[Objectives]The paper was to establish an ultra high performance liquid chromatography-quadrupole/linear ion trap complex mass spectrometry for the determination of 10 kinds ofα2-receptor agonists in animal derived f...[Objectives]The paper was to establish an ultra high performance liquid chromatography-quadrupole/linear ion trap complex mass spectrometry for the determination of 10 kinds ofα2-receptor agonists in animal derived food.[Methods]The samples were extracted with sodium carbonate buffer solution and ethyl acetate,and analyzed by mass spectrometry after solid phase extraction and high performance liquid chromatography separation.[Results]Ten kinds ofα2-receptor agonists showed a good linear relationship in the range of 1-100μg/mL,with the average recovery of over 69%and the relative standard deviation less than 8.32%.The detection limit of 10 kinds of α_(2)-receptor agonists was up to 1μg/kg.[Conclusions]The method has good selectivity and strong anti-interference ability,and can meet the requirements of 10 kinds ofα2-receptor agonists residues in animal derived food.展开更多
Control systems designed by the principle of matching gives rise to problems of evaluating the peak output. This paper proposes a practical method for computing the peak output of linear time-invariant and non-anticip...Control systems designed by the principle of matching gives rise to problems of evaluating the peak output. This paper proposes a practical method for computing the peak output of linear time-invariant and non-anticipative systems for a class of possible sets that are characterized with many bounding conditions on the two- and/or the infinity-norms of the inputs and their derivatives. The original infinite-dimensional convex optimization problem is approximated as a large-scale convex programme defined in a Euclidean space, which are associated with sparse matrices and thus can be solved efficiently in practice. The numerical results show that the method performs satisfactorily, and that using a possible set with many bounding conditions can help to reduce the design conservatism and thereby yield a better match.展开更多
基金Supported by Scientific Research Project of Dalian Customs(2022DK09).
文摘[Objectives]The paper was to establish an ultra high performance liquid chromatography-quadrupole/linear ion trap complex mass spectrometry for the determination of 10 kinds ofα2-receptor agonists in animal derived food.[Methods]The samples were extracted with sodium carbonate buffer solution and ethyl acetate,and analyzed by mass spectrometry after solid phase extraction and high performance liquid chromatography separation.[Results]Ten kinds ofα2-receptor agonists showed a good linear relationship in the range of 1-100μg/mL,with the average recovery of over 69%and the relative standard deviation less than 8.32%.The detection limit of 10 kinds of α_(2)-receptor agonists was up to 1μg/kg.[Conclusions]The method has good selectivity and strong anti-interference ability,and can meet the requirements of 10 kinds ofα2-receptor agonists residues in animal derived food.
文摘Control systems designed by the principle of matching gives rise to problems of evaluating the peak output. This paper proposes a practical method for computing the peak output of linear time-invariant and non-anticipative systems for a class of possible sets that are characterized with many bounding conditions on the two- and/or the infinity-norms of the inputs and their derivatives. The original infinite-dimensional convex optimization problem is approximated as a large-scale convex programme defined in a Euclidean space, which are associated with sparse matrices and thus can be solved efficiently in practice. The numerical results show that the method performs satisfactorily, and that using a possible set with many bounding conditions can help to reduce the design conservatism and thereby yield a better match.
