Fine-grained magnesium was tested under stress-controlled tension-tension cyclic loading at -30 ℃ and the tested sample was observed using scanning electron microscope and electron backscatter diffraction to explore ...Fine-grained magnesium was tested under stress-controlled tension-tension cyclic loading at -30 ℃ and the tested sample was observed using scanning electron microscope and electron backscatter diffraction to explore the fatigue behavior and crack propagation. The fatigue data showed that the material experienced cyclic softening followed by cyclic hardening before the final fracture failure. The microscopic observations demonstrated that the cracks were almost perpendicular to the loading direction with some zigzags and the cracks progressed along both small angle grain boundaries and large angle grain boundaries. Although the cracks were mainly propagated along large angle grain boundaries, the value of grain boundary angle was not the primary factor to determine the crack propagation direction. The local residual strain from the rolling process was released due to the crack propagation and there was more strain relaxation at regions closer to the cracks.展开更多
In order to obtain the exact friction coefficient between lining and wire rope, the tension of wire rope is studied as a factor which affects this coefficient. A mechanical model of a wire rope subjected to axial load...In order to obtain the exact friction coefficient between lining and wire rope, the tension of wire rope is studied as a factor which affects this coefficient. A mechanical model of a wire rope subjected to axial load was established to determine the torque of the wire rope. The contact motion between lining and wire rope was regarded as a screw rotation and the axial force of the lining resulting from the torque of the wire rope was analyzed. Theoretical formulas relating tension of the wire rope and the friction coefficient was obtained. Experiments between lining and wire rope with low sliding speed were carried out with friction tester made by us. Experimental results show that increment of the friction coefficient is proportional to that of the tension of the wire rope with a low sliding speed. The experimental results agree with the theoretical calculation; the errors are less than 6%, which oroves the validity of the theoretical model.展开更多
Petroleum sulfonate is one of the most important surfactants used in surfactant flooding for enhanced oil recovery, which is mainly obtained by treating high-boiling petroleum fractions in a stirred tank reactor(STR) ...Petroleum sulfonate is one of the most important surfactants used in surfactant flooding for enhanced oil recovery, which is mainly obtained by treating high-boiling petroleum fractions in a stirred tank reactor(STR) or in a fallingfilm reactor(FFR). The synthesis of petroleum sulfonate with ultra-low interfacial tension from viscous petroleum fractions was carried out in a rotating packed bed(RPB) reactor using dilute liquid sulfur trioxide as the sulfonating agent in this study. The effects of various experimental conditions on components content and oil-water interfacial tension(IFT) were investigated. Under the optimum conditions, the active matter content could reach up to 50.3% and the IFT could be equal to 4.7×10-3 m N/m. Compared with the traditional reactor, the active matter content is by 14.12% higher in the RPB as compared to that obtained in the STR. The uneven change of the test oil droplets during the IFT measurement was also discussed. The increase of heavy components content not only can eliminate the contraction phenomenon, but also can reduce the IFT to a minimum. This can be conducive to explaining the reason for producing IFT and the preparation of proper formulations for practical application.展开更多
In order to determine whether polyphosphoric acid （PPA） can partially or completely substitute styrene-butadiene- styrene （SBS） modifier while it does not adversely affect the resistance to thermal cracking of the...In order to determine whether polyphosphoric acid （PPA） can partially or completely substitute styrene-butadiene- styrene （SBS） modifier while it does not adversely affect the resistance to thermal cracking of the asphalt mixture, the low- temperature fracture properties of the PPA modified mixtures are evaluated and compared to the SBS modified mixtures. First, laboratory compacted test samples were tested by the indirect tensile test （IDT） and the newly developed fracture testing protocol, named as disk-shaped compact tension （DCT）. Then, the effects of the test temperature and air-void ratio on the low-temperature fracture properties of asphalt mixtures were analyzed. The results show that the fracture resistance of the PPA modified mixtures is worse than that of the SBS modified mixtures. However, for those modified mixtures that use the PPA substituting part of the SBS modifier, a relatively low-temperature fracture resistance can be obtained compared with the mixture only using the SBS modifier.展开更多
基金the support from the Basic Energy Sciences Office at the US Department of Energy under Award no.DESC0016333。
文摘Fine-grained magnesium was tested under stress-controlled tension-tension cyclic loading at -30 ℃ and the tested sample was observed using scanning electron microscope and electron backscatter diffraction to explore the fatigue behavior and crack propagation. The fatigue data showed that the material experienced cyclic softening followed by cyclic hardening before the final fracture failure. The microscopic observations demonstrated that the cracks were almost perpendicular to the loading direction with some zigzags and the cracks progressed along both small angle grain boundaries and large angle grain boundaries. Although the cracks were mainly propagated along large angle grain boundaries, the value of grain boundary angle was not the primary factor to determine the crack propagation direction. The local residual strain from the rolling process was released due to the crack propagation and there was more strain relaxation at regions closer to the cracks.
基金Projects 20060290505 supported by the Research Fund for the Doctoral Program of Higher EducationNCET-04-0488 by the New Century Excellent Talent Technological Project of Ministry of Education of China.
文摘In order to obtain the exact friction coefficient between lining and wire rope, the tension of wire rope is studied as a factor which affects this coefficient. A mechanical model of a wire rope subjected to axial load was established to determine the torque of the wire rope. The contact motion between lining and wire rope was regarded as a screw rotation and the axial force of the lining resulting from the torque of the wire rope was analyzed. Theoretical formulas relating tension of the wire rope and the friction coefficient was obtained. Experiments between lining and wire rope with low sliding speed were carried out with friction tester made by us. Experimental results show that increment of the friction coefficient is proportional to that of the tension of the wire rope with a low sliding speed. The experimental results agree with the theoretical calculation; the errors are less than 6%, which oroves the validity of the theoretical model.
基金supported by Project of the National Twelfth Five-Year Research Program of China (Grants. 2014BAE03B02)
文摘Petroleum sulfonate is one of the most important surfactants used in surfactant flooding for enhanced oil recovery, which is mainly obtained by treating high-boiling petroleum fractions in a stirred tank reactor(STR) or in a fallingfilm reactor(FFR). The synthesis of petroleum sulfonate with ultra-low interfacial tension from viscous petroleum fractions was carried out in a rotating packed bed(RPB) reactor using dilute liquid sulfur trioxide as the sulfonating agent in this study. The effects of various experimental conditions on components content and oil-water interfacial tension(IFT) were investigated. Under the optimum conditions, the active matter content could reach up to 50.3% and the IFT could be equal to 4.7×10-3 m N/m. Compared with the traditional reactor, the active matter content is by 14.12% higher in the RPB as compared to that obtained in the STR. The uneven change of the test oil droplets during the IFT measurement was also discussed. The increase of heavy components content not only can eliminate the contraction phenomenon, but also can reduce the IFT to a minimum. This can be conducive to explaining the reason for producing IFT and the preparation of proper formulations for practical application.
基金The National Natural Science Foundation of China(No.51278060)
文摘In order to determine whether polyphosphoric acid （PPA） can partially or completely substitute styrene-butadiene- styrene （SBS） modifier while it does not adversely affect the resistance to thermal cracking of the asphalt mixture, the low- temperature fracture properties of the PPA modified mixtures are evaluated and compared to the SBS modified mixtures. First, laboratory compacted test samples were tested by the indirect tensile test （IDT） and the newly developed fracture testing protocol, named as disk-shaped compact tension （DCT）. Then, the effects of the test temperature and air-void ratio on the low-temperature fracture properties of asphalt mixtures were analyzed. The results show that the fracture resistance of the PPA modified mixtures is worse than that of the SBS modified mixtures. However, for those modified mixtures that use the PPA substituting part of the SBS modifier, a relatively low-temperature fracture resistance can be obtained compared with the mixture only using the SBS modifier.
