Laboratory insights into the effects of methane hydrate on the anisotropic joint elastic-electrical properties in fractured sandstones

Fractured hydrate-bearing reservoirs show significantly anisotropic geophysical properties. The joint application of seismic and electromagnetic explorations is expected to accurately assess hydrate resources in the fractured reservoirs. However, the anisotropic joint elastic-electrical properties in such reservoirs that are the key to the successful application of the joint explorations, remain poorly understood. To obtain such knowledge, we designed and implemented dedicated laboratory experiments to study the anisotropic joint elastic-electrical properties in fractured artificial silica sandstones (with fracture density of about 6.2%, porosity of approximately 25.7%, and mean grainsize of 0.089 mm) with evolving methane hydrate. The experimental results showed that the anisotropic compressional wave velocities respectively increased and decreased with the forming and dissociating hydrate, and the variation in the increasing trend and the decreasing extent of the velocity perpendicular to the fractures were more significant than that parallel to the fractures, respectively. The experimental results also showed that the overall decreasing trend of the electrical conductivity parallel to the fractures was steeper than that perpendicular to the fractures during hydrate formation, and the general variations of the two conductivities with complex trend were similar during hydrate dissociation. The variations in the elastic and electrical anisotropic parameters with forming and dissociating hydrate were also found to be distinct. Interpretation of the experimental results suggested that the hydrate binding to the grains evolved to bridge the surfaces of fractures when saturation exceeded 10% during hydrate formation, and the bridging hydrate gradually evolved to floating in fractures during dissociation. The experimental results further showed that the anisotropic velocities and electrical conductivities were correlated with approximately consistent trends of different slopes during hydrate formation, and the joint elastic-electrical anisotropic parameters exhibited a sharp peak at the hydrate saturation of about 10%. The results suggested that the anisotropic joint properties can be employed not only to accurately estimate hydrate saturation but also possibly to identify hydrate distribution in the fractures.

A roughness parameter considering joint material properties and peak shear strength model for rock joints

This study aims at proposing a reasonable roughness parameter that can reflect the peak shear strength(PSS)of rock joints.Firstly,the contribution of the asperities with different apparent dip angles to shear strength is studied.Then the shear strength of the entire joint asperities is derived.The results showed that the PSS of the entire joint asperities is proportional to a key parameter hs,which is related to the geometric character of the joint surface and the joint material properties.The parameter hsis taken as the new roughness parameter,and it is reasonable to associate the PSS with the geometric characteristics of the joint surface.Based on the new roughness parameter and shear test results of 20 sets of joint specimens,a new PSS model for rock joints is proposed.The new model is validated with the artificial joints in this paper and real rock joints in published studies.Results showed that it is suitable for different types of rock joints except for gneiss joints.The new model has the form of the Mohr-Coulomb model,which can directly reflect the relationship between the 3 D roughness parameters and the peak dilation angle.

Effect of Post-weld Heat Treatment on Mechanical Characteristics of AZ31 Magnesium Alloy Welded Joints

Tungsten inert gas（TIG） welding was performed on 2.7 mm thick commercial extruded AZ31 B magnesium alloy plates. We investigated the effect of post-weld heat treatment（PWHT） on the microstructure, mechanical properties and precipitated phase of the weld joints. The results showed that during the annealing treatment（200 ℃-1 h, 250 ℃-1 h, 300 ℃-1 h, 350 ℃-1 h, 400 ℃-1 h, and 450 ℃-1 h）, the average grain size in the weld seam was the minimum after annealing at 400 ℃ for 1 hour, and then abnormally grew up after annealing at 450 ℃ for 1 hour. The mechanical properties enhanced when the joints were processed from 200 ℃-1 h to 400 ℃-1 h but sharply decreased with increasing annealing temperature. In contrast to the annealing treatment, solution treatment（250 ℃-10 h, 300 ℃-10 h, 350 ℃-10 h, 400 ℃-10 h, and 450 ℃-10 h） exhibited a better ductility but a slight deterioration in tensile strength. Especially speaking, no eutectic compounds（such as Mg17 Al12） were observed in the weld seam. The supersaturated Al atoms were precipitated in a coarse spherical shape dispersed in the weld seam. The precipitated Al atoms dissolved in the matrix substances at the condition（400 ℃-1 h） or（250 ℃-10 h）. The solution treatment caused grain coarsening and precipitated Al atoms dissolved in the weld seam substantially, which resulted in a drop in micro-hardness at the weld seam compared to the area of the annealed joints.

Influence of flash trap profiles on joint properties of friction welded CP-Ti tube to 304L stainless steel tube plate using external tool

Titanium tube and stainless steel tube plate were welded by an innovative friction welding of tube to tube plate using an external tool (FWTPET). Copper was used as an interlayer for joining the dissimilar materials and also to minimize the effect of intermetallics formed at the joint interface. The process parameters that govern FWTPET process are plunge rate, rotational speed, plunge depth, axial load and flash trap profile. Among them, the flash trap profile of the tube has a significant influence on the joint integrity. Various flash trap profiles like vertical slots, holes, zig-zag holes, and petals were made on the titanium tube welded to the stainless steel tube plate. Macroscopic and microscopic studies reveal defect-free joints. The presence of copper interlayer and intermetallics was evident from X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS) studies. The microhardness survey was presented across and along the interface. A novel test procedure called “plunge shear test” was developed to evaluate the joint properties of the welded joints. The highest shear fracture load of 31.58 kN was observed on the sample having petals as flash trap profile. The sheared surfaces were further characterized using SEM for fractography.

Research on the properties of MAG welded joint of X65 pipeline steel

With the worldwide pipeline construction boom, the pipeline welding technology has rapidly developed. Considering the needs of some projects, many tests of mechanical properties of X65 pipeline steel metal active-gus （MAG） welded joint have been carried out, and so do the analysis of metallographic structure characteristics and the impact fracture appearance of joint. The results show that, using MAG welding, the test data of mechanical properties of their girth welded joint are in conformity with the relevant technical standards （ API1104 ）. MAG welding with COz protection has the characteristics of low hydrogen, energy-saving and environmental protection. Therefore, it should be noted to develop the welding materials and equipments vigorously for this welding method.

An Average Failure Index Method for the Tensile Strength Prediction of Composite Adhesive-bonded π Joints

An average failure index method based on accurate FEA was proposed for the tensile strength prediction of composite out-of-plane adhesive-bonded π joints. Based on the simple and independent maximum stress failure criterion, the failure index was introduced to characterize the degree of stress components close to their corresponding material strength. With a brief load transfer analysis, the weak fillers were prominent and further detailed discussion was performed. The maximum value among the average failure indices which were related with different stress components was filtrated to represent the failure strength of the critical surface, which is either the two curved upside surfaces or the bottom plane of the fillers for composite π joints. The tensile strength of three kinds of π joints with different material systems, configurations and lay-ups was predicted by the proposed method and corresponding experiments were conducted. Good agreements between the numerical and experimental results give evidence of the effectiveness of the proposed method. In contrast to the existed time-consuming strength prediction methods, the proposed method provides a capability of quickly assessing the failure of complex out-of-plane joints and is easy and convenient to be widely utilized in engineering.

Joint DOA and polarization estimation for unequal power sources based on reconstructed noise subspace

In most literature about joint direction of arrival（DOA） and polarization estimation, the case that sources possess different power levels is seldom discussed. However, this case exists widely in practical applications, especially in passive radar systems. In this paper, we propose a joint DOA and polarization estimation method for unequal power sources based on the reconstructed noise subspace. The invariance property of noise subspace（IPNS） to power of sources has been proved an effective method to estimate DOA of unequal power sources. We develop the IPNS method for joint DOA and polarization estimation based on a dual polarized array. Moreover, we propose an improved IPNS method based on the reconstructed noise subspace, which has higher resolution probability than the IPNS method. It is theoretically proved that the IPNS to power of sources is still valid when the eigenvalues of the noise subspace are changed artificially. Simulation results show that the resolution probability of the proposed method is enhanced compared with the methods based on the IPNS and the polarimetric multiple signal classification（MUSIC） method. Meanwhile, the proposed method has approximately the same estimation accuracy as the IPNS method for the weak source.

Educational Function of the Family Property Legal System in China's Civil Code-Research on the Core Socialist Values

The educational function of law is to inherently and positively standardize and institutionalize core ideologies and values by directly affecting those ideologies,incorporating the outlook on values,ethics,life and honor and disgrace.The purpose of the Legislative Revision Plan of Integrating the Core Socialist Values into the Construction of Rule of Law,adopted by China's central government in 2018,is to comprehensively strengthen the educational function of law under the guidance of the socialist core values within the entire socialist legal system,to consolidate a solid socialist ideological foundation,and to improve ideology and ethics across China.As a family is the cell of a society and the first classroom of life,family value is not only at the core of a family but also an essential part of a society.The legal system relating to family property,based on the family property system and spousal inheritance right,can rationally adjust the family property relationship;this system can combine,cultivate and carry forward socialist core values,guide and cultivate ethics,and promote family values,family culture and family traditions.Moreover,it can educate people to formulate an appropriate outlook on life,values and money and sense of honor.Today,the legal system of family property,such as the joint possession of marital incomes and the unlimited right to spousal inheritance,has shown a negative effect on educational function,since it was born during the period of the relative shortage of family property in the past.Therefore,the Civil Code should follow the socialist core values,and update and innovate the family property legal system and thereby provide an effective and efficient path to rectify the hitherto negative effect on educational function of the family property legal system.

Transient liquid phase diffusion bonding of a single crystal superalloy DD6

DD6 alloy was bonded by transient liquid phase (TLP) diffusion bonding. The main compositions of the interlayer alloy employed were similar to those of the base metal, DD6, and a certain amount of element B was added as the melting point depressant. The results show that it is difficult to obtain the joints with the microstructures completely homogeneous. For the joint TLP diffusion bonded at 1290℃ for 12h, about half areas of the beam possessed a γ+γ′ microstructure, nearly identical with that of the base metal, and the other local areas consisted of γ-solution, borides, etc. Prolonging the bonding time to 24h, the inhomogeneous areas in the joint reduced, and the joint property improved. The joint stress-rupture strength at 980℃ and 1100℃ reached 90%-100% and 70%-80% of those of the base metal respectively.

Welding technique studies on the “West-East” pipeline project

This paper described the work of welding process design for the ＂ West-East＂ pipeline project, which is high pressure, large diameter and heavy wall thickness. According to the different geographical situation, climate, culture and the flexibility of the welding methods, this work recommended the semi-automatic process at the east and middle sections and automatic process at the west section of the pipeline project. The manual process is recommended on the tie-in joints and repairs. The double joint pipe and the 3 joint pipe are recommended at the water net place and some in-ditch welding place to reduce the welding volume. Also the special redesigned bevels are recommended for the automatic process and the semiautomatic process. Through all destructive tests, the results shows the welds are meet the requirements of related standards, specifications and design documents.

Twin-wire SAW welding of 70 kg class high strength steel

The twin-wire SAW welding process was investigated using Baosteel 70 kg class high strength steel, and the properties of the joints were studied using conventional single and double-faced grooves as well as an optimized groove. The results showed that by using an optimized double-faced groove, a small root face, and no back gouging, a small welding heat input was achieved and thus the joint strength and toughness were improved significantly. Also, removing back gouging reduced the labor required in the process. The weld reinforcement and deformation were observed to be rather small.

Joint elastic-electrical properties of sediments in the Yellow Sea

We measured in the laboratory compressional wave velocity and electrical resistivity on 434 sediment samples collected from the Yellow Sea to study the joint elastic-electrical properties of marine sediments. Porosity was found to reduce both elastic velocity and electrical resistivity of the marine sediments in a non-linear fashion; velocity showed an approximate linear increase with increasing logarithm of resistivity. Various effective medium models either implemented or developed were compared with the new dataset. The model results showed that the combined self-consistent approximation and differential effective medium model using critical porosity of 0.6 and 0.5 for velocity and resistivity respectively gave a reasonable description of the joint elastic-electrical behaviors of the marine sediments. The joint elastic-electrical properties of the marine sediments established would be used to estimate resistivity from measured velocity and vice versa, and could also be suitable for detection of gas hydrate or other suitable targets from joint seismic-resistivity surveys.

Microstructure and properties in dissimilar/similar weld joints between DP780 and DP980 steels processed by fiber laser welding

The microstructure and mechanical properties（strength, fatigue and formability） of dissimilar/similar weld joints between DP780 and DP980 steels were studied. The microstructure in fusion zone（FZ） was lath martensite（LM）, and alloying elements in the FZ were uniformly distributed. The hardness in the FZ of dissimilar weld joint was similar to the average value（375 HV） of the two similar weld joints. The microstructural evolution in heat affected zone（HAZ） of dissimilar/similar weld joints was as follows：LM（coarse-grained HAZ） →finer LM（fine-grained HAZ） →M-A constituent and ferrite（intercritically HAZ） →tempered martensite（TM） and ferrite（sub-critical HAZ）. Lower hardness in intercritically HAZ and sub-critical HAZ（softening zones） was observed compared to base metal（BM） in dissimilar/similar weld joints. The size of softening zone was 0.2-0.3 mm and reduction in hardness was ~7.6%-12.7% of BM in all the weld joints, which did not influence the tensile properties of weld joints such that fracture location was in BM. Formability of dissimilar weld joints was inferior compared to similar weld joints because of the softening zone, non-uniform microstructure and hardness on the two sides of FZ. The effect of microstructure on fatigue life was not influenced due to the presence of welding concavity.

Evaluation of tensile properties of a compositemetal joint with a novel metal insert design by experimental and numerical methods

Composite-metal joints with a metal insert are one kind of connecting structure.In this paper,tensile experimental tests were carried out to investigate tensile properties of a compositemetal joint with a novel metal insert design.Finite element models of the joint were established,and strain distribution and tensile strength were analyzed.The numerical results are in good agreement with the experimental results.Results show that the joint failure is dominated by shear properties of the resin layer.Increasing the resin layer thickness in a certain range will improve the tensile strength of the joint,while increasing the radius of the fillet on the ending side of the metal insert will decrease the joint strength.Increasing the resin layer plasticity will improve the joint strength.The effect of the embedded depth of the metal insert can be ignored.

Descriptors for DNA Sequences Based on Joint Diagonalization of Their Feature Matrices from Dinucleotide Physicochemical Properties

Numerical characterizations of DNA sequence can facilitate analysis of similar sequences. To visualize and compare different DNA sequences in less space, a novel descriptors extraction approach was proposed for numerical characterizations and similarity analysis of sequences. Initially, a transformation method was introduced to represent each DNA sequence with dinucleotide physicochemical property matrix. Then, based on the approximate joint diagonalization theory, an eigenvalue vector was extracted from each DNA sequence,which could be considered as descriptor of the DNA sequence. Moreover, similarity analyses were performed by calculating the pair-wise distances among the obtained eigenvalue vectors. The results show that the proposed approach can capture more sequence information, and can jointly analyze the information contained in all involved multiple sequences, rather than separately, whose effectiveness was demonstrated intuitively by constructing a dendrogram for the 15 beta-globin gene sequences.

Solid-Liquid State Bonding of Si3N4 Ceramics with Ceramic-Modified Brazing Alloy

Solid-liquid state bonding of Si3N4 ceramics with TiN-modified Ag-Cu-Ti brazing alloy was used'- to enhance joint strength. The effects of the TiN particles on the microstructures, interfacial reactions, and room-temperature properties of the joints were investigated. The results show that the TiN particles are gen- erally well dispersed in the Ag-Cu eutectic base and the interface between them is both clean and com-pact. Changes in the TiN volume fractions from 0 to 20% exert no noticeable effect on the interfacial reac-tion between Ag-Cu-Ti and the substrates. Other bonding parameters being constant, the TiN volume frac-tion in the filler material plays a key role in the joint properties. For TiN volume fractions below 20%, the joints are reinforced, especially joints with 5% and 20% TiN. The average shearing strength of joints with 5% TiN is 200.8 MPa, 30% higher than that of joints with no TiN (154.1 MPa). However, for TiN volumes frac- tions above 20%, the joint strengths decrease.

Development and application of software packages in welding engineering

The weldabiUty of some material is analyzed with simple calculating program in this paper, and weldability testing data are shared through database system. The welding procedures are designed with help of expert systems, and the knowledge is shared among welding engineers. Not only the preparing progress of the welding documents is completed with database systems but also the complex decision on the necessity of the qualification test according to the present procedure qualification records （PQRs） and manufacture codes is made. Moreover, the artificial neural network （ANN） technique is proven to be one of the effective ways to predict mechanical properties of welded joints when there are enough tested data to train the models. Finally, the achievements in modeling microstructure of welded joints are introduced, especially in solid transformation and grain growth in both heat-affected zone （HAZ） and welded molten pool.