Cases are presented to reveal how modern computerised infra-red thermal imaging has the potential to assist in early breast cancer detection. The history of thermography and some recent controversies surrounding mammo...Cases are presented to reveal how modern computerised infra-red thermal imaging has the potential to assist in early breast cancer detection. The history of thermography and some recent controversies surrounding mammography are discussed. Examples of thermal imaging combined with naturopathic interventions are described. Since 2002, more than 8000 women in New Zealand have chosen to include thermal imaging as a part of their breast health management. Breast thermal imaging combined with relevant health advice, resulted in a perceived worthwhile benefit to patients in managing overall health.展开更多
Alzheimers disease(AD)is a chronic neurodegenerative disease.The symptoms include memoryand spatial learning dificulties,language disorders,and loss of motivation,which get worse overtime,eventually ending in death.No...Alzheimers disease(AD)is a chronic neurodegenerative disease.The symptoms include memoryand spatial learning dificulties,language disorders,and loss of motivation,which get worse overtime,eventually ending in death.No ffective treatments are available for AD,currently.Currenttreatments only attenuate symptoms temporarily and are associated with severe side ffects.Nearinfra-red(NIR)light has been studied for a long time.We investigated the effect of NIR on ADusing a transgenic mouse model,which was obtained by co-injecting two vectors carrying ADmutations in amyloid precursor protein(APP)and presenilin-i(PSEN1)into C57BL/6J mice.The irradiation equipment consisted of an accommodating box and an LED array.The wave-length of NIR light emitted from LED was between 1040 nm and 1090 nm.The power densitydelivered at the level of the mice was approximately 15 mW/cm^(2),Firstly,we treated the micewith NIR for 40 days,Then,the irradiation was suspended for 28 days.Finally,another 15 daystreatment was brought to mice.We conducted Morris water maze and immunofluorescenceanalysis to evaluate the effects of treatment.Immunofuorescence analysis was based on mea-suring the quantity of plaques in mouse brain slices,Our results show that NIR light improvesmemory and spatial learning ability and reduces plaques moderately.NIR light represents apotential treatment for AD.展开更多
Introduction: Infra-red (IR) thermometry is a safe and valid method to determine internal and surface temperature in human subjects. Under conditions of brain damage (head injury or stroke) knowledge of changes in the...Introduction: Infra-red (IR) thermometry is a safe and valid method to determine internal and surface temperature in human subjects. Under conditions of brain damage (head injury or stroke) knowledge of changes in the temperature of intracranial tissue is justified because of the vulnerability of neurons to accelerated damage at temperatures at the upper end of the febrile range. Aim: To determine the temperature at the inner canthus (IC) of the eye as a potential surrogate for brain temperature. Methods: Invasive monitoring of deep brain structures, lateral ventricle and deep white matter. IR temperature readings obtained at right and left IC. Results: ?Strong correlations were evident between R and L IC and brain. Close, as well as poor, agreement between?? sites was shown in some patients and at some times. For right hemispheric lesions four had a better correlation between TbrV and TRIC when compared to TLIC.? When the correlation between TbrV and TLIC was better compared to TbrV and TRIC, four had a predominant right hemispheric lesion. Conclusions: Improved techniques for IR thermal imaging accuracy at the bedside has the potential to improve temperature measurement agreement. The predominant lesion side may have a bearing on maximum ipsilateral IC temperature Further studies are ongoing in this pilot study population.展开更多
In the present paper, an ‘in-house' genetic algorithm was numerically and experimentally validated. The genetic algorithm was applied to an optimization problem for improving the aerodynamic performances of an aircr...In the present paper, an ‘in-house' genetic algorithm was numerically and experimentally validated. The genetic algorithm was applied to an optimization problem for improving the aerodynamic performances of an aircraft wing tip through upper surface morphing. The optimization was performed for 16 flight cases expressed in terms of various combinations of speeds, angles of attack and aileron deflections. The displacements resulted from the optimization were used during the wind tunnel tests of the wing tip demonstrator for the actuators control to change the upper surface shape of the wing. The results of the optimization of the flow behavior for the airfoil morphing upper-surface problem were validated with wind tunnel experimental transition results obtained with infra-red Thermography on the wing-tip demonstrator. The validation proved that the 2D numerical optimization using the ‘in-house' genetic algorithm was an appropriate tool in improving various aspects of a wing's aerodynamic performances.展开更多
Background: Accurate temperature measurement is a critical step in evaluating health or disease especially in children and immmunocompromised subjects;inaccurate measurement may lead to improper diagnosis, wrong treat...Background: Accurate temperature measurement is a critical step in evaluating health or disease especially in children and immmunocompromised subjects;inaccurate measurement may lead to improper diagnosis, wrong treatment or inappropriate intervention. Several methods of temperature measurements exist and comparing these gives room for choosing a near ideal method in terms of speed, safety and accuracy. The study aimed to compare the forehead non touch infra-red thermometer with the axilllary mercury-in-glass method of temperature measurement in the Paediatric age-group. Methods: Study was given ethical approval as part of a larger study. Four hundred and thirty seven children aged 1 to 24 months were studied at the well-baby/immunizationclinic of the University of Ilorin Teaching Hospital over a 6-months period. Both non-touch infrared and theregular mercury-in-glass thermometers were used to take the body temperatures. Data were analysed with SPSS version 21. Pearson correlation was used to determine the relationship between the two methods of temperature measurements, while Bland-Altman method was used to test for level of agreement between them. Results: The mean age and SD was 5.81 ± 4.04 months. Pearson correlation showed a positive correlation between the axillary mercury-in-glass and forehead non-touch infra-red thermometry readings (r = 0.281, p < 0.001). Also, Bland-Altman method revealed a good agreement between both methods of thermometry as 96% of the readings were within the limits of agreement. Mean difference was 0.09°C (95% confidence interval 0.05 - 0.13). Conclusion: Axillary mercury-in-glass thermometer and forehead non touch infra-red thermometers have a good agreement and can be used interchangeably.展开更多
Background: Neonatal temperature response during illness is unpredictable. Whereas accurate temperature measurement is an important diagnostic step in Neonatal practice. Abnormalties in temperature pattern may be a po...Background: Neonatal temperature response during illness is unpredictable. Whereas accurate temperature measurement is an important diagnostic step in Neonatal practice. Abnormalties in temperature pattern may be a pointer to a sinister condition especially in neonates, whose thermoregulatory mechanism is immature. There are several methods of temperature measurements and the search for a suitable thermometry method in neonates continues. This study compared the forehead non touch infra-red thermometer (NTIT) with the axilllary mercury-in-glass (MIGT) method of temperature measurement in neonates. Method: Four hundred babies aged 1 to 28 days were recruited from the immunization clinic of the University of Ilorin Teaching Hospital between August 2016 and May 2017. Temperatures were taken using both NTIT and MIGT in the standard way and recorded.?Result: The mean age and SD was 5.10 ± 4.28?days. Pearson correlation showed a positive correlation between the Axillary Mercury-in-Glass and Forehead Non-Touch Infra-red thermometry readings (r?=?0.426, p??0.001). Bland-Altman method revealed a good agreement between both methods of thermometry as 95.5% of the readings were within the limits of agreement. Conclusion: Axillary Mercury-in-Glass thermometer and Forehead Non touch Infra-red thermometers have a good agreement and can be used interchangeably in neonates.展开更多
A hypothesis is advanced in which life began from a Darwinian selection among a diversification of molecular species containing the phosphate moiety which broke the constraints implicit in the Second Law of Thermodyna...A hypothesis is advanced in which life began from a Darwinian selection among a diversification of molecular species containing the phosphate moiety which broke the constraints implicit in the Second Law of Thermodynamics, discussed famously by Schrodinger, by obtaining energy from specific infrared frequencies located in the phosphorus-oxygen vibration at a frequency around 1000 cm-1. We propose the source of this energy was from the internal conversion of solar broadband energy by the phosphate mineral Apatite, present at the bottom of a primitive biogenesis pond. In this scenario, life is re-defined as being hotter than its environment and as using its excess energy, supplied by infra-red conversion, to react with its molecular environment and pump itself up the “entropy slope” thereby;replication is through breakages of increasingly large phosphate containing biopolymers. The idea has implications for modern explanations of living systems.展开更多
This study evaluated the possibility of infrared thermography to measure accurately the temperature of elements of a rotating device, within the scope of condition monitoring. The tested machine was a blower coupled t...This study evaluated the possibility of infrared thermography to measure accurately the temperature of elements of a rotating device, within the scope of condition monitoring. The tested machine was a blower coupled to a 500 kW electric motor, that operated in multiples regimes. The thermograms were acquired by a fixed thermographic camera and were processed and recorded every 15 minutes. Because the normal temperature variations could easily mask a drift caused by a failure, a corrected temperature was computed using autorecursive models. It was shown that an efficient temperature correction should compensate for the variations of the process, and for the ambient temperatures variations, either daily or seasonal. The standard deviation of the corrected temperature was of a few tenth of degree, making possible the detection of a drift of less than one degree and the prediction of potential failure.展开更多
Gas chromatography is an analytical tool for the separation of compounds in complex mixtures based on the polarity of compounds. Separation is achieved only for compounds that are volatile or that can be made volatile...Gas chromatography is an analytical tool for the separation of compounds in complex mixtures based on the polarity of compounds. Separation is achieved only for compounds that are volatile or that can be made volatile on derivatization of the compound using derivatizing agents. This is one of the widely accepted tools for the separation of compounds because of its simplicity, sensitivity, and effectiveness. The principle of separation of compounds depends on the partitioning behaviour difference between mobile and stationary phase, the sample is carried by a moving gas stream through a tube packed with a finely divided solid or may be coated with a film of a liquid. Different types of columns having a various composition of stationary phase are been used for the separation of different classes of compounds mixture or sample in a suitable solvent is introduced through the injector maintained at higher temperature which is capable of volatilizing the compound into the column.展开更多
In order to study adsorption of preservatives by eyeliner pen package,the chemical compositions of the commercially available Eyeliner package were analyzed by infrared spectrometer.It was found that these package com...In order to study adsorption of preservatives by eyeliner pen package,the chemical compositions of the commercially available Eyeliner package were analyzed by infrared spectrometer.It was found that these package components were PP,PET,modified PP,modified PET,ABS,nylon,PU and so on.The adsorption effects of these components on three preservatives,i.e.phenoxyethanol,Methyl paraben and Propyl paraben have been further studied by high performance liquid chromatography.The results demonstrated that the four chemical materials PET,PP,modified PP and ABS had no adsorption on the above three preservatives.However,the component named of water diversion core which was composed of modified PET,and nylon-made cotton head have been observed of slight adsorption in this study.And components as the function of preventing liquid leakage,which was made of PU,have presented the most serious adsorption on these three preservatives,with the adsorption order as Propyl Paraben>Methyl Paraben>phenoxyethanol.展开更多
Currently,there is variability in the spectral band thresholds for snow cover recognition using remote sensing in different regions and for complex terrains.Using Fengyun-3B Visible and Infra-Red Radiometer(FY-3B VIRR...Currently,there is variability in the spectral band thresholds for snow cover recognition using remote sensing in different regions and for complex terrains.Using Fengyun-3B Visible and Infra-Red Radiometer(FY-3B VIRR)satellite data,we applied random forest(RF)methodology and selected 13 feature variables to obtain snow cover.A training set was generated,containing approximately 1 million snow and nonsnow samples obtained in China from the snow monitoring reports issued by the National Satellite Meteorological Centre and four snow cover products from the Interactive Multi-sensor Snow and Ice Mapping System(IMS),the FY-3B Multi-Sensor Synergy(MULSS),the Moderate Resolution Imaging Spectroradiometer(MODIS)snow cover product(MYD10A1),and the National Cryosphere Desert Data Center(NCDC).This training set contained many different samples of cloud types and snow under forest cover to help effectively distinguish snow and clouds and improve the recognition rate of snow under forest cover.Then,two RF snow cover recognition models were constructed for the snow and nonsnow seasons and they were used to conduct daily snow cover recognition in China from 2011 to 2020.The results show that the RF models constructed based on FY-3B VIRR data have good recognition performance for shallow snow,understory snow,and snow on the Qinghai–Tibetan Plateau.The recognition accuracy against weather stations and the spatial consistency with the IMS product are better than the MULSS,MYD10A1,and NCDC products.The overall accuracy of the RF product is 90.6%,and the recall rate is 93.8%.The omission and commission errors are 6.2%and11.1%,respectively.Unlike other existing snow cover algorithms,the established RF model skips the complicated atmospheric correction and cloud identification processes and does not involve external auxiliary data;thus,it is more easily popularized and operationally applicable to generating long-time series snow cover products.展开更多
Composite materials are increasingly used in the aerospace industry.To fully realise the weight saving potential along with superior mechanical properties that composites offer in safety critical applications,reliable...Composite materials are increasingly used in the aerospace industry.To fully realise the weight saving potential along with superior mechanical properties that composites offer in safety critical applications,reliable Non-Destructive Testing(NDT)methods are required to prevent catastrophic failures.This paper will review the state of the art in the field and point to highlight the success and challenges that different NDT methods are faced to evaluate the integrity of critical aerospace composites.The focus will be on advanced certificated NDT methods for damage detection and characterization in composite laminates for use in the aircraft primary and secondary structures.展开更多
Objective:To evaluate the antioxidant and anti-inflammatory potential of the aqueous extract and polysaccharide fraction from two brown marine macroalga,Padina gymnospora(P.gymnospora)and Padina tetrastomatica(P.tetra...Objective:To evaluate the antioxidant and anti-inflammatory potential of the aqueous extract and polysaccharide fraction from two brown marine macroalga,Padina gymnospora(P.gymnospora)and Padina tetrastomatica(P.tetrastomatica)harvested from Gulf of Mannar of peninsular India.Methods:The antioxidant activity was evaluated using different in vitro systems,viz.,1,1-diphenyl-2-picrylhydrazyl(DPPH),2,2′-azino-bis-3ethylbenzothiozoline-6-sulfonic acid diammonium salt(ABTS),H_(2)O_(2)/HO.radical scavenging,Fe^(2+)ion chelating ability,and reducing potential.Folin–Ciocalteu method was used to determine the total phenolic content,and the results were expressed as mg of gallic acid equivalents(GE).Thiobarbituric acid-reactive substance formation inhibition assay was employed to assess the ability of the samples to inhibit lipid oxidation in a model system.COX_(II)and LOX_(V)inhibition assays were employed to assess the anti-inflammatory potential of aqueous extract and polysaccharide fraction.Results:The aqueous extract fraction of P.tetrastomatica realized high total phenolic content(288 mg GE/g),and its activity towards scavenging short-lived radicals(OH.and H_(2)O_(2))(27.8%and 68.3%,respectively;0.6 mg/mL)are higher than those registered for Padina gymnospora.Aqueous extract and polysaccharide fractions of P.gymnospora showed higher anti-inflammatory activities against LOX_(V)(56%and 53%,respectively)and COX_(II)(30%and 35%,respectively;1 mg/mL)enzymes.The correlation studies confirmed that polysaccharides present with the Padina sp.are responsible for their anti-inflammatory potential.IR spectral data of polysaccharide fraction revealed the presence of polysaccharide in alginate form and also confirmed the presence of sulphated polysaccharides as principle bioactive constituents.Conclusions:The study revealed that these seaweeds possess beneficial value as human food or health additives and can be used as a natural green remedy against oxidative stress induced inflammatory diseases.展开更多
A glycine–nitrate self-propagating high-temperature synthesis(SHS)was developed to produce composite MgO-Gd_(2)O_(3) nanopowders.The X-ray powder diffraction(XRD)analysis confirmed the SHS-product consists of cubic M...A glycine–nitrate self-propagating high-temperature synthesis(SHS)was developed to produce composite MgO-Gd_(2)O_(3) nanopowders.The X-ray powder diffraction(XRD)analysis confirmed the SHS-product consists of cubic MgO and Gd_(2)O_(3) phases with nanometer crystallite size and retains this structure after annealing at temperatures up to 1200℃.Near full dense high IR-transparent composite ceramics were fabricated by spark plasma sintering(SPS)at 1140℃and 60 MPa.The in-line transmittance of 1 mm thick MgO-Gd_(2)O_(3) ceramics exceeded 70%in the range of 4–5 mm and reached a maximum of 77%at a wavelength of 5.3 mm.The measured microhardness HV0.5 of the MgO-Gd2O3 ceramics is 9.5±0.4 GPa,while the fracture toughness(KIC)amounted to 2.0±0.5МPa·m1/2.These characteristics demonstrate that obtained composite MgO-Gd_(2)O_(3) ceramic is a promising material for protective infra-red(IR)windows.展开更多
文摘Cases are presented to reveal how modern computerised infra-red thermal imaging has the potential to assist in early breast cancer detection. The history of thermography and some recent controversies surrounding mammography are discussed. Examples of thermal imaging combined with naturopathic interventions are described. Since 2002, more than 8000 women in New Zealand have chosen to include thermal imaging as a part of their breast health management. Breast thermal imaging combined with relevant health advice, resulted in a perceived worthwhile benefit to patients in managing overall health.
基金supported by grants awarded by the National Major Scientic Research Program of China(Grant No.2011CB910404)the National Nature Science Foundation of China(Grant No.61227017)+1 种基金the State Key Basic Research Development Program of China(2012CB518103)National Outstanding Young Scientist Award of China(61425006).
文摘Alzheimers disease(AD)is a chronic neurodegenerative disease.The symptoms include memoryand spatial learning dificulties,language disorders,and loss of motivation,which get worse overtime,eventually ending in death.No ffective treatments are available for AD,currently.Currenttreatments only attenuate symptoms temporarily and are associated with severe side ffects.Nearinfra-red(NIR)light has been studied for a long time.We investigated the effect of NIR on ADusing a transgenic mouse model,which was obtained by co-injecting two vectors carrying ADmutations in amyloid precursor protein(APP)and presenilin-i(PSEN1)into C57BL/6J mice.The irradiation equipment consisted of an accommodating box and an LED array.The wave-length of NIR light emitted from LED was between 1040 nm and 1090 nm.The power densitydelivered at the level of the mice was approximately 15 mW/cm^(2),Firstly,we treated the micewith NIR for 40 days,Then,the irradiation was suspended for 28 days.Finally,another 15 daystreatment was brought to mice.We conducted Morris water maze and immunofluorescenceanalysis to evaluate the effects of treatment.Immunofuorescence analysis was based on mea-suring the quantity of plaques in mouse brain slices,Our results show that NIR light improvesmemory and spatial learning ability and reduces plaques moderately.NIR light represents apotential treatment for AD.
文摘Introduction: Infra-red (IR) thermometry is a safe and valid method to determine internal and surface temperature in human subjects. Under conditions of brain damage (head injury or stroke) knowledge of changes in the temperature of intracranial tissue is justified because of the vulnerability of neurons to accelerated damage at temperatures at the upper end of the febrile range. Aim: To determine the temperature at the inner canthus (IC) of the eye as a potential surrogate for brain temperature. Methods: Invasive monitoring of deep brain structures, lateral ventricle and deep white matter. IR temperature readings obtained at right and left IC. Results: ?Strong correlations were evident between R and L IC and brain. Close, as well as poor, agreement between?? sites was shown in some patients and at some times. For right hemispheric lesions four had a better correlation between TbrV and TRIC when compared to TLIC.? When the correlation between TbrV and TLIC was better compared to TbrV and TRIC, four had a predominant right hemispheric lesion. Conclusions: Improved techniques for IR thermal imaging accuracy at the bedside has the potential to improve temperature measurement agreement. The predominant lesion side may have a bearing on maximum ipsilateral IC temperature Further studies are ongoing in this pilot study population.
基金Bombardier Aerospace,Thales Canada,The Consortium in Research and Aerospace in Canada(CRIAQ)the Natural Sciences and Engineering Research Council of Canada(NSERC)for their financial support
文摘In the present paper, an ‘in-house' genetic algorithm was numerically and experimentally validated. The genetic algorithm was applied to an optimization problem for improving the aerodynamic performances of an aircraft wing tip through upper surface morphing. The optimization was performed for 16 flight cases expressed in terms of various combinations of speeds, angles of attack and aileron deflections. The displacements resulted from the optimization were used during the wind tunnel tests of the wing tip demonstrator for the actuators control to change the upper surface shape of the wing. The results of the optimization of the flow behavior for the airfoil morphing upper-surface problem were validated with wind tunnel experimental transition results obtained with infra-red Thermography on the wing-tip demonstrator. The validation proved that the 2D numerical optimization using the ‘in-house' genetic algorithm was an appropriate tool in improving various aspects of a wing's aerodynamic performances.
文摘Background: Accurate temperature measurement is a critical step in evaluating health or disease especially in children and immmunocompromised subjects;inaccurate measurement may lead to improper diagnosis, wrong treatment or inappropriate intervention. Several methods of temperature measurements exist and comparing these gives room for choosing a near ideal method in terms of speed, safety and accuracy. The study aimed to compare the forehead non touch infra-red thermometer with the axilllary mercury-in-glass method of temperature measurement in the Paediatric age-group. Methods: Study was given ethical approval as part of a larger study. Four hundred and thirty seven children aged 1 to 24 months were studied at the well-baby/immunizationclinic of the University of Ilorin Teaching Hospital over a 6-months period. Both non-touch infrared and theregular mercury-in-glass thermometers were used to take the body temperatures. Data were analysed with SPSS version 21. Pearson correlation was used to determine the relationship between the two methods of temperature measurements, while Bland-Altman method was used to test for level of agreement between them. Results: The mean age and SD was 5.81 ± 4.04 months. Pearson correlation showed a positive correlation between the axillary mercury-in-glass and forehead non-touch infra-red thermometry readings (r = 0.281, p < 0.001). Also, Bland-Altman method revealed a good agreement between both methods of thermometry as 96% of the readings were within the limits of agreement. Mean difference was 0.09°C (95% confidence interval 0.05 - 0.13). Conclusion: Axillary mercury-in-glass thermometer and forehead non touch infra-red thermometers have a good agreement and can be used interchangeably.
文摘Background: Neonatal temperature response during illness is unpredictable. Whereas accurate temperature measurement is an important diagnostic step in Neonatal practice. Abnormalties in temperature pattern may be a pointer to a sinister condition especially in neonates, whose thermoregulatory mechanism is immature. There are several methods of temperature measurements and the search for a suitable thermometry method in neonates continues. This study compared the forehead non touch infra-red thermometer (NTIT) with the axilllary mercury-in-glass (MIGT) method of temperature measurement in neonates. Method: Four hundred babies aged 1 to 28 days were recruited from the immunization clinic of the University of Ilorin Teaching Hospital between August 2016 and May 2017. Temperatures were taken using both NTIT and MIGT in the standard way and recorded.?Result: The mean age and SD was 5.10 ± 4.28?days. Pearson correlation showed a positive correlation between the Axillary Mercury-in-Glass and Forehead Non-Touch Infra-red thermometry readings (r?=?0.426, p??0.001). Bland-Altman method revealed a good agreement between both methods of thermometry as 95.5% of the readings were within the limits of agreement. Conclusion: Axillary Mercury-in-Glass thermometer and Forehead Non touch Infra-red thermometers have a good agreement and can be used interchangeably in neonates.
文摘A hypothesis is advanced in which life began from a Darwinian selection among a diversification of molecular species containing the phosphate moiety which broke the constraints implicit in the Second Law of Thermodynamics, discussed famously by Schrodinger, by obtaining energy from specific infrared frequencies located in the phosphorus-oxygen vibration at a frequency around 1000 cm-1. We propose the source of this energy was from the internal conversion of solar broadband energy by the phosphate mineral Apatite, present at the bottom of a primitive biogenesis pond. In this scenario, life is re-defined as being hotter than its environment and as using its excess energy, supplied by infra-red conversion, to react with its molecular environment and pump itself up the “entropy slope” thereby;replication is through breakages of increasingly large phosphate containing biopolymers. The idea has implications for modern explanations of living systems.
文摘This study evaluated the possibility of infrared thermography to measure accurately the temperature of elements of a rotating device, within the scope of condition monitoring. The tested machine was a blower coupled to a 500 kW electric motor, that operated in multiples regimes. The thermograms were acquired by a fixed thermographic camera and were processed and recorded every 15 minutes. Because the normal temperature variations could easily mask a drift caused by a failure, a corrected temperature was computed using autorecursive models. It was shown that an efficient temperature correction should compensate for the variations of the process, and for the ambient temperatures variations, either daily or seasonal. The standard deviation of the corrected temperature was of a few tenth of degree, making possible the detection of a drift of less than one degree and the prediction of potential failure.
文摘Gas chromatography is an analytical tool for the separation of compounds in complex mixtures based on the polarity of compounds. Separation is achieved only for compounds that are volatile or that can be made volatile on derivatization of the compound using derivatizing agents. This is one of the widely accepted tools for the separation of compounds because of its simplicity, sensitivity, and effectiveness. The principle of separation of compounds depends on the partitioning behaviour difference between mobile and stationary phase, the sample is carried by a moving gas stream through a tube packed with a finely divided solid or may be coated with a film of a liquid. Different types of columns having a various composition of stationary phase are been used for the separation of different classes of compounds mixture or sample in a suitable solvent is introduced through the injector maintained at higher temperature which is capable of volatilizing the compound into the column.
文摘In order to study adsorption of preservatives by eyeliner pen package,the chemical compositions of the commercially available Eyeliner package were analyzed by infrared spectrometer.It was found that these package components were PP,PET,modified PP,modified PET,ABS,nylon,PU and so on.The adsorption effects of these components on three preservatives,i.e.phenoxyethanol,Methyl paraben and Propyl paraben have been further studied by high performance liquid chromatography.The results demonstrated that the four chemical materials PET,PP,modified PP and ABS had no adsorption on the above three preservatives.However,the component named of water diversion core which was composed of modified PET,and nylon-made cotton head have been observed of slight adsorption in this study.And components as the function of preventing liquid leakage,which was made of PU,have presented the most serious adsorption on these three preservatives,with the adsorption order as Propyl Paraben>Methyl Paraben>phenoxyethanol.
基金Supported by the National Natural Science Foundation of China (U2242211)Hunan Provincial Natural Science Foundation (2021JC0009)Jiangsu Provincial Natural Science Foundation (BK20201505)。
文摘Currently,there is variability in the spectral band thresholds for snow cover recognition using remote sensing in different regions and for complex terrains.Using Fengyun-3B Visible and Infra-Red Radiometer(FY-3B VIRR)satellite data,we applied random forest(RF)methodology and selected 13 feature variables to obtain snow cover.A training set was generated,containing approximately 1 million snow and nonsnow samples obtained in China from the snow monitoring reports issued by the National Satellite Meteorological Centre and four snow cover products from the Interactive Multi-sensor Snow and Ice Mapping System(IMS),the FY-3B Multi-Sensor Synergy(MULSS),the Moderate Resolution Imaging Spectroradiometer(MODIS)snow cover product(MYD10A1),and the National Cryosphere Desert Data Center(NCDC).This training set contained many different samples of cloud types and snow under forest cover to help effectively distinguish snow and clouds and improve the recognition rate of snow under forest cover.Then,two RF snow cover recognition models were constructed for the snow and nonsnow seasons and they were used to conduct daily snow cover recognition in China from 2011 to 2020.The results show that the RF models constructed based on FY-3B VIRR data have good recognition performance for shallow snow,understory snow,and snow on the Qinghai–Tibetan Plateau.The recognition accuracy against weather stations and the spatial consistency with the IMS product are better than the MULSS,MYD10A1,and NCDC products.The overall accuracy of the RF product is 90.6%,and the recall rate is 93.8%.The omission and commission errors are 6.2%and11.1%,respectively.Unlike other existing snow cover algorithms,the established RF model skips the complicated atmospheric correction and cloud identification processes and does not involve external auxiliary data;thus,it is more easily popularized and operationally applicable to generating long-time series snow cover products.
基金the support of NVIDIA Corporation with the donation of the Titan Xp GPU used for this researchsupported by EPSRC grant EP/R002495/1the European Metrology Research Programme through grant 17IND08。
文摘Composite materials are increasingly used in the aerospace industry.To fully realise the weight saving potential along with superior mechanical properties that composites offer in safety critical applications,reliable Non-Destructive Testing(NDT)methods are required to prevent catastrophic failures.This paper will review the state of the art in the field and point to highlight the success and challenges that different NDT methods are faced to evaluate the integrity of critical aerospace composites.The focus will be on advanced certificated NDT methods for damage detection and characterization in composite laminates for use in the aircraft primary and secondary structures.
基金Supported by the funding under the Science and Engineering Research Council(SERC)Scheme(SR/FTP/CS-63/2007)from Department of Science and Technology,New Delhi,India.
文摘Objective:To evaluate the antioxidant and anti-inflammatory potential of the aqueous extract and polysaccharide fraction from two brown marine macroalga,Padina gymnospora(P.gymnospora)and Padina tetrastomatica(P.tetrastomatica)harvested from Gulf of Mannar of peninsular India.Methods:The antioxidant activity was evaluated using different in vitro systems,viz.,1,1-diphenyl-2-picrylhydrazyl(DPPH),2,2′-azino-bis-3ethylbenzothiozoline-6-sulfonic acid diammonium salt(ABTS),H_(2)O_(2)/HO.radical scavenging,Fe^(2+)ion chelating ability,and reducing potential.Folin–Ciocalteu method was used to determine the total phenolic content,and the results were expressed as mg of gallic acid equivalents(GE).Thiobarbituric acid-reactive substance formation inhibition assay was employed to assess the ability of the samples to inhibit lipid oxidation in a model system.COX_(II)and LOX_(V)inhibition assays were employed to assess the anti-inflammatory potential of aqueous extract and polysaccharide fraction.Results:The aqueous extract fraction of P.tetrastomatica realized high total phenolic content(288 mg GE/g),and its activity towards scavenging short-lived radicals(OH.and H_(2)O_(2))(27.8%and 68.3%,respectively;0.6 mg/mL)are higher than those registered for Padina gymnospora.Aqueous extract and polysaccharide fractions of P.gymnospora showed higher anti-inflammatory activities against LOX_(V)(56%and 53%,respectively)and COX_(II)(30%and 35%,respectively;1 mg/mL)enzymes.The correlation studies confirmed that polysaccharides present with the Padina sp.are responsible for their anti-inflammatory potential.IR spectral data of polysaccharide fraction revealed the presence of polysaccharide in alginate form and also confirmed the presence of sulphated polysaccharides as principle bioactive constituents.Conclusions:The study revealed that these seaweeds possess beneficial value as human food or health additives and can be used as a natural green remedy against oxidative stress induced inflammatory diseases.
基金funded by the Russian Science Foundation(Research Project No.19-73-10127)。
文摘A glycine–nitrate self-propagating high-temperature synthesis(SHS)was developed to produce composite MgO-Gd_(2)O_(3) nanopowders.The X-ray powder diffraction(XRD)analysis confirmed the SHS-product consists of cubic MgO and Gd_(2)O_(3) phases with nanometer crystallite size and retains this structure after annealing at temperatures up to 1200℃.Near full dense high IR-transparent composite ceramics were fabricated by spark plasma sintering(SPS)at 1140℃and 60 MPa.The in-line transmittance of 1 mm thick MgO-Gd_(2)O_(3) ceramics exceeded 70%in the range of 4–5 mm and reached a maximum of 77%at a wavelength of 5.3 mm.The measured microhardness HV0.5 of the MgO-Gd2O3 ceramics is 9.5±0.4 GPa,while the fracture toughness(KIC)amounted to 2.0±0.5МPa·m1/2.These characteristics demonstrate that obtained composite MgO-Gd_(2)O_(3) ceramic is a promising material for protective infra-red(IR)windows.