Transient creep at very low strain rates (less than 10-10 s-1) is still unclear. The traditional uniaxial creep testing is less useful due to unsatisfied resolution strain (~10-6). To study transient creep behavio...Transient creep at very low strain rates (less than 10-10 s-1) is still unclear. The traditional uniaxial creep testing is less useful due to unsatisfied resolution strain (~10-6). To study transient creep behavior at such low strain rates, a high-resolution strain measurement using the helicoid spring specimen technique was employed in a fine-grained Al-5356 alloy at temperatures ranging from 0.47Tm to 0.74Tm (Tm: melting point). To clarify transient creep mechanism at such low strain rates, transmission electron microscopy (TEM) was used in microstructure observation of crept specimens. The abnormal transient creep, high temperature strengthening at T〉Tp (Tp: the phase transformation temperature, 0.58Tm) or intermediate temperature softening at 0.4Tm〈T£Tp and double-normal type (creep curves including double work-hardening stages) at T=Tp, were firstly observed. The substructure observation in a crept specimen at T=0.58Tm and e=1×10-4 shows pile-up dislocations including many small jogs with equal interval, and dislocations emitted from grain boundaries. The b-Al3Mg2 phase dissolves under the condition of testing temperatures higher than 523 K, which causes solid-solution quantity of Mg atoms to increase. Therefore, the “abnormal transient creep” may be related to the difference of solid solution strengthening caused by phase change during the creep tests.展开更多
Stress waves propagate along vertical,radial and circumferential directions when a non-uniformly distributed load is applied at one end of a three-dimensional shaft.As a result,the receiving signals are usually mixed ...Stress waves propagate along vertical,radial and circumferential directions when a non-uniformly distributed load is applied at one end of a three-dimensional shaft.As a result,the receiving signals are usually mixed with undesired interference components,often featuring as high-frequency fluctuations.Previous studies have revealed that sectional geometry(shape and size)greatly affects the high-frequency interference.In this study,low strain dynamic testing on full-scale X-section concrete is conducted in order to investigate the influences of high-frequency interference on velocity responses at the pile head.Emphasis is placed on the frequency and peak value of interference waves at various receiving points.Additionally,the effects of the geometrical,and mechanical properties of the pile shaft on high-frequency interference are elaborated on through the three-dimensional finite element method.The results show that the measured wave is obscured by interference waves superposed by two types of high-frequency components.The modulus and cross-sectional area are contributing factors to the frequency and peak value of the interference waves.On the other hand,the position with the least interference is determined,to some extent,by the accurate shape of the X-section.展开更多
Instantaneous creep in face-centered cubic metals, 5N Al(99.999%), 2N Al (99%) and 4N Cu (99.99%) with different grain sizes, was firstly investigated by sudden stress-change experiments at ultra- low strain rat...Instantaneous creep in face-centered cubic metals, 5N Al(99.999%), 2N Al (99%) and 4N Cu (99.99%) with different grain sizes, was firstly investigated by sudden stress-change experiments at ultra- low strain rates ε ≤10-10 s-1 and temperature T 〈 0.32 Tn. The experimental results indicate that the observed instantaneous creep is strongly dependent on grain size, the concentration of impurity, and stacking fault energy. Creep in high-purity aluminum, 5N Al, with a very large grain size, d 〉 1600μm, shows non-viscous behavior, and is controlled by the recovery of dislocations in the boundary of dislocation cells. On the other hand, for 5N A1 with a small grain size, d=30μm, and low-purity aluminum, 2N A1, with d8= 25μm, creep shows viscous behavior and may be related to 'low temperature grain boundary sliding'. For high-purity copper, 4N Cu, with d= 40 grn and lower stacking fault energy, creep shows a non-viscous behavior, and is controlled by the recovery process of dislocations. For all of the samples, creep shows anelastic behavior.展开更多
The high-frequency interference exists obviously in low strain integrity testing of large-diameter pipe pile when a transientpoint load is applied. An analytical solution of vertical vibratory response of large-diamet...The high-frequency interference exists obviously in low strain integrity testing of large-diameter pipe pile when a transientpoint load is applied. An analytical solution of vertical vibratory response of large-diameter pipe piles in low strain testing isdeduced in this paper. The analytical solution is verified by both numerical simulation and model test results. The time-domainvelocity responses on pile top are analyzed. The calculation results indicate that the time-domain responses at various pointssuffer different high-frequency interferences, thus the peak values and phases of different points are different. The influence ofvibratory modes on high-frequency interference is analyzed. It is found that the high-frequency interference at 90° point main-ly derives from the second flexural mode, but for other points it mainly originates from the first flexural mode. The factors af-fecting the frequency and peak value of interference waves have been investigated in this study. The results indicate that thelarger radius angle between the receiving and 90° points leads to greater peak value of high frequency wave crest. The leasthigh-frequency interference is detected at the angle of 90°. The frequency of interference waves is decreased with the increaseof pile radius, while the peak value is almost constant. The frequency is also related to pile modulus, i.e. the larger pile modu-lus results in greater frequency. The peak value varies with impulse width and soil resistance, i.e., the wider impulse width andlarger soil resistance cause smaller peak value. In conclusion, the frequency of interference waves is dependent on the geomet-rical and mechanics characteristics of the piles such as pile radius and modulus, but independent of the external conditionssuch as impulse width and soil resistance. On the other hand, the peak value of interference waves is mainly dependent on theexternal conditions but independent of the geometrical and mechanics characteristics of the piles. In practice, some externalmeasures should be adopted to weaken high-frequency interference such as using soft hammer, hammer cushion and adoptingsuitable receiving point.展开更多
KVPO_(4)F with excellent structural stability and high operating voltage has been identified as a promising cathode for potassium-ion batteries(PIBs),but limits in sluggish ion transport and severe volume change cause...KVPO_(4)F with excellent structural stability and high operating voltage has been identified as a promising cathode for potassium-ion batteries(PIBs),but limits in sluggish ion transport and severe volume change cause insufficient potassium storage capability.Here,a high-energy and low-strain KVPO_(4)F composite cathode assisted by multifunctional K_(2)C_(4)O_(4)electrode stabilizer is exquisitely designed.Systematical electrochemical investigations demonstrate that this composite cathode can deliver a remarkable energy density up to 530 Wh kg^(-1)with 142.7 mAh g^(-1)of reversible capacity at 25 mA g^(-1),outstanding rate capability of 70.6 mAh g^(-1)at 1000 mA g^(-1),and decent cycling stability.Furthermore,slight volume change(~5%)and increased interfacial stability with thin and even cathode-electrolyte interphase can be observed through in situ and ex situ characterizations,which are attributed to the synergistic effect from in situ potassium compensation and carbon deposition through self-sacrificing K_(2)C_(4)O_(4)additive.Moreover,potassium-ion full cells manifest significant improvement in energy density and cycling stability.This work demonstrates a positive impact of K_(2)C_(4)O_(4)additive on the comprehensive electrochemical enhancement,especially the activation of high-voltage plateau capacity and provides an efficient strategy to enlighten the design of other high-voltage cathodes for advanced high-energy batteries.展开更多
The effect of ultraviolet mutagenesis on a heterotrophic strain(Providencia JAT-1) mutation was studied and bioleaching of low grade copper ore with mutant bacteria was investigated. The results show that the activity...The effect of ultraviolet mutagenesis on a heterotrophic strain(Providencia JAT-1) mutation was studied and bioleaching of low grade copper ore with mutant bacteria was investigated. The results show that the activity of bacteria was improved after ultraviolet mutagenesis; the best irradiation time was 120 s. Compared to the original bacteria, the cells density of mutant bacteria at stationary phase increased by 26% and ammonia produced by mutant bacteria increased by 12%. Higher activity of bacteria leads to a higher copper extraction rate. The bioleaching performance of Providencia JAT-1 was improved after UV mutagenesis. The copper extraction rate with mutant bacteria increased by 10.6% compared to the original bacteria. The ore surface was corroded and the fine particles were absent after bioleaching. Free copper oxide and copper silicates could be leached out easily by using JAT-1; a small part of the copper sulfide can also be leached out. Bioleaching using JAT-1 is more effective than ammonia leaching and copper extraction rate with mutant bacteria was 21.1% higher than that by ammonia leaching under the same condition.展开更多
Studies were made of the symmetric tensile-compressive low cycle fatigue behaviour and the influence of dynamic strain aging(DSA)pre-treatment of 18-8 austenitic stainless steel. Within the testing amplitude range of ...Studies were made of the symmetric tensile-compressive low cycle fatigue behaviour and the influence of dynamic strain aging(DSA)pre-treatment of 18-8 austenitic stainless steel. Within the testing amplitude range of strain.±0.5 % to±1.5 %,the three processes of cyclic hardening,cyclic saturation and cyclic softening were observed.In the same amplitude of strain,the peak stress of the samples pre-treated by DSA is higher than that of solid-solu- tion and cold working pre-treatment,but no remarkable differences of the fatigue lives of them were found.TEM observation shows that the uniform and stable dislocation networks with high density form after DSA pre-treatment,which increases the cyclic peak stress.The cyclic softening results from the low dislocation density and elongated cell structure with low energy.展开更多
Grain refinement is one of the effective methods to develop new generation low carbon microalloyed steels possessing excellent combination of mechanical properties. The microstructural evolution and ferrite grain refi...Grain refinement is one of the effective methods to develop new generation low carbon microalloyed steels possessing excellent combination of mechanical properties. The microstructural evolution and ferrite grain refinement at the deformation temperature of 865℃, above Ar3, with different strain rates were investigated using single pass isothermal hot compression experiments for a low carbon Nb-Ti microalloyed steel. The physical processes that occurred during deformation were discussed by observing the optical microstructure and analyzing the true stress-true strain responses. At strain rates of 0.001 and 0.01s^-1, there is no evidence of work hardening behavior during hot deformation and strain-induced transformation (SIT) leads to dynamic flow softening in flow curves. Optical microscopy observation shows that ultrafine and equiaxed ferrite with grain sizes of 2μm can be obtained by applying deformation with strain rate of 0.1 s^-1 due to SIT just after deformation. Furthermore, increasing the strain rate from 0.001 to 0.1 s^-1 reduces both the grain size of the equiaxed ferrite and the amount of deformed ferrite.展开更多
The strain-induced ferrite formed under different conditions was observed with SEM and optical microscope.The nucleation sites of strain-induced ferrite include grain boundary,grain inside,deformed band and annealing ...The strain-induced ferrite formed under different conditions was observed with SEM and optical microscope.The nucleation sites of strain-induced ferrite include grain boundary,grain inside,deformed band and annealing twin boundary.The shapes of the ferrite accordingly are equiaxed irregular polygonal,strip-shaped and acicular.展开更多
In this work, a parametric approach is presented and utilized to determine the creep properties of weldments; then the model of creep strain for cross weld specimen is given. On the basis of the experimental results, ...In this work, a parametric approach is presented and utilized to determine the creep properties of weldments; then the model of creep strain for cross weld specimen is given. On the basis of the experimental results, attempt has been made to establish equations of the isochronous stress-strain for weld joint that can predict the function of loading and service time in use of the creep data of base metal and weld metal.展开更多
A series of tests of deformation-induced ferrite transformation (DIP-T) in a low carbon steel were carried out by the Gleeble-3500 hot simulation machine at a temperature range of Ae3-Ar3. The overall stress-strain ...A series of tests of deformation-induced ferrite transformation (DIP-T) in a low carbon steel were carried out by the Gleeble-3500 hot simulation machine at a temperature range of Ae3-Ar3. The overall stress-strain curves during DIFT can be divided into three typical types: "double-humped"," single-humped" and "transitional". The peaks exhibited in the curve are involved with deformation-induced transformation which happened in grains or at the grain boundaries. According to the stress-time curve and strain-time curve, strain capacity dramatically postponed the strain-induced transformation, which leads to the start of the transformation right ahead of the finish of deformation and the majority of the ferrite transformation process mainly happened after the deformation. Deformation-induced transformation is a metadynamic transformation process with dynamic nucleation.展开更多
The dynamic recrystallization and static recrystallization in a low carbon steel were investigated through single-pass and double-pass experiments. The results indicate that as the deformation temperature increases an...The dynamic recrystallization and static recrystallization in a low carbon steel were investigated through single-pass and double-pass experiments. The results indicate that as the deformation temperature increases and the strain rate decreases, the shape of the stress-strain curve is changed from dynamic recovery shape to dynamic recrystallization shape. The austenite could not recrystallize within a few seconds after deformation at temperature below 900 ℃. According to the change in microstructure during deformation, the controlled rolling of low carbon steel can be divided into four stages: dynamic recrystallization, dynamic recovery, strain-induced ferrite transformation, and rolling in two-phase region. According to the microstructure after deformation, the controlled rolling of low carbon steel can be divided into five regions: non-recrystallized austenite, partly-recrystallized austenite, fully-recrystallized austenite, austenite to ferrite transformation, and dual phase.展开更多
The cyclic stress-strain responses (CSSR), Neuber's rule (NR) and cyclic strain-life relation (CSLR) are treated as probabilistic curves in local stress and strain method of low cycle fatigue analysis. The randomn...The cyclic stress-strain responses (CSSR), Neuber's rule (NR) and cyclic strain-life relation (CSLR) are treated as probabilistic curves in local stress and strain method of low cycle fatigue analysis. The randomness of loading and the theory of fatigue damage accumulation (TOFDA) are considered. The probabilistic analysis of local stress, local strain and fatigue life are constructed based on the first-order Taylor's series expansions. Through this method proposed fatigue reliability analysis can be accomplished.展开更多
For a study of the movement and deformation of coal-rock mass and low protected seams below a stope,as well as for fracture developments and rules of evolution of permeability,we designed a plane strain model test sta...For a study of the movement and deformation of coal-rock mass and low protected seams below a stope,as well as for fracture developments and rules of evolution of permeability,we designed a plane strain model test stand to carry out model tests of similar materials in order to improve the effect of gas drainage from low protected seams and to measure the movement and deformation of coal-rock mass using a method of non-contact close-range photogrammetry.Our results show that 1) using paraffin melting to take the place of coal seam mining can satisfy the mining conditions of a protective seam;2) coal-rock mass under goafs has an upward movement after the protective seam has been mined,causing floor heaving;3) low protected seams become swollen and deformed,providing a good pressure-relief effect and causing the coal-rock mass under both sides of coal pillars to become deformed by compression and 4) the evolution of permeability of low protected seams follows the way of initial values→a slight decrease→a great increase→stability→final decrease.Simultaneously,the coefficient of air permeability increased at a decreasing rate with an increase in interlayer spacing.展开更多
Photoluminescence(PL) and Raman spectra under uniaxial strain were measured in mono- and bi-layer MoSe;to comparatively investigate the evolution of excitonic gaps and Raman phonons with strain. We observed that the...Photoluminescence(PL) and Raman spectra under uniaxial strain were measured in mono- and bi-layer MoSe;to comparatively investigate the evolution of excitonic gaps and Raman phonons with strain. We observed that the strain dependence of excitonic gaps shows a nearly linear behavior in both flakes. One percent of strain increase gives a reduction of;2 meV(;5 me V) in A-exciton gap in monolayer(bilayer) MoSe;. The PL width remains little changed in monolayer MoSe;while it increases rapidly with strain in the bilayer case. We have made detailed discussions on the observed strain-modulated results and compared the difference between monolayer and bilayer cases. The hybridization between 4d orbits of Mo and 4p orbits of Se, which is controlled by the Se–Mo–Se bond angle under strain, can be employed to consistently explain the observations. The study may shed light into exciton physics in few-layer MoSe;and provides a basis for their applications.展开更多
To increase the detectability of split Hopkinson pressure bar (SHPB) of low-impedance materials, modifications were conducted on traditional SHPB apparatus with a PMMA tube to output transmitted signal, and weak sig...To increase the detectability of split Hopkinson pressure bar (SHPB) of low-impedance materials, modifications were conducted on traditional SHPB apparatus with a PMMA tube to output transmitted signal, and weak signals were further amplified by semiconductor strain gauges. Experiments on soft rubbers and cushioning foam materials were carried out. In order to analyze the accuracy of the experimental results, the stress equilibrium issues involved in the assumptions of SHPB were investigated. First, by way of re-constructing loading process of incident wave, the stress- strain curve was obtained, along with the stress equilibrium ratio of specimen. Secondly, the influences on the accuracy of stress-strain curves were investigated through the elastic modulus comparisons. And the results illustrate that the bilinear incident wave from experiments can ensure the stress equilibrium deformation of specimen after 2 normalized times, much sooner than ramp incident waves. Moreover, it even facilitates specimen deformation with a constant strain rate. The results confirm that the detectability of the modified SHPB can be down to tens kPa with enough accuracy level.展开更多
基金Project(12JCYBJC32100)supported by Tianjin Research Program of Application Foundation and Advanced Technologyin part by Grants-in-Aid from the Japan Society for the Promotion of Science(JSPS)
文摘Transient creep at very low strain rates (less than 10-10 s-1) is still unclear. The traditional uniaxial creep testing is less useful due to unsatisfied resolution strain (~10-6). To study transient creep behavior at such low strain rates, a high-resolution strain measurement using the helicoid spring specimen technique was employed in a fine-grained Al-5356 alloy at temperatures ranging from 0.47Tm to 0.74Tm (Tm: melting point). To clarify transient creep mechanism at such low strain rates, transmission electron microscopy (TEM) was used in microstructure observation of crept specimens. The abnormal transient creep, high temperature strengthening at T〉Tp (Tp: the phase transformation temperature, 0.58Tm) or intermediate temperature softening at 0.4Tm〈T£Tp and double-normal type (creep curves including double work-hardening stages) at T=Tp, were firstly observed. The substructure observation in a crept specimen at T=0.58Tm and e=1×10-4 shows pile-up dislocations including many small jogs with equal interval, and dislocations emitted from grain boundaries. The b-Al3Mg2 phase dissolves under the condition of testing temperatures higher than 523 K, which causes solid-solution quantity of Mg atoms to increase. Therefore, the “abnormal transient creep” may be related to the difference of solid solution strengthening caused by phase change during the creep tests.
基金National Natural Science Foundation of China under Grant Nos.51622803 and 51878103China Postdoctoral Science Foundation under Grant No.2021M692689。
文摘Stress waves propagate along vertical,radial and circumferential directions when a non-uniformly distributed load is applied at one end of a three-dimensional shaft.As a result,the receiving signals are usually mixed with undesired interference components,often featuring as high-frequency fluctuations.Previous studies have revealed that sectional geometry(shape and size)greatly affects the high-frequency interference.In this study,low strain dynamic testing on full-scale X-section concrete is conducted in order to investigate the influences of high-frequency interference on velocity responses at the pile head.Emphasis is placed on the frequency and peak value of interference waves at various receiving points.Additionally,the effects of the geometrical,and mechanical properties of the pile shaft on high-frequency interference are elaborated on through the three-dimensional finite element method.The results show that the measured wave is obscured by interference waves superposed by two types of high-frequency components.The modulus and cross-sectional area are contributing factors to the frequency and peak value of the interference waves.On the other hand,the position with the least interference is determined,to some extent,by the accurate shape of the X-section.
基金Funded by the Tianjin Research Program of Application Foundation and Advanced Technology(12JCYBJC32100)the Scientific Research Foundation for the Returned Overseas Chinese Scholars,State Education Ministryin part by Grants-in-Aid from the Japan Society for the Promotion of Science(JSPS)
文摘Instantaneous creep in face-centered cubic metals, 5N Al(99.999%), 2N Al (99%) and 4N Cu (99.99%) with different grain sizes, was firstly investigated by sudden stress-change experiments at ultra- low strain rates ε ≤10-10 s-1 and temperature T 〈 0.32 Tn. The experimental results indicate that the observed instantaneous creep is strongly dependent on grain size, the concentration of impurity, and stacking fault energy. Creep in high-purity aluminum, 5N Al, with a very large grain size, d 〉 1600μm, shows non-viscous behavior, and is controlled by the recovery of dislocations in the boundary of dislocation cells. On the other hand, for 5N A1 with a small grain size, d=30μm, and low-purity aluminum, 2N A1, with d8= 25μm, creep shows viscous behavior and may be related to 'low temperature grain boundary sliding'. For high-purity copper, 4N Cu, with d= 40 grn and lower stacking fault energy, creep shows a non-viscous behavior, and is controlled by the recovery process of dislocations. For all of the samples, creep shows anelastic behavior.
基金supported by the National Natural Science Foundation of China(Grant No.51008115)the Provincial Science Foundation of Jiangsu(Grant No.BK2008040)
文摘The high-frequency interference exists obviously in low strain integrity testing of large-diameter pipe pile when a transientpoint load is applied. An analytical solution of vertical vibratory response of large-diameter pipe piles in low strain testing isdeduced in this paper. The analytical solution is verified by both numerical simulation and model test results. The time-domainvelocity responses on pile top are analyzed. The calculation results indicate that the time-domain responses at various pointssuffer different high-frequency interferences, thus the peak values and phases of different points are different. The influence ofvibratory modes on high-frequency interference is analyzed. It is found that the high-frequency interference at 90° point main-ly derives from the second flexural mode, but for other points it mainly originates from the first flexural mode. The factors af-fecting the frequency and peak value of interference waves have been investigated in this study. The results indicate that thelarger radius angle between the receiving and 90° points leads to greater peak value of high frequency wave crest. The leasthigh-frequency interference is detected at the angle of 90°. The frequency of interference waves is decreased with the increaseof pile radius, while the peak value is almost constant. The frequency is also related to pile modulus, i.e. the larger pile modu-lus results in greater frequency. The peak value varies with impulse width and soil resistance, i.e., the wider impulse width andlarger soil resistance cause smaller peak value. In conclusion, the frequency of interference waves is dependent on the geomet-rical and mechanics characteristics of the piles such as pile radius and modulus, but independent of the external conditionssuch as impulse width and soil resistance. On the other hand, the peak value of interference waves is mainly dependent on theexternal conditions but independent of the geometrical and mechanics characteristics of the piles. In practice, some externalmeasures should be adopted to weaken high-frequency interference such as using soft hammer, hammer cushion and adoptingsuitable receiving point.
基金the financial support from the National Key R&D Program of China(Grant No.2023YFE0202000)the National Natural Science Foundation of China(Grant No.52102213)+1 种基金Natural Science Foundation of Jilin Province(Grant No.20230101128JC)Double-Thousand Talents Plan of Jiangxi Province(jxsq2023102005)
文摘KVPO_(4)F with excellent structural stability and high operating voltage has been identified as a promising cathode for potassium-ion batteries(PIBs),but limits in sluggish ion transport and severe volume change cause insufficient potassium storage capability.Here,a high-energy and low-strain KVPO_(4)F composite cathode assisted by multifunctional K_(2)C_(4)O_(4)electrode stabilizer is exquisitely designed.Systematical electrochemical investigations demonstrate that this composite cathode can deliver a remarkable energy density up to 530 Wh kg^(-1)with 142.7 mAh g^(-1)of reversible capacity at 25 mA g^(-1),outstanding rate capability of 70.6 mAh g^(-1)at 1000 mA g^(-1),and decent cycling stability.Furthermore,slight volume change(~5%)and increased interfacial stability with thin and even cathode-electrolyte interphase can be observed through in situ and ex situ characterizations,which are attributed to the synergistic effect from in situ potassium compensation and carbon deposition through self-sacrificing K_(2)C_(4)O_(4)additive.Moreover,potassium-ion full cells manifest significant improvement in energy density and cycling stability.This work demonstrates a positive impact of K_(2)C_(4)O_(4)additive on the comprehensive electrochemical enhancement,especially the activation of high-voltage plateau capacity and provides an efficient strategy to enlighten the design of other high-voltage cathodes for advanced high-energy batteries.
基金Project(2012BAB08B02)supported by the National Key Technologies R&D Program for the 12th Five-year Plan,ChinaProjects(51304011,51374035)supported by the National Natural Science Foundation of China
文摘The effect of ultraviolet mutagenesis on a heterotrophic strain(Providencia JAT-1) mutation was studied and bioleaching of low grade copper ore with mutant bacteria was investigated. The results show that the activity of bacteria was improved after ultraviolet mutagenesis; the best irradiation time was 120 s. Compared to the original bacteria, the cells density of mutant bacteria at stationary phase increased by 26% and ammonia produced by mutant bacteria increased by 12%. Higher activity of bacteria leads to a higher copper extraction rate. The bioleaching performance of Providencia JAT-1 was improved after UV mutagenesis. The copper extraction rate with mutant bacteria increased by 10.6% compared to the original bacteria. The ore surface was corroded and the fine particles were absent after bioleaching. Free copper oxide and copper silicates could be leached out easily by using JAT-1; a small part of the copper sulfide can also be leached out. Bioleaching using JAT-1 is more effective than ammonia leaching and copper extraction rate with mutant bacteria was 21.1% higher than that by ammonia leaching under the same condition.
文摘Studies were made of the symmetric tensile-compressive low cycle fatigue behaviour and the influence of dynamic strain aging(DSA)pre-treatment of 18-8 austenitic stainless steel. Within the testing amplitude range of strain.±0.5 % to±1.5 %,the three processes of cyclic hardening,cyclic saturation and cyclic softening were observed.In the same amplitude of strain,the peak stress of the samples pre-treated by DSA is higher than that of solid-solu- tion and cold working pre-treatment,but no remarkable differences of the fatigue lives of them were found.TEM observation shows that the uniform and stable dislocation networks with high density form after DSA pre-treatment,which increases the cyclic peak stress.The cyclic softening results from the low dislocation density and elongated cell structure with low energy.
文摘Grain refinement is one of the effective methods to develop new generation low carbon microalloyed steels possessing excellent combination of mechanical properties. The microstructural evolution and ferrite grain refinement at the deformation temperature of 865℃, above Ar3, with different strain rates were investigated using single pass isothermal hot compression experiments for a low carbon Nb-Ti microalloyed steel. The physical processes that occurred during deformation were discussed by observing the optical microstructure and analyzing the true stress-true strain responses. At strain rates of 0.001 and 0.01s^-1, there is no evidence of work hardening behavior during hot deformation and strain-induced transformation (SIT) leads to dynamic flow softening in flow curves. Optical microscopy observation shows that ultrafine and equiaxed ferrite with grain sizes of 2μm can be obtained by applying deformation with strain rate of 0.1 s^-1 due to SIT just after deformation. Furthermore, increasing the strain rate from 0.001 to 0.1 s^-1 reduces both the grain size of the equiaxed ferrite and the amount of deformed ferrite.
文摘The strain-induced ferrite formed under different conditions was observed with SEM and optical microscope.The nucleation sites of strain-induced ferrite include grain boundary,grain inside,deformed band and annealing twin boundary.The shapes of the ferrite accordingly are equiaxed irregular polygonal,strip-shaped and acicular.
基金supports provided by Natural Science Foundation of Shanghai(contract No.03ZR14022)the“Tenth Five”National Key Technological Research and Development Program(contract No.2001BA803B03)National Natural Science Foundation of China(contract No.50225517)are gratefully acknowledged.
文摘In this work, a parametric approach is presented and utilized to determine the creep properties of weldments; then the model of creep strain for cross weld specimen is given. On the basis of the experimental results, attempt has been made to establish equations of the isochronous stress-strain for weld joint that can predict the function of loading and service time in use of the creep data of base metal and weld metal.
文摘A series of tests of deformation-induced ferrite transformation (DIP-T) in a low carbon steel were carried out by the Gleeble-3500 hot simulation machine at a temperature range of Ae3-Ar3. The overall stress-strain curves during DIFT can be divided into three typical types: "double-humped"," single-humped" and "transitional". The peaks exhibited in the curve are involved with deformation-induced transformation which happened in grains or at the grain boundaries. According to the stress-time curve and strain-time curve, strain capacity dramatically postponed the strain-induced transformation, which leads to the start of the transformation right ahead of the finish of deformation and the majority of the ferrite transformation process mainly happened after the deformation. Deformation-induced transformation is a metadynamic transformation process with dynamic nucleation.
基金Item Sponsored by High Technology Development Programof China (2001AA332020) and National Natural ScienceFoundation of China (50271015)
文摘The dynamic recrystallization and static recrystallization in a low carbon steel were investigated through single-pass and double-pass experiments. The results indicate that as the deformation temperature increases and the strain rate decreases, the shape of the stress-strain curve is changed from dynamic recovery shape to dynamic recrystallization shape. The austenite could not recrystallize within a few seconds after deformation at temperature below 900 ℃. According to the change in microstructure during deformation, the controlled rolling of low carbon steel can be divided into four stages: dynamic recrystallization, dynamic recovery, strain-induced ferrite transformation, and rolling in two-phase region. According to the microstructure after deformation, the controlled rolling of low carbon steel can be divided into five regions: non-recrystallized austenite, partly-recrystallized austenite, fully-recrystallized austenite, austenite to ferrite transformation, and dual phase.
文摘The cyclic stress-strain responses (CSSR), Neuber's rule (NR) and cyclic strain-life relation (CSLR) are treated as probabilistic curves in local stress and strain method of low cycle fatigue analysis. The randomness of loading and the theory of fatigue damage accumulation (TOFDA) are considered. The probabilistic analysis of local stress, local strain and fatigue life are constructed based on the first-order Taylor's series expansions. Through this method proposed fatigue reliability analysis can be accomplished.
基金the Major Programs of the National Basic Research Program of China (No.2005CB221503)the National Natural Science Foundation of China (Nos. 70533050 and 50674089) for their support of this project
文摘For a study of the movement and deformation of coal-rock mass and low protected seams below a stope,as well as for fracture developments and rules of evolution of permeability,we designed a plane strain model test stand to carry out model tests of similar materials in order to improve the effect of gas drainage from low protected seams and to measure the movement and deformation of coal-rock mass using a method of non-contact close-range photogrammetry.Our results show that 1) using paraffin melting to take the place of coal seam mining can satisfy the mining conditions of a protective seam;2) coal-rock mass under goafs has an upward movement after the protective seam has been mined,causing floor heaving;3) low protected seams become swollen and deformed,providing a good pressure-relief effect and causing the coal-rock mass under both sides of coal pillars to become deformed by compression and 4) the evolution of permeability of low protected seams follows the way of initial values→a slight decrease→a great increase→stability→final decrease.Simultaneously,the coefficient of air permeability increased at a decreasing rate with an increase in interlayer spacing.
基金supported by the National Basic Research Program of China(Grant No.2012CB921701)the National Natural Science Foundation of China(Grant Nos.11474357 and 11004245)supported by the Fundamental Research Funds for the Central Universities of China and the Research Funds of Renmin University of China
文摘Photoluminescence(PL) and Raman spectra under uniaxial strain were measured in mono- and bi-layer MoSe;to comparatively investigate the evolution of excitonic gaps and Raman phonons with strain. We observed that the strain dependence of excitonic gaps shows a nearly linear behavior in both flakes. One percent of strain increase gives a reduction of;2 meV(;5 me V) in A-exciton gap in monolayer(bilayer) MoSe;. The PL width remains little changed in monolayer MoSe;while it increases rapidly with strain in the bilayer case. We have made detailed discussions on the observed strain-modulated results and compared the difference between monolayer and bilayer cases. The hybridization between 4d orbits of Mo and 4p orbits of Se, which is controlled by the Se–Mo–Se bond angle under strain, can be employed to consistently explain the observations. The study may shed light into exciton physics in few-layer MoSe;and provides a basis for their applications.
基金Supported by the National Natural Science Foundation(11272267,11102168,10932008)111 Project(B07050)
文摘To increase the detectability of split Hopkinson pressure bar (SHPB) of low-impedance materials, modifications were conducted on traditional SHPB apparatus with a PMMA tube to output transmitted signal, and weak signals were further amplified by semiconductor strain gauges. Experiments on soft rubbers and cushioning foam materials were carried out. In order to analyze the accuracy of the experimental results, the stress equilibrium issues involved in the assumptions of SHPB were investigated. First, by way of re-constructing loading process of incident wave, the stress- strain curve was obtained, along with the stress equilibrium ratio of specimen. Secondly, the influences on the accuracy of stress-strain curves were investigated through the elastic modulus comparisons. And the results illustrate that the bilinear incident wave from experiments can ensure the stress equilibrium deformation of specimen after 2 normalized times, much sooner than ramp incident waves. Moreover, it even facilitates specimen deformation with a constant strain rate. The results confirm that the detectability of the modified SHPB can be down to tens kPa with enough accuracy level.