Low palladium content CeO_(2)/ZnO composite for acetone sensor with sub-second response prepared by ultrasonic method

In practical applications,noble metal doping is often used to prepare high performance gas sensors,but more noble metal doping will lead to higher preparation costs.In this study,CeO_(2)/ZnO-Pd with low palladium content was prepared by ultrasonic method with fast response and high selectivity for acetone sensing.With the same amount of palladium added,the selectivity coefficient of CeO_(2)/ZnO-Pd is 1.88 times higher than that of the stirred sensor.Compared with the pure PdO-doped CeO_(2)/ZnO-PdO material,the content of Pd in CeO_(2)/ZnO-PdO is about 30%of that in CeO_(2)/ZnO-PdO,but the selectivity coefficient for acetone is 2.56 times higher.The CeO_(2)/ZnO-Pd sensor has a higher response(22.54)to 50×10^(−6) acetone at 300℃and the selectivity coefficient is 2.57 times that of the CeO_(2)/ZnO sensor.The sensor has a sub-second response time(0.6 s)and still has a 2.36 response to 330×10^(−9) of acetone.Ultrasonic doping makes Pd particles smaller and increases the contact area with gas.Meanwhile,the composition of n-p-n heterojunction and the synergistic effect of Pd/PdO improve the sensor performance.It shows that ultrasonic Pd doping provides a way to improve the utilization rate of doped metals and prepare highly selective gas sensors.

Research and Application of Log Defect Detection and Visualization System Based on Dry Coupling Ultrasonic Method

In order to optimize the wood internal quality detection and evaluation system and improve the comprehensive utilization rate of wood,this paper invented a set of log internal defect detection and visualization system by using the ultrasonic dry coupling agent method.The detection and visualization analysis of internal log defects were realized through log specimen test.The main conclusions show that the accuracy,reliability and practicability of the system for detecting the internal defects of log specimens have been effectively verified.The system can make the edge of the detected image smooth by interpolation algorithm,and the edge detection algorithm can be used to detect and reflect the location of internal defects of logs accurately.The content mentioned above has good application value for meeting the requirement of increasing demand for wood resources and improving the automation level of wood nondestructive testing instruments.

Optimal design of butterfly-shaped linear ultrasonic motor using finite element method and response surface methodology

A new method for optimizing a butterfly-shaped linear ultrasonic motor was proposed to maximize its mechanical output. The finite element analysis technology and response surface methodology were combined together to realize the optimal design of the butterfly-shaped linear ultrasonic motor. First, the operation principle of the motor was introduced. Second, the finite element parameterized model of the stator of the motor was built using ANSYS parametric design language and some structure parameters of the stator were selected as design variables. Third, the sample points were selected in design variable space using latin hypercube Design. Through modal analysis and harmonic response analysis of the stator based on these sample points, the target responses were obtained. These sample points and response values were combined together to build a response surface model. Finally, the simplex method was used to find the optimal solution. The experimental results showed that many aspects of the design requirements of the butterfly-shaped linear ultrasonic motor have been fulfilled. The prototype motor fabricated based on the optimal design result exhibited considerably high dynamic performance, such as no-load speed of 873 ram/s, maximal thrust of 27.5 N, maximal efficiency of 43%, and thrust-weight ratio of 45.8.

SiC nanoparticles reinforced magnesium matrix composites fabricated by ultrasonic method

SiC nanoparticles reinforced magnesium matrix composites were fabricated by ultrasonic method.The AZ91 alloy and SiC nanoparticles with the average diameter of 50 nm were used as the matrix alloy and the reinforcement,respectively.The addition of nanoparticles was 0.1%,0.3%,and 0.5%(mass fraction) of the composites.The results of microstructural evaluation and mechanical properties indicate that the nanoparticles can be dispersed into magnesium alloys efficiently and uniformly with the aid of ultrasonic vibration.As compared with the matrix alloys,the grains of composites were refined and the mechanical properties of composites were improved significantly.The SEM and DSC analyses show that the SiC nanoparticles can act as the heterogeneous nucleation of α-Mg.Also,the strengthening mechanism responsible for the composites reinforced with SiC nanoparticles was discussed.

A new method of measuring optical turbulence of atmospheric surface layer at Antarctic Taishan Station with ultrasonic anemometer

To find the optimal location for large-aperture telescopes is a goal of astronomy. Chinese Antarctic astronomy has begun to flourish in recent years, and it is an urgent need in basic astronomical work to measure and analyze the optical turbulence spatiotemporal distribution in the Antarctic region. We analyzed turbulence data measured by a mobile atmospheric parameter measurement system from 30 December 2013 to 10 February 2014 at Antarctic Taishan Station. Because there is a discrepancy between the refractive index structure constant Cn2 measured by an ultrasonic anemometer with a single-point temperature structure function method and by micro-thermometer, a new method to measure C,2 with a temperature spectrum method is proposed herein. Through comparing long-term continuous Cn2 data derived from ultrasonic anemometer with those via the new method and micro-thermometer, trend, magnitude and measured weak turbulence of-2× 10-16m-2/3 are generally satisfactory. The reason for the discrepancy in Cn2 measurement between the ultrasonic anemometer with the old method and micro-thermometer is investigated.

TECHNOLOGY OF QUANTITATIVE ANALYSIS ON VIBRATORY STRESS RELIEF BASED ON ULTRASONIC TIME-OF-ARRIVAL METHOD

The effect of vibratory stress relief （VSR） is usually evaluated with the indirect method of observing the change of amplitude frequency response characteristics of structures. A new kind of evaluating method of VSR based on the ultrasonic time-of-arrival method （UTM）, which can obtain the residual stress directly through measuring the propagation time of ultrasonic wave in the material, is presented. At first, the principle of the measuring method of residual stress based on UTM is analyzed. Then the measuring system of the method is described, which is in virtue of ultrasonic flaw detector and high-sampling-rate digital oscillograph. And a set of calibration system that contains a piece of standard specimen is also introduced. Experimental results prove the relation between the residual stress and the propagation time of ultrasonic in workpieces. Finally, the measuring and calibration systems are applied in evaluating the effect of VSR. The final test results show that the method is effective.

Application of Compactness Detection to Complicated Concrete-Filled Steel Tube by Ultrasonic Method

An example of using ultrasonic method to detect the compactness of complicated concrete-filled steel tube in certain high-rise building was discussed in this study.Because of the particularity of the complicated concrete-filled steel tubular column,the plane detection method and embedded sounding pipe method were adopted in the process of effectively detecting the column.According to the results of the plane detection method and embedded sounding pipe method,the cementing status of steel tube and concrete can be concluded,which cannot be judged by the hammering method in the rectangular steel tube-reinforced concrete.

The Optimization of Ultrasonic Extraction Process of Total Flavonoids from Rhodiola Crenulata by Response Surface Method

[Objectives]To study the optimal extraction process of total flavonoids in Rhodiola rosea L.,and further facilitate the development and utilization of Rhodiola rosea L. [Methods]With Rhodiola crenulata as raw material,ethanol as extractant,ultrasonic extraction as the extraction method,the single factor method was first used for preliminary investigation of effect of ethanol volume fraction,solid-liquid ratio,extraction temperature and extraction time on the flavonoids extraction rate,and then the Box-Behnken response surface method was used to optimize the extraction process of total flavonoids in R. crenulata. [Results] The optimal extraction conditions: ethanol concentration of 72%;solid-liquid ratio of 1∶ 43; extraction temperature of 66℃; extraction time of 50 min. Under these conditions,the extraction rate of total flavonoids from R. crenulata was 2. 591%. [Conclusions] The results showed that the method of response surface was reasonable and feasible for the optimization of ultrasonic extraction of total flavonoids from R. crenulata.

Technology of Extracting Kiwi Fruit Seed Oil with Ultrasonic-Assisted Enzyme and Response Surface Method

Taken kiwi fruit as raw material, this paper extracted kiwi fruit seed oil with ultrasonic-assisted enzyme, researched the influence of factors such as liquid-to-solid ratio, granularity, type of enzyme, ultrasonic power, treating time, enzymolysis temperature, enzymolysis time, pH and enzyme additive on oil extraction, and optimized the extracting technology of kiwi fruit seed oil with response surface method. The result shows that the best technical parameter is: material granularity: 60, liquid-to-solid ratio: 1:10 (g/mL), ultrasonic power: 400 W, treating time: 30 min, enzyme amount: 2.50%, pH: 9.2, enzymolysis temperature: 53°C, enzymolysis time: 2.80 h;and the extracting ratio under such condition is 92.57%.

An efficient nano-adsorbent via surfactants/dual surfactants assisted ultrasonic co-precipitation method for sono-removal of monoazo and diazo anionic dyes

To preserve the environment for civilization,we should remove the pollutants like toxic dyes by friendly and cost efficacious method.In this study,the effect of surfactants or mixed surfactants on physicochemical,optical and adsorption properties of ternary mixed oxide CeO_(2)-ZrO_(2)-Al_(2) O_3(CZA) are investigated.The ternary mixed oxide CZA was prepared by surfactants or mixed surfactants assisted ultrasonic coprecipitation method.The physicochemical and optical properties are estimated by different techniques like XRD,TEM,EDX,FTIR,S_(BET) and UV-Vis/DR.The CZA_T and CZA_C have hybrid shapes and high surface area.The adsorption properties of ternary mixed oxides adsorbents were characterized by sono-removing anionic dyes such as Congo red(CR) and Remazol red RB-133(RR).The different factors like contact time,different dye concentrations and temperatures also studied.The kinetics and isotherms applications showed that,the adsorption process was followed pseudo second order kinetics and the Freundlich isotherm model.Also,the adsorption is spontaneous and endothermic process through the thermodynamic study.Finally,the results showed that the ternary mixed oxide nano-adsorbent(CeO_(2)-ZrO_(2)-Al_(2) O_3) is promising and functional materials for anionic dye sweep from wastewater.

The Testing Strength Curves of Lightweight Aggregate Concrete by Rebound Method and Ultrasonic-rebound Combined Method

The strength curves of lightweight aggregate concrete （LWAC） were tested based on detecting LWAC with density of 1 400-1 900 kg/m3 and LWAC with strength grade of LC15-LC50 by rebound method and ultrasonic-rebound combined method.The results show that the common measured strength curves tested by above two methods can not satisfy the required accuracy of LWAC strength test.In addition,specified compressive strength curves of testing LWAC by rebound method and ultrasonic-rebound combined method are obtained,respectively.

Damage analysis for particle reinforced metal matrix composite by ultrasonic method

The damage characteristic of particle reinforced metal matrix composite (PMMC) was studied by ultrasonic non-destructive evaluation method. After the sample was damaged induced by tensile load, the ultrasonic wave that propagated in the sample were collected. The damage parameter was defined by ultrasonic parameter and the wave signals were analyzed by correlation method. The results show that with the increase of tensile load, the damage parameter increases and the correlation coefficient decreases. The fracture section morphologies of PMMC under tensile load were observed by SEM. It is found that there are many concaves in the metal matrix. Therefore the damage evolution can be concluded. The initial damage is induced by void nucleation, growth and subsequent coalescence in the matrix or interface separation.

Tactile sensitivity in ultrasonic haptics: Do different parts of hand and different rendering methods have an impact on perceptual threshold?

Background Ultrasonic tactile representation utilizes focused ultrasound to create tactile sensations on the bare skin of a user's hand that is not in contact with a device.This study is a preliminary investigation on whether different ultrasonic haptic rendering methods have an impact on the perceptual threshold.Methods This study conducted experiments with the adaptive step method to obtain participants'perceptual thresholds.We examine(1)whether different parts on the palm of the hand have different perceptual thresholds;(2)whether the perceptual threshold is different when the ultrasonic focus point is stationary and when it moves in different trajectories;(3)whether different moving speeds of the ultrasonic focus point have an influence on the perceptual threshold;and(4)whether the addition of a DC offset to the modulating wave has an impact on the perceptual threshold.Results The results show that the center of the palm is more sensitive to ultrasonic haptics than the fingertip;compared with a fast-moving focus point,the palm is more sensitive to a stationary and slow-moving focus point.When the modulating wave has a DC offset,the palm is sensitive to a much smaller modulation amplitude.Conclusion For the future ultrasonic tactile representation systems,dynamic adjustment of intensity is required to compensate the difference in perceptual thresholds under different rendering methods to achieve more realistic ultrasonic haptics.

LEAD SCREW LINEAR ULTRASONIC MOTOR USING BENDING VIBRATION MODES

The operating principle of a lead screw linear ultrasonic motor using bending vibration modes is analyzed. The simplified beam bending vibration model is used to analyze the dynamics characteristics of the motor. Motion trajectory equations are derived for driving points of the stator. The motor operation and driving mechanisms are investigated. The vibration modes and the construction of the motor are analyzed by using the finite element method （FEM）. A prototype motor is built and its stator dimension is 13 mm × 13 mm× 30 mm. The motor is experimentally characterized and the maximum output force of 5- 2 N is obtained.

Effect of ultrasonic on structure and electrochemical performance of α-Ni(OH)_2 electrodes

Al/Co co-doped α-Ni（OH）2 samples were prepared by either ultrasonic co-precipitation method （Sample B） or co-precipitation method （Sample A）. The crystal structure and particle size distribution of the prepared samples were examined by X-ray diffraction （XRD） and laser particle size analyzer, respectively. The results show that Sample B has more crystalline defects and smaller average diameter than Sample A. The cyclic voltammetry and electrochemical impedance spectroscopy measurements indicate that Sample B has better electrochemical performance than Sample A, such as better reaction reversibility, lower charge-transfer resistance and better cyclic stability. Proton diffusion coefficient of Sample B is 1.96×10-10cm2/s, which is two times as large as that （9.78×10-11cm2/s） of Sample A. The charge-discharge tests show that the discharge capacity （308 mA·h/g） of Sample B is 25 mA·h/g higher than that of Sample A （283 mA·h/g）.

Phase aberration correction in ultrasonic phased array non-destructive testing systems

Phase aberration correction for medical ultrasound systems has attracted a great deal of attention. Since phased array techniques are now widely employed for industrial non-destructive testing （NDT） applications in various fields, the problem of phase aberrations in the process of NDT testing is considered. The technique of cross-covariance for phase aberration correction is presented. The performance of the technique for phase aberration correction is tested by means of echo signals obtained in practical non-destructive testing experiment. The results show that the technique has the better accuracy of phase correction.

Finite element modeling of heating phenomena of cracks excited by high-intensity ultrasonic pulses

A three-dimensional thermo-mechanical coupled finite element model is built up to simulate the phenomena of dynamical contact and frictional heating of crack faces when the plate containing the crack is excited by high-intensity ultrasonic pulses. In the finite element model, the high-power ultrasonic transducer is modeled by using a piezoelectric thermal-analogy method, and the dynamical interaction between both crack faces is modeled using a contact-impact theory. In the simulations, the frictional heating taking place at the crack faces is quantitatively calculated by using finite element thermal-structural coupling analysis, especially, the influences of acoustic chaos to plate vibration and crack heating are calculated and analysed in detail. Meanwhile, the related ultrasonic infrared images are also obtained experimentally, and the theoretical simulation results are in agreement with that of the experiments. The results show that, by using the theoretical method, a good simulation of dynamic interaction and friction heating process of the crack faces under non-chaotic or chaotic sound excitation can be obtained.

SIMULATION ON HEATING PROCESS IN ULTRASONIC WELDING OF PLASTICS

The energy conversion during ultrasonic plastic welding is analyzed on the basis of the theory of vis- coelastic mechanics,.The temperature field and the temperature change of the ABS specimen with ener- gy director during ultrasonic welding is simulated with finite element method(FEM). In the simu- lation process,the melting of the energy energy is also considered. The calculation results are in good agreement with the temperature measurement results, which proves that the simulation results are reli- able.

Fracturing behavior of brittle solids containing 3D internal crack of different depths under ultrasonic fracturing

Ultrasonic fracturing(UF)can be used to form crack networks for oil or gas in the mining industry and hard rock excavation.In this paper,the three-dimensional internal laser-engraved crack method(3DILC)is introduced to make penny-shaped internal crack within the samples without any damage to the surfaces.Physical experiments were performed on the transparent samples with internal cracks at different depths.The macro-and micro-fracture fractography characteristics were focused on and analyzed in details.Based on fractography,the mechanisms of the UF were revealed.The propagation paths of cracks of different depths were simulated based on the Paris fatigue model and compared with experimental results.The results show that the 3D-ILC method is a powerful tool for the experimental research on the internal crack propagation in the UF.Under the action of ultrasonic field,fractography shows the characteristics of beach marks,lance-like pattern,rime-like pattern and glass powder.It can be judged that the mechanisms of UF include high cycle fatigue fracture,shear fracture,and friction.The results of the numerical simulation using the Paris fatigue model are consistent with the experimental results.

Modeling and Experimental Analysis of Roughness Effect on Ultrasonic Nondestructive Evaluation of Micro-crack

A high-precision evaluation of ultrasonic detection sensitivity for a micro-crack can be restricted by a corroded rough surface when the surface microtopography is of the same order of magnitude as the crack depth.In this study,a back-surface micro-crack is considered as a research target.A roughness-modified ultrasonic testing model for micro-cracks is established based on a multi-Gaussian beam model and the principle of phase-screen approximation.The echo signals of micro-cracks and noises corresponding to different rough front surfaces and rough back surfaces are obtained based on a reference reflector signal acquired from a two-dimensional simulation model.Further compari-son between the analytical and numerical models shows that the responses of micro-cracks under the effects of dif-ferent corroded rough surfaces can be accurately predicted.The numerical and analytical results show that the echo signal amplitude of the micro-crack decreases significantly with an increase in roughness,whereas the noise ampli-tude slightly increases.Moreover,the effect of the rough front surface on the echo signal of the micro-crack is greater than that of the rough back surface.When the root-mean-square(RMS)height of the surface microtopography is less than 15μm,the two rough surfaces have less influence on the echo signals detected by a focused transducer with a frequency of 5 MHz and diameter of 6 mm.A method for predicting and evaluating the detection accuracy of micro-cracks under different rough surfaces is proposed by combining the theoretical model and a finite element simulation.Then,a series of rough surface samples containing different micro-cracks are fabricated to experimentally validate the evaluation method.