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LEAST-SQUARES METHOD-BASED FEATURE FITTING AND EXTRACTION IN REVERSE ENGINEERING 被引量:3
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作者 Ke YinglinSun QingLu ZhenCollege of Mechanical andEnergy Engineering,Zhejiang University,Hangzhou 310027, China 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2003年第2期163-166,共4页
The main purpose of reverse engineering is to convert discrete data pointsinto piecewise smooth, continuous surface models. Before carrying out model reconstruction it issignificant to extract geometric features becau... The main purpose of reverse engineering is to convert discrete data pointsinto piecewise smooth, continuous surface models. Before carrying out model reconstruction it issignificant to extract geometric features because the quality of modeling greatly depends on therepresentation of features. Some fitting techniques of natural quadric surfaces with least-squaresmethod are described. And these techniques can be directly used to extract quadric surfaces featuresduring the process of segmentation for point cloud. 展开更多
关键词 reverse engineering feature extraction least-squares method segmentationand surface fitting
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NEGATIVE NORM LEAST-SQUARES METHODS FOR THE INCOMPRESSIBLE MAGNETOHYDRODYNAMIC EQUATIONS 被引量:2
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作者 高少芹 段火元 《Acta Mathematica Scientia》 SCIE CSCD 2008年第3期675-684,共10页
The purpose of this article is to develop and analyze least-squares approximations for the incompressible magnetohydrodynamic equations. The major advantage of the least-squares finite element method is that it is not... The purpose of this article is to develop and analyze least-squares approximations for the incompressible magnetohydrodynamic equations. The major advantage of the least-squares finite element method is that it is not subjected to the so-called Ladyzhenskaya-Babuska-Brezzi (LBB) condition. The authors employ least-squares functionals which involve a discrete inner product which is related to the inner product in H^-1(Ω). 展开更多
关键词 The incompressible MHDs equation negative norm VORTICITY least-squares mixed finite element method
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ON THE BREAKDOWNS OF THE GALERKIN AND LEAST-SQUARES METHODS 被引量:2
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作者 Zhong Baojiang(钟宝江) 《Numerical Mathematics A Journal of Chinese Universities(English Series)》 SCIE 2002年第2期137-148,共12页
The Galerkin and least-squares methods are two classes of the most popular Krylov subspace methOds for solving large linear systems of equations. Unfortunately, both the methods may suffer from serious breakdowns of t... The Galerkin and least-squares methods are two classes of the most popular Krylov subspace methOds for solving large linear systems of equations. Unfortunately, both the methods may suffer from serious breakdowns of the same type: In a breakdown situation the Galerkin method is unable to calculate an approximate solution, while the least-squares method, although does not really break down, is unsucessful in reducing the norm of its residual. In this paper we first establish a unified theorem which gives a relationship between breakdowns in the two methods. We further illustrate theoretically and experimentally that if the coefficient matrix of a lienar system is of high defectiveness with the associated eigenvalues less than 1, then the restarted Galerkin and least-squares methods will be in great risks of complete breakdowns. It appears that our findings may help to understand phenomena observed practically and to derive treatments for breakdowns of this type. 展开更多
关键词 large linear systems iterative methods Krylov subspace methods GALERKIN method least-squares method FOM GMRES breakdown stagnation restarting preconditioners.
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Initial costates derived by near-optimal reference sequence and least-squares method
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作者 Shaozhao LU Yao ZHANG Quan HU 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 2024年第5期377-391,共15页
In this paper,we present a novel initial costates solver for initializing time-optimal trajectory problems in relative motion with continuous low thrust.The proposed solver consists of two primary components:training ... In this paper,we present a novel initial costates solver for initializing time-optimal trajectory problems in relative motion with continuous low thrust.The proposed solver consists of two primary components:training a Multilayer Perceptron(MLP)for generating reference sequence and Time of Flight(TOF)to the target,and deriving a system of linear algebraic equations for obtaining the initial costates.To overcome the challenge of generating training samples for the MLP,the backward generation method is proposed to obtain five different training databases.The training database and sample form are determined by analyzing the input and output correlation using the Pearson correlation coefficient.The best-performing MLP is obtained by analyzing the training results with various hyper-parameter combinations.A reference sequence starting from the initial states is obtained by integrating forward with the near-optimal control vector from the output of MLP.Finally,a system of linear algebraic equations for estimating the initial costates is derived using the reference sequence and the necessary conditions for optimality.Simulation results demonstrate that the proposed initial costates solver improves the convergence ratio and reduce the function calls of the shooting function.Furthermore,Monte-Carlo simulation illustrates that the initial costates solver is applicable to different initial velocities,demonstrating excellent generalization ability. 展开更多
关键词 Relative motion Expanding training database Multilayer perceptron Initial costates least-squares method
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Application of neural network model coupling with the partial least-squares method for forecasting watre yield of mine 被引量:2
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作者 陈南祥 曹连海 黄强 《Journal of Coal Science & Engineering(China)》 2005年第1期40-43,共4页
Scientific forecasting water yield of mine is of great significance to the safety production of mine and the colligated using of water resources. The paper established the forecasting model for water yield of mine, co... Scientific forecasting water yield of mine is of great significance to the safety production of mine and the colligated using of water resources. The paper established the forecasting model for water yield of mine, combining neural network with the partial least square method. Dealt with independent variables by the partial least square method, it can not only solve the relationship between independent variables but also reduce the input dimensions in neural network model, and then use the neural network which can solve the non-linear problem better. The result of an example shows that the prediction has higher precision in forecasting and fitting. 展开更多
关键词 地下水 水量 矿山 人工神经网络 数学模型 动态预报模型
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Least-squares reverse time migration in visco-acoustic media based on symplectic stereo-modeling method
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作者 LI Jingshuang ZHANG Xiangjia +1 位作者 HE Xijun ZHOU Yanjie 《Global Geology》 2023年第4期237-250,共14页
The authors proposed a symplectic stereo-modeling method(SSM)in the Birkhoffian dynam-ics and apply it to the visco-acoustic least-squares reverse time migration(LSRTM).The SSM adopts ste-reo-modeling operator in spac... The authors proposed a symplectic stereo-modeling method(SSM)in the Birkhoffian dynam-ics and apply it to the visco-acoustic least-squares reverse time migration(LSRTM).The SSM adopts ste-reo-modeling operator in space and symplectic Runge-Kutta scheme in time,resulting in great ability in suppressing numerical dispersion and long-time computing.These advantages are further confirmed by numerical dispersion analysis,long-time computation test and computational efficiency comparison.After these theoretical analyses and experiments,acoustic and visco-acoustic LSRTM are tested and compared between SSM method and the conventional symplectic method(CSM)using the fault and marmousi models.Meanwhile,dynamic source encoding and exponential decay moving average gradients method are adopted to reduce the computation cost and improve the convergence rate.The imaging results show that LSRTM based on visco-acoustic wave equations effectively takes into account the influence of viscosity can therefore compensate for the amplitude attenuation.Besides,SSM method not only has high numerical accuracy and computational efficiency,but also performs effectively in LSRTM. 展开更多
关键词 least-squares reverse time migration visco-acoustic equation Birkhoffian dynamic symplectic stereo-modeling dynamic source encoding
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Solution of shallow-water equations using least-squares finite-element method 被引量:3
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作者 S.J. Liang J,-H, Tang M.-S. Wu 《Acta Mechanica Sinica》 SCIE EI CAS CSCD 2008年第5期523-532,共10页
A least-squares finite-element method (LSFEM) for the non-conservative shallow-water equations is presented. The model is capable of handling complex topography, steady and unsteady flows, subcritical and supercriti... A least-squares finite-element method (LSFEM) for the non-conservative shallow-water equations is presented. The model is capable of handling complex topography, steady and unsteady flows, subcritical and supercritical flows, and flows with smooth and sharp gradient changes. Advantages of the model include: (1) sources terms, such as the bottom slope, surface stresses and bed frictions, can be treated easily without any special treatment; (2) upwind scheme is no needed; (3) a single approximating space can be used for all variables, and its choice of approximating space is not subject to the Ladyzhenskaya-Babuska-Brezzi (LBB) condition; and (4) the resulting system of equations is symmetric and positive-definite (SPD) which can be solved efficiently with the preconditioned conjugate gradient method. The model is verified with flow over a bump, tide induced flow, and dam-break. Computed results are compared with analytic solutions or other numerical results, and show the model is conservative and accurate. The model is then used to simulate flow past a circular cylinder. Important flow charac-teristics, such as variation of water surface around the cylinder and vortex shedding behind the cylinder are investigated. Computed results compare well with experiment data and other numerical results. 展开更多
关键词 least-square finite-element method Shallow-water equations DAM-BREAK Vortex shedding
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Least-squares finite-element method for shallow-water equations with source terms 被引量:2
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作者 Shin-Jye Liang Tai-Wen Hsu 《Acta Mechanica Sinica》 SCIE EI CAS CSCD 2009年第5期597-610,共14页
Numerical solution of shallow-water equations (SWE) has been a challenging task because of its nonlinear hyperbolic nature, admitting discontinuous solution, and the need to satisfy the C-property. The presence of s... Numerical solution of shallow-water equations (SWE) has been a challenging task because of its nonlinear hyperbolic nature, admitting discontinuous solution, and the need to satisfy the C-property. The presence of source terms in momentum equations, such as the bottom slope and friction of bed, compounds the difficulties further. In this paper, a least-squares finite-element method for the space discretization and θ-method for the time integration is developed for the 2D non-conservative SWE including the source terms. Advantages of the method include: the source terms can be approximated easily with interpolation functions, no upwind scheme is needed, as well as the resulting system equations is symmetric and positive-definite, therefore, can be solved efficiently with the conjugate gradient method. The method is applied to steady and unsteady flows, subcritical and transcritical flow over a bump, 1D and 2D circular dam-break, wave past a circular cylinder, as well as wave past a hump. Computed results show good C-property, conservation property and compare well with exact solutions and other numerical results for flows with weak and mild gradient changes, but lead to inaccurate predictions for flows with strong gradient changes and discontinuities. 展开更多
关键词 Shallow-water equations Source terms least-squares finite-element method DAM-BREAK C-property
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Meshless Least-Squares Method for Solving the Steady-State Heat Conduction Equation 被引量:7
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作者 刘岩 张雄 陆明万 《Tsinghua Science and Technology》 SCIE EI CAS 2005年第1期61-66,共6页
The meshless weighted least-squares (MWLS) method is a pure meshless method that com- bines the moving least-squares approximation scheme and least-square discretization. Previous studies of the MWLS method for elas... The meshless weighted least-squares (MWLS) method is a pure meshless method that com- bines the moving least-squares approximation scheme and least-square discretization. Previous studies of the MWLS method for elastostatics and wave propagation problems have shown that the MWLS method possesses several advantages, such as high accuracy, high convergence rate, good stability, and high com- putational efficiency. In this paper, the MWLS method is extended to heat conduction problems. The MWLS computational parameters are chosen based on a thorough numerical study of 1-dimensional problems. Several 2-dimensional examples show that the MWLS method is much faster than the element free Galerkin method (EFGM), while the accuracy of the MWLS method is close to, or even better than the EFGM. These numerical results demonstrate that the MWLS method has good potential for numerical analyses of heat transfer problems. 展开更多
关键词 MESHLESS least-squares heat conduction STEADY-STATE
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A two-step weighted least-squares method for joint estimation of source and sensor locations: A general framework 被引量:9
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作者 Ding WANG Jiexin YIN +2 位作者 Tao TANG Ruirui LIU Zhidong WU 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 2019年第2期417-443,共27页
It is well known that the Two-step Weighted Least-Squares(TWLS) is a widely used method for source localization and sensor position refinement. For this reason, we propose a unified framework of the TWLS method for jo... It is well known that the Two-step Weighted Least-Squares(TWLS) is a widely used method for source localization and sensor position refinement. For this reason, we propose a unified framework of the TWLS method for joint estimation of multiple disjoint sources and sensor locations in this paper. Unlike some existing works, the presented method is based on more general measurement model, and therefore it can be applied to many different localization scenarios.Besides, it does not have the initialization and local convergence problem. The closed-form expression for the covariance matrix of the proposed TWLS estimator is also derived by exploiting the first-order perturbation analysis. Moreover, the estimation accuracy of the TWLS method is shown analytically to achieve the Cramér-Rao Bound(CRB) before the threshold effect takes place. The theoretical analysis is also performed in a common mathematical framework, rather than aiming at some specific signal metrics. Finally, two numerical experiments are performed to support the theoretical development in this paper. 展开更多
关键词 Cramér-Rao Bound(CRB) DISJOINT sources General framework Performance analysis Sensor position refinement SOURCE localization WEIGHTED least-squares
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Modelling of wind power forecasting errors based on kernel recursive least-squares method 被引量:6
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作者 Man XU Zongxiang LU +1 位作者 Ying QIAO Yong MIN 《Journal of Modern Power Systems and Clean Energy》 SCIE EI 2017年第5期735-745,共11页
Forecasting error amending is a universal solution to improve short-term wind power forecasting accuracy no matter what specific forecasting algorithms are applied. The error correction model should be presented consi... Forecasting error amending is a universal solution to improve short-term wind power forecasting accuracy no matter what specific forecasting algorithms are applied. The error correction model should be presented considering not only the nonlinear and non-stationary characteristics of forecasting errors but also the field application adaptability problems. The kernel recursive least-squares(KRLS) model is introduced to meet the requirements of online error correction. An iterative error modification approach is designed in this paper to yield the potential benefits of statistical models, including a set of error forecasting models. The teleconnection in forecasting errors from aggregated wind farms serves as the physical background to choose the hybrid regression variables. A case study based on field data is found to validate the properties of the proposed approach. The results show that our approach could effectively extend the modifying horizon of statistical models and has a better performance than the traditional linear method for amending short-term forecasts. 展开更多
关键词 Forecasting error amending Kernel recursive least-squares(KRLS) Spatial and temporal teleconnection Wind power forecast
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Drilling-based measuring method for the c-φ parameter of rock and its field application 被引量:1
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作者 Bei Jiang Fenglin Ma +5 位作者 Qi Wang Hongke Gao Dahu Zhai Yusong Deng Chuanjie Xu Liangdi Yao 《International Journal of Mining Science and Technology》 SCIE EI CAS CSCD 2024年第1期65-76,共12页
The technology of drilling tests makes it possible to obtain the strength parameter of rock accurately in situ. In this paper, a new rock cutting analysis model that considers the influence of the rock crushing zone(R... The technology of drilling tests makes it possible to obtain the strength parameter of rock accurately in situ. In this paper, a new rock cutting analysis model that considers the influence of the rock crushing zone(RCZ) is built. The formula for an ultimate cutting force is established based on the limit equilibrium principle. The relationship between digital drilling parameters(DDP) and the c-φ parameter(DDP-cφ formula, where c refers to the cohesion and φ refers to the internal friction angle) is derived, and the response of drilling parameters and cutting ratio to the strength parameters is analyzed. The drillingbased measuring method for the c-φ parameter of rock is constructed. The laboratory verification test is then completed, and the difference in results between the drilling test and the compression test is less than 6%. On this basis, in-situ rock drilling tests in a traffic tunnel and a coal mine roadway are carried out, and the strength parameters of the surrounding rock are effectively tested. The average difference ratio of the results is less than 11%, which verifies the effectiveness of the proposed method for obtaining the strength parameters based on digital drilling. This study provides methodological support for field testing of rock strength parameters. 展开更多
关键词 Digital drilling Rock crushing zone c-u parameter Measurement method Field application
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First-Order System Least-Squares Methods for a Flux Control Problem by the Stokes Flow
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作者 Soorok Ryu Sang Dong Kim Hyung-Chun Lee 《Communications in Computational Physics》 SCIE 2010年第4期738-758,共21页
This article deals with a first-order least-squares approach to the solution of an optimal control problem governed by Stokes equations.As with our earlier work on a velocity control by the Stokes flow in[S.Ryu,H.-C.L... This article deals with a first-order least-squares approach to the solution of an optimal control problem governed by Stokes equations.As with our earlier work on a velocity control by the Stokes flow in[S.Ryu,H.-C.Lee and S.D.Kim,SIAM J.Numer.Anal.,47(2009),pp.1524-1545],we recast the objective functional as a H1 seminorm in the velocity control term.By introducing a velocity-flux variable and using the Lagrange multiplier rule,a first-order optimality system is obtained.We show that the least-squares principle based on L2 norms applied to this system yields the optimal discretization error estimates for each variable in H1 norm,including the velocity flux.For numerical tests,multigrid method is employed to the discrete algebraic system,so that the velocity and flux controls are obtained. 展开更多
关键词 Optimal control OPTIMIZATION least-squares finite element methods Lagrange multiplier Stokes equations.
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Complex derivatives valuation: applying the Least-Squares Monte Carlo Simulation Method with several polynomial basis
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作者 Ursula Silveira Monteiro de Lima Carlos Patricio Samanez 《Financial Innovation》 2016年第1期1-14,共14页
Background:This article investigates the Least-Squares Monte Carlo Method by using different polynomial basis in American Asian Options pricing.The standard approach in the option pricing literature is to choose the b... Background:This article investigates the Least-Squares Monte Carlo Method by using different polynomial basis in American Asian Options pricing.The standard approach in the option pricing literature is to choose the basis arbitrarily.By comparing four different polynomial basis we show that the choice of basis interferes in the option's price.Methods:We assess Least-Squares Method performance in pricing four different American Asian Options by using four polynomial basis:Power,Laguerre,Legendre and Hermite A.To every American Asian Option priced,three sets of parameters are used in order to evaluate it properly.Results:We show that the choice of the basis interferes in the option's price by showing that one of them converges to the option's value faster than any other by using fewer simulated paths.In the case of an Amerasian call option,for example,we find that the preferable polynomial basis is Hermite A.For an Amerasian put option,the Power polynomial basis is recommended.Such empirical outcome is theoretically unpredictable,since in principle all basis can be indistinctly used when pricing the derivative.Conclusion:In this article The Least-Squares Monte Carlo Method performance is assessed in pricing four different types of American Asian Options by using four different polynomial basis through three different sets of parameters.Our results suggest that one polynomial basis is best suited to perform the method when pricing an American Asian option.Theoretically all basis can be indistinctly used when pricing the derivative.However,our results does not confirm these.We find that when pricing an American Asian put option,Power A is better than the other basis we have studied here whereas when pricing an American Asian call,Hermite A is better. 展开更多
关键词 Complex derivatives valuation least-squares Monte Carlo method Amerasian options Polynomial basis
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A comparison study on structure-function relationship of polysaccharides obtained from sea buckthorn berries using different methods:antioxidant and bile acid-binding capacity 被引量:1
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作者 Qiaoyun Li Zuman Dou +5 位作者 Qingfei Duan Chun Chen Ruihai Liu Yueming Jiang Bao Yang Xiong Fu 《Food Science and Human Wellness》 SCIE CSCD 2024年第1期494-505,共12页
In this study,the structural characters,antioxidant activities and bile acid-binding ability of sea buckthorn polysaccharides(HRPs)obtained by the commonly used hot water(HRP-W),pressurized hot water(HRP-H),ultrasonic... In this study,the structural characters,antioxidant activities and bile acid-binding ability of sea buckthorn polysaccharides(HRPs)obtained by the commonly used hot water(HRP-W),pressurized hot water(HRP-H),ultrasonic(HRP-U),acid(HRP-C)and alkali(HRP-A)assisted extraction methods were investigated.The results demonstrated that extraction methods had significant effects on extraction yield,monosaccharide composition,molecular weight,particle size,triple-helical structure,and surface morphology of HRPs except for the major linkage bands.Thermogravimetric analysis showed that HRP-U with filamentous reticular microstructure exhibited better thermal stability.The HRP-A with the lowest molecular weight and highest arabinose content possessed the best antioxidant activities.Moreover,the rheological analysis indicated that HRPs with higher galacturonic acid content and molecular weight showed higher viscosity and stronger crosslinking network(HRP-C,HRP-W and HRP-U),which exhibited stronger bile acid binding capacity.The present findings provide scientific evidence in the preparation technology of sea buckthorn polysaccharides with good antioxidant and bile acid binding capacity which are related to the structure affected by the extraction methods. 展开更多
关键词 Sea buckthorn Extraction method STRUCTURE Rheological properties Antioxidant activity Bile acid binding capacity
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Linearized waveform inversion for vertical transversely isotropic elastic media:Methodology and multi-parameter crosstalk analysis
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作者 Ke Chen Lu Liu +5 位作者 Li-Nan Xu Fei Hu Yuan Yang Jia-Hui Zuo Le-Le Zhang Yang Zhao 《Petroleum Science》 SCIE EI CAS CSCD 2024年第1期252-271,共20页
Seismic migration and inversion are closely related techniques to portray subsurface images and identify hydrocarbon reservoirs.Seismic migration aims at obtaining structural images of subsurface geologic discontinuit... Seismic migration and inversion are closely related techniques to portray subsurface images and identify hydrocarbon reservoirs.Seismic migration aims at obtaining structural images of subsurface geologic discontinuities.More specifically,seismic migration estimates the reflectivity function(stacked average reflectivity or pre-stack angle-dependent reflectivity)from seismic reflection data.On the other hand,seismic inversion quantitatively estimates the intrinsic rock properties of subsurface formulations.Such seismic inversion methods are applicable to detect hydrocarbon reservoirs that may exhibit lateral variations in the inverted parameters.Although there exist many differences,pre-stack seismic migration is similar with the first iteration of the general linearized seismic inversion.Usually,seismic migration and inversion techniques assume an acoustic or isotropic elastic medium.Unconventional reservoirs such as shale and tight sand formation have notable anisotropic property.We present a linearized waveform inversion(LWI)scheme for weakly anisotropic elastic media with vertical transversely isotropic(VTI)symmetry.It is based on two-way anisotropic elastic wave equation and simultaneously inverts for the localized perturbations(ΔVp_(0)/Vp_(0)/Vs_(0)/Vs_(0)/,Δ∈,Δδ)from the long-wavelength reference model.Our proposed VTI-elastic LWI is an iterative method that requires a forward and an adjoint operator acting on vectors in each iteration.We derive the forward Born approximation operator by perturbation theory and adjoint operator via adjoint-state method.The inversion has improved the quality of the images and reduces the multi-parameter crosstalk comparing with the adjoint-based images.We have observed that the multi-parameter crosstalk problem is more prominent in the inversion images for Thomsen anisotropy parameters.Especially,the Thomsen parameter is the most difficult to resolve.We also analyze the multi-parameter crosstalk using scattering radiation patterns.The linearized waveform inversion for VTI-elastic media presented in this article provides quantitative information of the rock properties that has the potential to help identify hydrocarbon reservoirs. 展开更多
关键词 Elastic ANISOTROPY least-squares imaging Waveform inversion Computational geophysics
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An Adaptive Least-Squares Mixed Finite Element Method for Fourth Order Parabolic Problems
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作者 Ning Chen Haiming Gu 《Applied Mathematics》 2013年第4期675-679,共5页
A least-squares mixed finite element (LSMFE) method for the numerical solution of fourth order parabolic problems analyzed and developed in this paper. The Ciarlet-Raviart mixed finite element space is used to approxi... A least-squares mixed finite element (LSMFE) method for the numerical solution of fourth order parabolic problems analyzed and developed in this paper. The Ciarlet-Raviart mixed finite element space is used to approximate. The a posteriori error estimator which is needed in the adaptive refinement algorithm is proposed. The local evaluation of the least-squares functional serves as a posteriori error estimator. The posteriori errors are effectively estimated. The convergence of the adaptive least-squares mixed finite element method is proved. 展开更多
关键词 ADAPTIVE method least-squares Mixed Finite Element method Fourth Order PARABOLIC Problems least-squares Functional A POSTERIORI Error
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LEAST-SQUARES MIXED FINITE ELEMENT METHOD FOR A CLASS OF STOKES EQUATION
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作者 顾海明 羊丹平 +1 位作者 隋树林 刘新民 《Applied Mathematics and Mechanics(English Edition)》 SCIE EI 2000年第5期557-566,共10页
A least-squares mixed finite element method was formulated for a class of Stokes equations in two dimensional domains. The steady state and the time-dependent Stokes' equations were considered. For the stationary ... A least-squares mixed finite element method was formulated for a class of Stokes equations in two dimensional domains. The steady state and the time-dependent Stokes' equations were considered. For the stationary equation, optimal H-t and L-2-error estimates are derived under the standard regularity assumption on the finite element partition ( the LBB-condition is not required). Far the evolutionary equation, optimal L-2 estimates are derived under the conventional Raviart-Thomas spaces. 展开更多
关键词 least-squares mixed finite element method error estimates
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Robustness Study and Superior Method Development and Validation for Analytical Assay Method of Atropine Sulfate in Pharmaceutical Ophthalmic Solution
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作者 Md. Nazmus Sakib Chowdhury Sreekanta Nath Dalal +4 位作者 Md. Ariful Islam Md. Anwar Hossain Pranab Kumar Das Shakawat Hossain Parajit Das 《American Journal of Analytical Chemistry》 CAS 2024年第5期151-164,共14页
Background: The robustness is a measurement of an analytical chemical method and its ability to contain unaffected by little with deliberate variation of analytical chemical method parameters. The analytical chemical ... Background: The robustness is a measurement of an analytical chemical method and its ability to contain unaffected by little with deliberate variation of analytical chemical method parameters. The analytical chemical method variation parameters are based on pH variability of buffer solution of mobile phase, organic ratio composition changes, stationary phase (column) manufacture, brand name and lot number variation;flow rate variation and temperature variation of chromatographic system. The analytical chemical method for assay of Atropine Sulfate conducted for robustness evaluation. The typical variation considered for mobile phase organic ratio change, change of pH, change of temperature, change of flow rate, change of column etc. Purpose: The aim of this study is to develop a cost effective, short run time and robust analytical chemical method for the assay quantification of Atropine in Pharmaceutical Ophthalmic Solution. This will help to make analytical decisions quickly for research and development scientists as well as will help with quality control product release for patient consumption. This analytical method will help to meet the market demand through quick quality control test of Atropine Ophthalmic Solution and it is very easy for maintaining (GDP) good documentation practices within the shortest period of time. Method: HPLC method has been selected for developing superior method to Compendial method. Both the compendial HPLC method and developed HPLC method was run into the same HPLC system to prove the superiority of developed method. Sensitivity, precision, reproducibility, accuracy parameters were considered for superiority of method. Mobile phase ratio change, pH of buffer solution, change of stationary phase temperature, change of flow rate and change of column were taken into consideration for robustness study of the developed method. Results: The limit of quantitation (LOQ) of developed method was much low than the compendial method. The % RSD for the six sample assay of developed method was 0.4% where the % RSD of the compendial method was 1.2%. The reproducibility between two analysts was 100.4% for developed method on the contrary the compendial method was 98.4%. 展开更多
关键词 ROBUSTNESS method Validation HPLC Compendial method method Development GDP LOQ
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Hybrid Strategy of Partitioned and Monolithic Methods for Solving Strongly Coupled Analysis of Inverse and Direct Piezoelectric and Circuit Coupling
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作者 Daisuke Ishihara Syunnosuke Nozaki +1 位作者 Tomoya Niho Naoto Takayama 《Computer Modeling in Engineering & Sciences》 SCIE EI 2024年第8期1371-1386,共16页
The inverse and direct piezoelectric and circuit coupling are widely observed in advanced electro-mechanical systems such as piezoelectric energy harvesters.Existing strongly coupled analysis methods based on direct n... The inverse and direct piezoelectric and circuit coupling are widely observed in advanced electro-mechanical systems such as piezoelectric energy harvesters.Existing strongly coupled analysis methods based on direct numerical modeling for this phenomenon can be classified into partitioned or monolithic formulations.Each formulation has its advantages and disadvantages,and the choice depends on the characteristics of each coupled problem.This study proposes a new option:a coupled analysis strategy that combines the best features of the existing formulations,namely,the hybrid partitioned-monolithic method.The analysis of inverse piezoelectricity and the monolithic analysis of direct piezoelectric and circuit interaction are strongly coupled using a partitioned iterative hierarchical algorithm.In a typical benchmark problem of a piezoelectric energy harvester,this research compares the results from the proposed method to those from the conventional strongly coupled partitioned iterative method,discussing the accuracy,stability,and computational cost.The proposed hybrid concept is effective for coupled multi-physics problems,including various coupling conditions. 展开更多
关键词 Structure-piezoelectric-circuit interaction energy harvesting partitioned method monolithic method hybrid method
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