(KIM)and The Minerals,Metals & Materials Society(TMS)announces The ...The Joint Conference Organizing Committee of The Chinese Society of Metals(CSM),The Japan Insti-tute of Metals(JIM),The Korean Institute of Metals(KIM)and The Minerals,Metals & Materials Society(TMS)announces The First Pacific Rim International Conference on Advanced Materials and Processing(PRICM-1)which will be held in Hangzhou,China,in the last week of June,1992 lasting about four days.It is agreed that the PRICM-1 will be organized by The Chinese Society of Metals.展开更多
明确不同水氮互作对强筋优质小麦师栾02-1产量和加工品质的影响,为强筋小麦生产中如何通过合理灌溉和优化氮肥施用量来实现协同提高籽粒产量和加工品质的目标提供理论依据。2017-2020年,大田条件下设置浇水次数和施氮量二因子裂区试验,...明确不同水氮互作对强筋优质小麦师栾02-1产量和加工品质的影响,为强筋小麦生产中如何通过合理灌溉和优化氮肥施用量来实现协同提高籽粒产量和加工品质的目标提供理论依据。2017-2020年,大田条件下设置浇水次数和施氮量二因子裂区试验,主区为浇水次数,设春浇一水(W1,拔节水)和春浇两水(W2,拔节水+开花水);副区为氮肥施用量,设N0、N1、N2、N3、N4和N5(0、60、120、180、240和300 kg hm^(-2))6个水平。结果表明,施氮量0~300 kg hm^(-2)时,不同降水年型春浇一水、春浇两水小麦产量随施氮量的增加均先增加后减少,产量最高值对应的施氮量均为240 kg hm^(-2)。施氮量120~300 kg hm^(-2)时,春浇两水处理产量显著高于春浇一水处理。水氮互作对小麦单位面积收获穗数的影响最大,其次是千粒重,对穗粒数的影响最小。施氮量0~300 kg hm^(-2)时,2017-2018年度(丰水年型),春浇两水小麦湿面筋含量、沉降值、吸水率、面团稳定时间、拉伸能量、最大拉伸阻力平均值均高于春浇一水,而2018-2019、2019-2020年度(干旱年型)则相反:春浇一水高于春浇两水。不同降水年型春浇一水、春浇两水小麦湿面筋含量和沉降值随施氮量的增加先增加后减少或逐渐增加,二者最大值对应的施氮量为240 kg hm^(-2)或300 kg hm^(-2);稳定时间、拉伸能量和最大拉伸阻力随施氮量的增加均先增加后减少,施氮量240 kg hm^(-2)时达到最大值。不同降水年型强筋优质小麦师栾02-1生育期春浇两水、施氮量240 kg hm^(-2)时,籽粒产量和加工品质表现最佳。展开更多
基金Supported by State Administration of Traditional Chinese Medicine High-level Key Discipline Construction Project of Traditional Chinese Medicine-Ethnic Minority Pharmacy (Zhuang Pharmacy) (zyyzdxk-2023165)General Scientific Research Program of Guangxi University of Chinese Medicine in 2020 (2020MS063)+4 种基金Key R&D Project of Guangxi Science and Technology Department (Guike AB21196057)Young Talent Cultivation Program of Guangxi International Zhuang Medicine Hospital (2022001)Funding Project of High-level Talent Cultivation and Innovation Team of Guangxi University of Chinese Medicine (2022A008)Guangxi Traditional Chinese Medicine Interdisciplinary Innovation Team Project (GZKJ2309)State Administration of Traditional Chinese Medicine"Twelfth Five-Year Plan"Key Discipline of Traditional Chinese Medicine (Ethnic Pharmacy)Zhuang Pharmacy.
文摘[Objectives]To establish a thin-layer chromatography(TLC)method for the determination of rubiadin-1-methyl ether in Yao Medicine Chuanlianzhu(Damnacanthus giganteus).[Methods]A silica gel G thin-layer plate was adopted for TLC.Petroleum ether(60-90℃)-chloroform-methanol-water(7:15:3:1)was used as the developing solvent and inspected under ultraviolet lamp(365 nm).The content was determined by Inertsil ODS-3 C 18 column(4.60 mm×250 mm,5μm),mobile phase:acetonitrile-0.2%phosphoric acid gradient elution,detection wavelength 277 nm,flow rate 1.0 mL/min,column temperature 30℃,injection volume 10μL.[Results]The spots of 10 Chuanlianzhu samples from different origins showed the same color at the same position as the control,and the spots were clear and specific.The injection volume of rubiadin-1-methyl ether showed a good linear relationship in the range of 2.90-145μg(R=0.9996).The average recovery rate of rubiadin-1-methyl ether in the low,medium and high dose groups of Yao Medicine Chuanlianzhu was 98.72%,and RSD=1.78%.[Conclusions]This method can effectively identify Yao Medicine Chuanlianzhu medicinal materials and accurately determine the content of rubiadin-1-methyl ether in the medicinal materials.It provides a scientific basis for the development and utilization of Yao Medicine Chuanlianzhu medicinal resources.
文摘为利用干酪乳杆菌制备发酵菠萝果汁饮品,本研究对干酪乳杆菌LK-1(Lactobacillus casei LK-1,L. casei LK-1)的生长曲线、产酸、耐酸和耐糖等特性进行研究分析,并以活菌数和总酸为指标,通过单因素实验及响应面法考察L. casei LK-1发酵菠萝果汁的最佳条件。结果表明,L. casei LK-1在pH5~7和0%~10%质量分数葡萄糖环境下,具备良好的生长繁殖能力;在酸性(pH3)和高糖(40%质量分数葡萄糖)环境中培养3 h,其存活率分别为76%和71%;在MRS培养基中培养48 h,产酸量为5.35 g/kg,产酸能力良好,适用于果汁的发酵。L. casei LK-1发酵菠萝果汁的最佳条件为:初始pH6.8,发酵温度37℃,接种量1%(v/v),发酵时间30 h,此条件下制备的发酵菠萝果汁饮品活菌数为8.99±0.04 lg CFU/mL,总酸含量为7.16±0.26 g/kg,且色泽鲜亮,酸甜适口,风味较好,为L. casei LK-1在发酵食品中的进一步应用提供了理论和技术依据。
基金supported by National Natural Science Foundation of China(Grant Nos.51975202(Junjia Cui received the grant)and 52175315(Guangyao Li received the grant)).
文摘Aluminum alloy thin-walled structures are widely used in the automotive industry due to their advantages related to light weight and crashworthiness.They can be produced at room temperature by the electrohydraulic forming process.In the present study,the influence of the related parameters on the forming quality of a 6063 aluminum alloy sinusoidal corrugation tube has been assessed.In particular,the orthogonal experimental design(OED)and central composite design(CCD)methods have been used.Through the range analysis and variance analysis of the experimental data,the influence degree of wire diameter(WD)and discharge energy(DE)on the forming quality was determined.Multiple regression analysis was performed using the response surface methodology.A prediction model for the attaching-die state coefficient was established accordingly.The following optimal arrangement of parameters was obtained(WD=0.759 mm,DE=2.926 kJ).The attaching-die state coefficient reached the peak value of 0.001.Better optimized wire diameter and discharge energy for a better attaching-die state could be screened by CCD compared with OED.The response surface method in CCD was more suitable for the design and optimization of the considered process parameters.
文摘The Joint Conference Organizing Committee of The Chinese Society of Metals(CSM),The Japan Insti-tute of Metals(JIM),The Korean Institute of Metals(KIM)and The Minerals,Metals & Materials Society(TMS)announces The First Pacific Rim International Conference on Advanced Materials and Processing(PRICM-1)which will be held in Hangzhou,China,in the last week of June,1992 lasting about four days.It is agreed that the PRICM-1 will be organized by The Chinese Society of Metals.
文摘明确不同水氮互作对强筋优质小麦师栾02-1产量和加工品质的影响,为强筋小麦生产中如何通过合理灌溉和优化氮肥施用量来实现协同提高籽粒产量和加工品质的目标提供理论依据。2017-2020年,大田条件下设置浇水次数和施氮量二因子裂区试验,主区为浇水次数,设春浇一水(W1,拔节水)和春浇两水(W2,拔节水+开花水);副区为氮肥施用量,设N0、N1、N2、N3、N4和N5(0、60、120、180、240和300 kg hm^(-2))6个水平。结果表明,施氮量0~300 kg hm^(-2)时,不同降水年型春浇一水、春浇两水小麦产量随施氮量的增加均先增加后减少,产量最高值对应的施氮量均为240 kg hm^(-2)。施氮量120~300 kg hm^(-2)时,春浇两水处理产量显著高于春浇一水处理。水氮互作对小麦单位面积收获穗数的影响最大,其次是千粒重,对穗粒数的影响最小。施氮量0~300 kg hm^(-2)时,2017-2018年度(丰水年型),春浇两水小麦湿面筋含量、沉降值、吸水率、面团稳定时间、拉伸能量、最大拉伸阻力平均值均高于春浇一水,而2018-2019、2019-2020年度(干旱年型)则相反:春浇一水高于春浇两水。不同降水年型春浇一水、春浇两水小麦湿面筋含量和沉降值随施氮量的增加先增加后减少或逐渐增加,二者最大值对应的施氮量为240 kg hm^(-2)或300 kg hm^(-2);稳定时间、拉伸能量和最大拉伸阻力随施氮量的增加均先增加后减少,施氮量240 kg hm^(-2)时达到最大值。不同降水年型强筋优质小麦师栾02-1生育期春浇两水、施氮量240 kg hm^(-2)时,籽粒产量和加工品质表现最佳。
