Dependence of Lower Molding Temperature Limit and Molding Time on Molding Mechanism in Dental Thermoforming

Effectiveness and safety of a sports mouthguard depend on its thickness and material, and the thermoforming process affects these. The purpose of this study was to clarify the effects of differences in molding mechanisms on the lower molding temperature limit and molding time in dental thermoforming. Ethylene vinyl acetate resin mouthguard sheet and two thermoforming machines;vacuum blower molding machine and vacuum ejector/pressure molding machine were used. The molding pressures for suction molding were −0.018 MPa for vacuum blower molding and −0.090 MPa for vacuum ejector molding, and for pressure molding was set to 0.090 MPa or 0.450 MPa. Based on the manufacturer’s standard molding temperature of 95˚C, the molding temperature was lowered in 2.5˚C increments to determine the lower molding temperature limit at which no molding defects occurred. In order to investigate the difference in molding time depending on the molding mechanism, the duration of molding pressure was adjusted in each molding machine, and the molding time required to obtain a sample without molding defects was measured. The molding time of each molding machine were compared using one-way analysis of variance. The lower molding temperature limit was 90.0˚C for the vacuum blower machine, 77.5˚C for the vacuum ejector machine, 77.5˚C for the pressure molding machine at 0.090 MPa, and 67.5˚C for the pressure molding machine at 0.45 MPa. The lower molding temperature limit was higher for lower absolute values of molding pressure. The molding time was shorter for pressure molding than for suction molding. Significant differences were observed between all conditions except between the pressure molding machine at 0.090 MPa and 0.45 MPa (P < 0.01). A comparison of the differences in lower molding temperature limit and molding time due to molding mechanisms in dental thermoforming revealed that the lower molding temperature limit depends on the molding pressure and that the molding time is longer for suction molding than for pressure molding.

Association between Low Ambient Temperature and the Severity of Acute Ischemic Stroke

Objective:To explore the relationships among ambient temperature,ischemic stroke severity,and blood pressure.Methods:Meteorological data(2005–2015)were collected from the Guangzhou Meteorological Data Service.Ischemic stroke patients from the Department of Neurology of the First Affiliated Hospital,Sun Yat-sen University were retrospectively evaluated,each winter from 2005 to 2015.Patient demographics,baseline measurements,and National Institute of Health Stroke Scale(NIHSS)score were evaluated.Results:Three hundred sixty-two patients were included.The median latency from symptom onset to admission was 2 d(IQR:1–3 d).During recruitment,the highest and lowest temperatures were 39℃and 1.3℃,respectively.Hypertension was the most common comorbidity(75.1%).NIHSS scores at admission and discharge were higher in the cold-exposed group than in the controls regardless of the average temperature at admission.In addition,systolic and diastolic blood pressure values at admission were higher in the cold-exposed group than in the controls.When stratified by hypertensive status,the average and minimum temperatures at admission were negatively associated with systolic and diastolic blood pressure values in hypertensive patients.Reductions in the average and minimum temperatures at symptom onset were associated with more severe stroke.Conclusion:Ischemic stroke patients with symptom onset in winter had higher systolic blood pressure values and more serious neurologic deficits upon admission.

A two-dimensional air streamer discharge modified model based on artificial stability term under non-uniform electric field at low temperature and sub-atmospheric pressure

In this paper, an improved air discharge fluid model under non-uniform electric field is constructed based on the plasma module COMSOL Multiphysics with artificial stability term, and the boundary conditions developed in the previous paper are applied to the calculation of photoionization rate. Based on the modified model, the characteristics of low temperature subatmospheric air discharge under 13 kV direct current voltage are discussed, including needle-plate and needle-needle electrode structures. Firstly, in order to verify the reliability of the model, a numerical example and an experimental verification were carried out for the modified model respectively. Both verification results show that the model can ensure the accuracy and repeatability of the calculation. Secondly, according to the calculation results of the modified model, under the same voltage and spacing, the reduced electric field under low temperature subatmosphere pressure is larger than that under normal temperature and atmospheric pressure. The high electric field leads to the air discharge at low temperature and sub atmospheric pressure entering the streamer initiation stage earlier, and has a faster propagation speed in the streamer development stage, which shortens the overall discharge time. Finally, the discharge characteristics of the two electrode structures are compared, and it is found that the biggest difference between them is that there is a pre-ionization region near the cathode in the needle-needle electrode structure. When the pre-ionization level reaches 1013 cm-3, the propagation speed of the positive streamer remains unchanged throughout the discharge process, and is no longer affected by the negative streamer. The peak value of electric field decreases with the increase of pre-ionization level, and tends to be constant during streamer propagation. Based on the previous paper, this paper constructs the air discharge model under non-uniform electric field, complements with the previous paper, and forms a relatively complete set of air discharge simulation system under low temperature and sub atmospheric pressure, which provides a certain reference for future research.

A two-dimensional air streamer discharge model based on the improved Helmholtz equation at low temperature and sub-atmospheric pressure

In this paper,an efficient boundary condition is applied to solve the photoionization rate,and a two-dimensional numerical simulation is carried out for the development and propagation of an air streamer at low temperature and sub-atmospheric pressure.The results show that the new boundary condition improves the calculation accuracy,but the influence of photoionization on the streamer discharge process is not obvious.The discharge current in the development of streamer discharge is defined,and the corresponding expression of the positive and negative streamer discharge current is given.The influence of the electric field exceeding the threshold value on the discharge process is preliminarily introduced.In the process of discharge,only the propagation velocity of the streamer is obviously higher than that of normal temperature and pressure,and the trend of the other parameters is basically the same as that described in the previous paper.The above results give us a deeper understanding of the discharge characteristics under low temperature and sub-atmospheric pressure,which has certain significance for the development of aviation and high voltage engineering.

Low-temperature heat conduction characteristics of diamond/Cu composite by pressure infiltration method

In this paper,diamond/CuCr and diamond/CuB composites were prepared using the pressure infiltration method.The physical property measurement system(PPMS)was adopted to evaluate the thermal conductivity of diamond/Cu and MoCu composites within the range of100–350 K,and a scanning electron microscope(SEM)was utilized to analyze the microstructure and fracture appearance of the materials.The research indicates that the thermal conductivity of diamond/Cu composite within the range of100–350 K is 2.5–3.0 times that of the existing MoCu material,and the low-temperature thermal conductivity of diamond/Cu composite presents an exponential relationship with the temperature.If B element was added to a Cu matrix and a low-temperature binder was used for prefabricated elements,favorable interfacial adhesion,relatively high interfacial thermal conductivity,and favorable low-temperature heat conduction characteristics would be apparent.

Thickening and Rheological Properties of Crystalline Polyester Used in Low Pressure Sheet Molding Compounds

Low pressure sheet molding compound （LPMC,1.0-3.0 MPa,95-103 ℃） is a new kind of thermosetting material with crystalline polyester as a physical thickenner.LPMC is different from conventional SMC using an earth oxide thickening agent （e.g.MgO） as chemical thickenner,it relies on the physical thickening of crystalline polyester.Crystalline polyester resin is the key material to mold LPMC parts.Currently there was no report about the thickening mechanism of crystalline polyester in LPMC.In this article,crystalline polyester resins,whose melting points were between 45 ℃ and 89 ℃,were synthesized by a two-step esterification.The melt points of crystalline polyesters are controlled by regulating the mol ratio of the two glycols and the two acids.And by means of varying the content of crystalline polyester resin,the thickening effect on resin paste is investigated.In addition,the thickening mechanism of crystalline polyester in LPMC was investigated by FTIR and DSC analysis.The effects of the diameters and viscosity of crystalline polyester on the rheological property and fiber distribution of LPMC sheets were studied,too.Results show that the thickening effect is excellent when the weight content of crystalline polyester resin is 3%.And there exists three kinds of functions acting in the process of thickening：swelling,hydrogen bonds and induction crystallization.During the preparing process of resin paste in LPMC,the temperature of resin paste must be kept at 90 ℃.In addition,crystalline polyester make LPMC have a perfect fluid property.When the viscosity of LPMC sheet is beyond 1 kPa s,the fiber orientation is not obvious.But when the viscosity of LPMC sheet is about 500 Pa s,the fiber shows a certain degree of orientation.Moreover the study of physical and chemical thickening mechanism of crystalline polyester and the rheological discipline of LPMC sheets in the hot mould will provide the researchers and enterprises with theory guidance.

Structures and Low Temperature Magnetic Anomalies of High Pressure RE_2CuO_4

A series of oxygen-doped RE_2CuO_4 (RE=Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm) was synthesized using high-pressure/oxygen-doped technique. The structures and low temperature magnetic properties were investigated. The XRD patterns indicate that the structures of high oxygen pressure RE_2CuO_4 (only for RE=Sm, Eu) samples are pure T′ phase, but when RE= Gd, Tb, Dy, Ho, Er, Tm, the structures turn to disorder. The magnetic anomalies that occurred at T^30 K are observed in high oxygen pressure RE_2CuO_4. It is found that the transition temperatures of weak ferromagnetic anomalies are nearly independent of the rare-earth components. Thus, the O-doping plays an important role in anomalous magnetic properties of RE_2CuO_(4+δ). The magnetic anomalies in RE_2CuO_4 are considered to be due to ferromagnetic clusters formed in the Cu-O plane after the oxygen doping.

Advanced high-pressure transport measurement system integrated with low temperature and magnetic field

We briefly introduce a new high-pressure transport measurement system integrated with low temperature and magnetic field that is being established as one of the user experimental stations of the Synergetic Extreme Condition User Facilities in the Huairou District of Beijing, China. To demonstrate the capabilities of the system for condensed matter research, the emergence of some pressure-induced phenomena and physics related to superconductivity found previously is also introduced, and then a perspective for such an advanced high-pressure system is presented.

Pressure-Induced Metallization and Electrical Phase Diagram for Polycrystalline CaB_6 under High Pressure and Low Temperature

The electrical properties of polycrystaltine CaB6 are revealed by in-situ resistance measurements under high pressure and low temperature. Due to the existence of grain boundaries, polycrystalline CaB6 behaves with semiconducting transport properties, which is different from the semimetallic CaB6 single crystals. The temperaturedependent resistance measurement results show that before the structural phase transition at 12.3 GPa the high pressure first induces the metallization at 6.5 GPa for CAB6. Moreover, the phase diagram for CaB6 is drawn based on the investigated electric conducting properties and at least three different conducting phases are found even at moderate high pressure and low temperature, indicating that the electric nature of CaB6 is very sensitive to the environment.

Polymer Surface Treatment by Atmospheric Pressure Low Temperature Surface Discharge Plasma:Its Characteristics and Comparison with Low Pressure Oxygen Plasma Treatment

The polymer treatment with a low-temperature plasma jet generated on the atmospheric pressure surface discharge （SD） plasma is performed. The change of the surface property over time, in comparison with low pressure oxygen （O2） plasma treatment, is examined. As one compares the treatment by atmospheric pressure plasma to that by the low pressure O2 plasma of PS （polystyrene） the treatment effects were almost in complete agreement. However, when the atmospheric pressure plasma was used for PP（polypropylene）, it produced remarkable hydrophilic effects.

Determination of Thermodynamic Parameters of Some Fluorochlorohydrocarbons in Acetone by Gas Chromatography at Low Temperature and Pressurization

1 INTRODUCTIONGas chromatography(GC)has been proved to perform satisfactorily in vapor-liquid equilib-rium measurements and in the study of solution theory.Infinite dilution data are useful notonly for design calculations but also for theoretical development of correlations.Studies inthis field have been carried on at the Zhejiang University.

Practice and Cognition of Midway VSP in High Temperature and High Pressure Field of South China Sea

Ying-Qiong Basin is a typical high-temperature and overpressure basin, which is the main battlefield of oil and gas exploration in South China Sea and has made great breakthroughs in recent years. During drilling process in high pressure, the relationship between the deep and the pressure is directly related to the drilling safety and costs. In order to improve prediction accuracy, the VSP operation is carried out through the midway, and three points have been obtained: 1) The VSP has a higher accuracy of the interface depth in certain depth range of the drill bit. 2) When the low-frequency trend prediction is accurate before the drill bit, interval velocity of the VSP inversion is consistent with the formation velocity. 3) The VSP pressure forecast is based on the inversion layer velocity and under-compaction pressure. If the velocity prediction is not accurate, the pressure forecast must be erroneous. If the pressure has other sources, the formation pressure is not accurate even if the inversion velocity is accurate. The application scope and exploration effect of midway VSP operation are summarized and applied to Ledong 10-1 block in Yinggehai basin, which realize the breakthrough in the field of high temperature overpressure and provide the basis for other similar exploration areas to do VSP operation.

Study on Numerical Simulation of Mold Filling and Solidification Processes under Pressure Conditions

The mold filling and solidification simulation for the high pressure die casting (HPDC) and low pressure die casting (LPDC) processes were studied. A mathematical model considering the turbulent flow and heat transfer phenomenon during the HPDC process has been established and parallel computation technique was used for the mold filling simulation of the process. The laminar flow characteristics of the LPDC process were studied and a simplified model for the mold filling process of wheel castings has been developed. For the solidification simulation under pressure conditions, the cyclic characteristics and the complicated boundary conditions were considered and techniques to improve the computational efficiency are discussed. A new criterion for predicting shrinkage porosity of Al alloy under low pressure condition has been developed in the solidification simulation process.

Start-up and contaminants removal characteristics of aerobic granules-membrane bioreactor at low temperature

In order to understand the effect of low temperature on the formation process of aerobic granules and contaminants removal characteristics,the aerobic granules-membrane bioreactor (AGS-MBR) has been started up and operated at low temperature using the carbon resource of sodium acetate. Aerobic granules cultivated in AGS-MBR possess smooth surface and compact structure in morphology as well as better settling property and higher biomass after 38 days. The average parameters of aerobic granules are: diameter 3. 1 mm,wet density 1. 041 g/mL,sludge volume index 42. 35 mL/g and settling velocity 20. 6 - 45. 2 cm/min. During the start-up of AGS-MBR,the respectively average contaminants removal efficiencies at low temperature are 91. 9% for chemical oxygen demand (COD) ,89. 2% for NH4 + -N and 86. 3% for PO43- -P,and the overgrowth of filamentous bacteria has been well controlled. In addition,the hollow fiber microfiltration (MF) membrane fouling is light and the regime membrane layer is capable of enhancing membrane filtration as well as the average growth of trans-membrane pressure (TMP) is 1. 07 kPa/d. Compared with the conventional cultivation of aerobic granules,the sludge granulation time significantly decreases from 73 days to 38 days by the application of microfiltration membrane at low temperature.

Comparison between Theoretical and Experimental Radial Electron Temperature Profiles in a Low Density Weakly Ionized Plasma

Experimental and theoretical studies of the radial distribution function of the electron temperature (RDFT) in a low-density plasma and weakly ionized gas for the abnormal glow region are presented. Experimentally, the electron temperatures and densities are measured by a Langmuir probe moved radially from the center to the edge of the cathode electrode for helium gas at different pressures in the low-pressure glow discharge. The comparison of the final experimental data for the radial distribution of electron temperatures and densities for different low pressures ranging from 0.2 to 1.2 torr, with the final proved equation of RDFT confirms that the electron temperatures decrease with increasing product of radial distance and gas pressures, showing a radial decrement dependence of the electron temperature from the center to the edge of the electrode. This is attributed to the increase of the number of electron-atom collisions at higher gas pressures and consequently of the rate of ionization. For the axial distance (L) from the tip of the probe to cathode electrode and the cathode electrode radius (R), a theoretical and experimental comparison for the two conditions L R and L > R, for both cases the produced plasma temperatures decrease and densities increase. It is concluded that the RDFT accurately shows a dramatic decrease for L R by 60% less than RDFT values for L > R similar as for conditions of magnetized and unmagnetized effect for DC plasma. This means that the rate of plasma loss by diffusion decreased for L R, agrees well with the applied of magnetic field

基于Moldflow的储物盒注塑成型模拟及试验验证

对储物盒盖的注塑难点进行分析,得出模具应设计成单热流道双腔结构。选取熔体温度、注射时间、保压压力、保压时间为研究对象,利用Moldflow 2018模流分析软件,构建4因素4水平正交试验,通过极差分析,得出储物盒盖在熔体温度226℃、注射时间14 s、保压压力70 MPa、保压时间10 s的条件下,变形总量最小,为0.45 mm。对获得的最优参数进行了试验验证,验证结果表明,成型后储物盒盖整体外观良好;佐证了Moldflow 2018有限元分析数据准确,正交试验构建及模具设计合理。

基于Moldflow的电蚊香加热器上盖翘曲的优化分析

分析了电蚊香上盖的结构和成型工艺,使用Moldflow软件确定浇口最佳位置,并优化浇注过程中的工艺参数,通过对成型过程的模流分析,合理调整模具温度,优化保压曲线,以减小由于收缩不均所引起的翘曲问题,为注塑模具设计提供合理依据。这种利用模流分析软件Moldflow进行注塑模具优化设计的方法,缩短了开发周期,使得注塑模具设计更具有准确性。

Frost-heaving pressure in geotechnical engineering materials during freezing process

Energy and resources including coal, oil, and gas are in demand all over the world. Because these resources near the earth's surface have been exploited for many years, the extraction depth has increased.As mining shafts in the coal extraction process become deeper, especially in western China, an artificial freezing method is used and is concentrated in the fractured rock mass. The frost-heaving pressure(FHP)is directly related to the degree of damage of the fractured rock mass. This paper is focused on FHP during the freezing process, with emphasis on the frost-heaving phenomenon in engineering materials. A review of the frost phenomenon in the geotechnical engineering literature indicates that:(1) During the soil freezing process, the ice content that is influenced by unfrozen water and the freezing rate are the determining factors of FHP;(2) During the freezing process of rock and other porous media, the resulting cracks should be considered because the FHP may damage the crack structure;(3) The FHP in a joint rock mass is analyzed by the joint deformation in field and experimental tests and can be simulated by the equivalent expansion method including water migration and joint deformation.

Influence of tectonic uplift-erosion on formation pressure

The formation of abnormally low-pressure hydrocarbon reservoirs in petroliferous basins has a close relationship with tectonic uplift and the consequent erosion. In order to understand abnormally low-pressure reservoirs and to provide a scientific basis for exploration and development, we established, through numerical simulation and theoretical analysis, a set of equations for the formation pressure in a closed system influenced by uplift-erosion, discussed the relationship between the genesis of abnormal pressure and uplift-erosion, and put forward the concept of balance pressure （P b ）. The results showed that abnormally high pressure coefficient may form when the current formation pressure was higher than P b , and abnormally low pressure may form when the current formation pressure was lower than P b . In the Santanghu Basin, the current formation pressure of abnormally low pressure reservoirs is lower than P b , so tectonic uplift-erosion leads to the decrease of the pressure coefficient. There is a positive correlation between the pressure drop caused by the decrease of fluid temperature and the rebound of rock porosity and strata erosion. Calculation results indicated that the reservoir pressure of Jurassic strata in the Santanghu Basin was decreased by 11.6-17.1 MPa due to tectonic uplift-erosion during the Late Yanshanian period.

Interannual and Interdecadal Variability of East Asian Acas and Their Impact on Temperature of China in Winter Season for the Last Century

The interannual and interdecadal varinbility of the Siberian High (SH) and the Aleutian Low (AL) from aspects of strength and location for the past one hundred years as well as their possible relations with temperature changes over China's Mainland are investigated. The data sets used are the historical sea level pressure for 1871-1995 and surface air temperature (SAT) over China in the last 100 years. The results show that the SAT in different regions over China, central strength of the SH and the AL, the south-reaching latitude of the 1030 hPa contour of the SH and the pressure gradient between the SH and the AL experienced two obvious changes during this period. One occurred in the 1920s, with a more prominent one in the 1980s. These variations are closely linked with the change of winter temperature over China in the interdecadal timescale. In the last 50 years, there is a remarkable interannual correlation between the strength of Active Centers of Atmosphere (Acas) and the winter temperature of northern and eastern regions in China. The abrupt change of Acas in the 1980s is consistent with the rising of the SAT in China. Since the late 1980s, the atmospheric circulation is experiencing a remarkable modulation, which may cause the interdecadal transition of warming trend.