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固溶处理对Mg-1.5Er-1.0Zn-0.3Zr合金组织和性能的影响
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作者 贺俊光 冯武云 +2 位作者 文九巴 龚圆 郑向阳 《材料热处理学报》 CAS CSCD 北大核心 2024年第9期124-133,共10页
采用光学显微镜(OM)、扫描电镜(SEM)、电化学实验和拉伸实验等研究固溶处理对Mg-1.5Er-1.0Zn-0.3Zr合金组织、耐蚀性能和力学性能的影响。结果表明:铸态合金的显微组织主要由α-Mg基体、Mg_(3)Er_(2)Zn_(3)、Mg_(24)Er_(5)和MgErZn_(2)... 采用光学显微镜(OM)、扫描电镜(SEM)、电化学实验和拉伸实验等研究固溶处理对Mg-1.5Er-1.0Zn-0.3Zr合金组织、耐蚀性能和力学性能的影响。结果表明:铸态合金的显微组织主要由α-Mg基体、Mg_(3)Er_(2)Zn_(3)、Mg_(24)Er_(5)和MgErZn_(2)相组成。经固溶处理后,第二相逐渐溶解在镁基体中,且合金平均晶粒尺寸有不同程度的增大。合金经460℃固溶处理8 h后的综合性能较好,其腐蚀速率为(0.44±0.051)mm/y,抗拉强度、屈服强度和伸长率分别为(227.97±4.84)MPa、(137.96±5.03)MPa和(14.42±1.06)%。 展开更多
关键词 mg-1.5Er-1.0zn-0.3zr合金 固溶处理 腐蚀性能
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固溶态Mg-3Zn-Y-1.5Nd-0.4Zr合金组织演变及力学性能优化
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作者 董宇星 任聪林 +1 位作者 许春香 张金山 《热加工工艺》 北大核心 2023年第2期124-128,共5页
研究了固溶处理(T4处理)对Mg-3Zn-1Y-1.5Nd-0.4Zr合金的组织演变与力学性能的影响。采用X射线衍射,扫面电子显微镜和能谱仪对铸态及固溶态Mg-3Zn-1Y-1.5Nd-0.4Zr合金的微观组织进行分析,采用单轴拉伸测试和显微硬度测试对铸态及固溶态Mg... 研究了固溶处理(T4处理)对Mg-3Zn-1Y-1.5Nd-0.4Zr合金的组织演变与力学性能的影响。采用X射线衍射,扫面电子显微镜和能谱仪对铸态及固溶态Mg-3Zn-1Y-1.5Nd-0.4Zr合金的微观组织进行分析,采用单轴拉伸测试和显微硬度测试对铸态及固溶态Mg-3Zn-1Y-1.5Nd-0.4Zr合金的力学性能进行测试。结果表明,铸态Mg-3Zn-1Y-1.5Nd-0.4Zr合金晶界处连续的第二相在固溶过程中发生断裂并球化现象,其综合力学性能先增加后减小。Mg-3Zn-1Y-1.5Nd-0.4Zr合金在490℃下保温26 h时力学性能最佳,其极限抗拉强度,屈服强度和伸长率分别为278.20 MPa,226.79 MPa和13.53%。固溶处理过程中,Mg-3Zn-1Y-1.5Nd-0.4Zr合金因为第二相发生球化现象,第二相中溶质元素的溶解产生固溶强化,使固溶态Mg-3Zn-1Y-1.5Nd-0.4Zr合金的综合力学性能得到提高。 展开更多
关键词 mg-3zn-1Y-1.5Nd-0.4zr合金 固溶处理 组织演变 力学性能
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时效温度对Zn-1.5Cu-1.2Mg-0.2Zr合金组织与耐蚀性的影响
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作者 程军权 周一文 +6 位作者 王红星 张炎 许殷泽 赵贵崔 顾沈逸 丁仁旻 蒋兖卿 《材料热处理学报》 CAS CSCD 北大核心 2023年第4期95-101,共7页
采用金属型铸造的方法制备了Zn-1.5Cu-1.2Mg-0.2Zr锌合金,利用扫描电镜、能谱仪、X射线衍射、电化学工作站和浸泡实验等研究了不同温度时效处理对其微观组织和耐蚀性的影响。结果表明:铸态锌合金的微观组织主要由η相(含Cu的Zn固溶体)、... 采用金属型铸造的方法制备了Zn-1.5Cu-1.2Mg-0.2Zr锌合金,利用扫描电镜、能谱仪、X射线衍射、电化学工作站和浸泡实验等研究了不同温度时效处理对其微观组织和耐蚀性的影响。结果表明:铸态锌合金的微观组织主要由η相(含Cu的Zn固溶体)、η+Mg_(2)Zn_(11)共晶体和少量的Zn-Zr化合物组成;随时效温度的升高,合金η相晶粒内析出的片状第二相数量先增加后减少,腐蚀速率呈先降低后增加的趋势;220℃时效处理的锌合金腐蚀速率最小,自腐蚀电流密度和模拟体液浸泡腐蚀速率分别为5.23μA·cm^(-2)和0.053 mm·year^(-1),这可能是由于220℃时效处理后合金η相晶粒内析出的片状第二相的数量最多且分布均匀。 展开更多
关键词 zn-1.5Cu-1.2mg-0.2zr锌合金 时效温度 腐蚀速率
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Al-9.0Zn-2.5Mg-1.5Cu-0.15Zr-0.4Sc合金的等温淬火性能 被引量:1
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作者 戴晓元 熊超宇 张浩 《材料热处理学报》 EI CAS CSCD 北大核心 2019年第8期31-38,共8页
采用盐浴分级淬火的实验方法,通过测试Al-9.0Zn-2.5Mg-1.5Cu-0.15Zr-0.4Sc铝合金的电导率与硬度,绘制了其时间—温度—转换率(TTT)曲线和时间—温度—性能(TTP)曲线,利用差示扫描量热法(DSC),X射线衍射(XRD),透射电镜(TEM)等观察分析了... 采用盐浴分级淬火的实验方法,通过测试Al-9.0Zn-2.5Mg-1.5Cu-0.15Zr-0.4Sc铝合金的电导率与硬度,绘制了其时间—温度—转换率(TTT)曲线和时间—温度—性能(TTP)曲线,利用差示扫描量热法(DSC),X射线衍射(XRD),透射电镜(TEM)等观察分析了合金等温过程中的组织变化,结合Johnson-Mehl-Avrami方程研究了合金等温过程中的相变动力学。研究表明:随着保温时间的延长,淬火态合金的电导率呈上升趋势,时效态硬度呈下降趋势;Al-9.0Zn-2.5Mg-1.5Cu-0.15Zr-0.4Sc铝合金的TTT曲线和TTP曲线的鼻尖温度在330℃附近;合金的淬火温度敏感区间为270~390℃。实验铝合金过饱和固溶体在330℃等温处理时快速分解,第二相脱溶析出速率达到最高,较大的相变驱动力和较高的扩散速率是合金第二相快速析出和长大的主要原因。合金固溶后,在淬火敏感区间之外可适当降低冷却速率,这样不仅可以保持合金的力学性能,还可降低合金的内应力。 展开更多
关键词 Al-9.0zn-2.5mg-1.5Cu-0.15zr-0.4Sc合金 TTT曲线 TTP曲线 淬火敏感性
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固溶处理对挤压态Mg-1.5Zn-0.5Y-0.5Zr合金耐蚀及力学性能的影响
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作者 陈军修 杨洋 +2 位作者 展杰 许玉 孙俭恒 《常州大学学报(自然科学版)》 CAS 2023年第3期1-7,共7页
为提高挤压态Mg-1.5Zn-0.5Y-0.5Zr合金的耐蚀性能,研究了不同固溶温度对其耐蚀和力学性能的影响,通过微观组织观察、电化学测试、体外浸泡实验、拉伸实验研究了固溶处理后样品的微观组织与性能。结果表明,固溶处理后合金中的W相减少,耐... 为提高挤压态Mg-1.5Zn-0.5Y-0.5Zr合金的耐蚀性能,研究了不同固溶温度对其耐蚀和力学性能的影响,通过微观组织观察、电化学测试、体外浸泡实验、拉伸实验研究了固溶处理后样品的微观组织与性能。结果表明,固溶处理后合金中的W相减少,耐蚀性能提高,但当温度达到550℃时,会进一步造成晶粒粗化,降低了合金的耐蚀性能。合金的强度和塑性随着固溶温度的升高而降低。综合固溶处理后合金的耐蚀和力学性能,推荐500℃为最佳固溶处理温度。 展开更多
关键词 mg-1.5zn-0.5Y-0.5zr合金 固溶处理 微观组织 耐蚀性能 力学性能
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退火温度对挤压态Mg-1.5Zn-0.4Zr合金组织和性能的影响 被引量:1
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作者 鲍文科 高世阳 +3 位作者 魏文庆 刘均波 马海健 岳中政 《热加工工艺》 北大核心 2020年第22期129-131,共3页
采用OM、拉伸试验、浸泡腐蚀试验等研究了160~280℃退火对挤压态Mg-1.5Zn-0.4Zr合金组织与性能的影响。结果表明:随着退火温度的升高,Mg-1.5Zn-0.4Zr合金晶粒先减小后增大。200℃退火合金晶粒基本为细小等轴晶,尺寸均匀。与挤压态Mg-1.5... 采用OM、拉伸试验、浸泡腐蚀试验等研究了160~280℃退火对挤压态Mg-1.5Zn-0.4Zr合金组织与性能的影响。结果表明:随着退火温度的升高,Mg-1.5Zn-0.4Zr合金晶粒先减小后增大。200℃退火合金晶粒基本为细小等轴晶,尺寸均匀。与挤压态Mg-1.5Zn-0.4Zr合金相比,不同温度退火合金的强度均有所降低,伸长率、耐腐蚀性均有所提高。200℃退火合金的伸长率、耐腐蚀性最佳,强度也处在较高水平,为Mg-1.5Zn-0.4Zr合金的最佳退火温度。 展开更多
关键词 mg-1.5zn-0.4zr合金 退火 显微组织 力学性能 耐腐蚀性
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Microstructure and mechanical property of a high-strength Mg-10Gd-6Y-1.5Zn-0.5Zr alloy prepared by multi-pass equal channel angular pressing 被引量:12
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作者 Huan Liu He Huang +4 位作者 Xiaowei Yang Cheng Li Jingli Yan Jinghua Jiang Aibin Ma 《Journal of Magnesium and Alloys》 SCIE EI CAS 2017年第2期231-237,共7页
In this work,a high-strength Mg–10Gd–6Y–1.5Zn–0.5Zr(wt.%)alloy was fabricated by successive multi-pass equal channel angular pressing(ECAP).The microstructure and mechanical property of as-cast and ECAP alloys wer... In this work,a high-strength Mg–10Gd–6Y–1.5Zn–0.5Zr(wt.%)alloy was fabricated by successive multi-pass equal channel angular pressing(ECAP).The microstructure and mechanical property of as-cast and ECAP alloys were systematically researched by X-ray diffractometer,scanning electron microscopy,transmission electron microscopy and compression test.The results show that the microstructure of as-cast alloy consists ofα-Mg grains,Mg24Y5 networks,18R blocks,fine 14H lamellas,and fewY-rich particles.After 8 passes ECAP,dynamic recrystallization ofα-Mg is developed and their average grain size decreases to about 1μm.The network Mg_(24)Y_(5) phase at grain boundaries is broken into small particles with average diameter lower than 0.5μm.Moreover,18R blocks are kinked and delaminated,or broken into small particles and blended with Mg24Y5 particles.14H lamellas grow gradually or are dynamically precipitated within certainα-Mg grains.Compression tests indicate that 8p ECAP alloy exhibits excellent mechanical property with compressive strength of 537 MPa and fracture strain of 17.0%.The significant improvement for both strength and ductility of deformed alloy could be ascribed to DRX grains,refined Mg24Y5 particles,18R kinking and dynamical precipitation of 14H. 展开更多
关键词 mg-10Gd-6Y-1.5zn-0.5zr LPSO phase Equal channel angular pressing Compression strength Fracture strain
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Effects of Ce on microstructure of semi-continuously cast Mg-1.5Zn-0.2Zr magnesium alloy ingots 被引量:2
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作者 赵凯阳 彭晓东 +3 位作者 谢卫东 魏群义 杨艳 魏国兵 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2010年第B07期324-330,共7页
Mg-1.5Zn-0.2Zr-xCe (x=0, 0.1, 0.3, 0.5, mass fraction, %) alloys were prepared by conventional semi-continuous casting. The effect of rare earth Ce on the microstructure of Mg-1.5Zn-0.2Zr-xCe alloys was studied and th... Mg-1.5Zn-0.2Zr-xCe (x=0, 0.1, 0.3, 0.5, mass fraction, %) alloys were prepared by conventional semi-continuous casting. The effect of rare earth Ce on the microstructure of Mg-1.5Zn-0.2Zr-xCe alloys was studied and the distribution of Ce was analyzed by optical microscopy (OM), X-ray diffractometry (XRD) and scanning electron microscopy (SEM). The results indicate that Ce element exists in the form of Mg12Ce phase and has an obvious refining effect on the microstructure of test alloys. As the Ce content increases, the grain size reduces, the grain boundaries turn thinner, and the distribution of Mg12Ce precipitates becomes more and more dispersed. The Mg-1.5Zn-0.2Zr alloy with 0.3%Ce has the best refinement effect. From center to periphery of the ingot, the amount of granular precipitates in the grain reduces. In longitudinal section of the ingot, some relative long columnar grains appear. 展开更多
关键词 mg-1.5zn-0.2zr alloy CE semi-continuous casting REFINEMENT
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Microstructure and mechanical properties of Mg-3.0Nd-0.4Zn-0.4Zr magnesium alloy 被引量:2
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作者 L.H.Wen Z.S.Ji +1 位作者 M.L.Hu H.Y.Ning 《Journal of Magnesium and Alloys》 SCIE EI CAS 2014年第1期85-91,共7页
Mg-3.0Nd-0.4Zn-0.4Zr magnesium alloy were prepared by cast-extruding and chip-extruding.Microstructure,tensile and creep properties of the alloy were investigated.The results show that the alloy exhibit particle dynam... Mg-3.0Nd-0.4Zn-0.4Zr magnesium alloy were prepared by cast-extruding and chip-extruding.Microstructure,tensile and creep properties of the alloy were investigated.The results show that the alloy exhibit particle dynamic recrystallization during extrusion.The cast extruded-T6 rods at room temperature have a highest tensile strength of 258.5 MPa and a highest yield strength of 135.7 MPa.With the increase of test temperature,the strength of the alloy declines and the elongation increases.At 473 K,creep strain in the primary creep stage increases with increasing the creep stresses.Under 110 MPa,time spent during primary creep decreases with increasing the test temperatures.Stress exponent and creep activation energy of the alloy are 4.4 and 104 kJ/mol,respectively.Creep of the alloy can be controlled by dislocation climb mechanism.The morphology of the fracture surfaces was examined by employing scanning electron microscope. 展开更多
关键词 mg-3.0Nd-0.4zn-0.4zr alloy Hot extrusion MICROSTRUCTURE PROPERTIES Fracture behavior
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Effects of heat treatment on microstructure and mechanical properties of Mg-6Zn-4Sm-0.4Zr alloy 被引量:1
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作者 Xiao-feng Huang Yu Zhang +3 位作者 Feng Guo Jian-chang Yang Ying Ma Yuan Hao 《China Foundry》 SCIE 2018年第2期103-109,共7页
A new rare earth magnesium alloy(Mg-6 Zn-4 Sm-0.4 Zr, wt.%) was prepared by permanent mould casting. The microstructure and mechanical properties of the alloy sample in as-cast and various heat treatment situations we... A new rare earth magnesium alloy(Mg-6 Zn-4 Sm-0.4 Zr, wt.%) was prepared by permanent mould casting. The microstructure and mechanical properties of the alloy sample in as-cast and various heat treatment situations were characterized with an optical microscope(OM), X-ray diffractometer(XRD), scanning electron microscope(SEM) equipped with energy dispersive spectroscope(EDS), transmission electron microscope(TEM) and mechanical tests at room temperature, respectively. The experimental results show that the as-cast alloy mainly consists of α-Mg, eutectic Mg_2Zn_3, MgZnSm and Mg_(41)Sm_5. These eutectic phases with continuous or semicontinuous morphology principally distribute along grain boundaries. Almost all the eutectic compounds dissolve in α-Mg and the grains have no obvious growth trend after optimum solution treatment at 490 °C for 18 h. Meanwhile, the ultimate tensile strength(UTS) of 229 MPa and elongation(EL) to rupture of 9.78% can be achieved through the optimal solution treatment, which increase by 37 MPa and 57.74%, respectively, compared with that of the as-cast alloy. Further aging treatments at 200 °C for different durations lead to the conspicuous increment of mechanical properties and prominent age-hardening response. Peak-aged alloy(treated at 200 °C for 12 h) reveals better mechanical properties(UTS 258 MPa, EL 9.42%, hardness 73.4 HV) compared with the same alloy treated in other aging conditions, which is mainly ascribed to precipitated Mg_2Zn_3 and MgZn_2 phases. Fracture analysis demonstrates that the as-cast alloy belongs to inter-granular and cleavage fracture patterns, while the solutionized alloy(treated at 490 °C for 18 h) reveals trans-granular and quasi-cleavage fracture modes. For the peak-aged alloy, the fracture pattern obeys the mixture of trans-granular and cleavage modes. 展开更多
关键词 mg-6zn-4Sm-0.4zr alloy heat treatment microstructure evolution mechanical properties fracture mode
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热处理工艺对Mg-6Zn-2Sm-0.4Zr镁合金显微组织和力学性能的影响 被引量:9
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作者 张玉 黄晓锋 +3 位作者 马振铎 李雅 马颖 郝远 《中国有色金属学报》 EI CAS CSCD 北大核心 2017年第10期1961-1969,共9页
通过在Mg-6Zn合金中添加0.4%Zr和2%Sm(质量分数)制备出一种新型Mg-6Zn-2Sm-0.4Zr合金;利用光学显微镜(OM)、扫描电镜(SEM)及能谱仪(EDS)、X射线衍射仪(XRD)、显微硬度及力学性能测试研究铸造Mg-6Zn-2Sm-0.4Zr合金在铸态、固溶、时效处... 通过在Mg-6Zn合金中添加0.4%Zr和2%Sm(质量分数)制备出一种新型Mg-6Zn-2Sm-0.4Zr合金;利用光学显微镜(OM)、扫描电镜(SEM)及能谱仪(EDS)、X射线衍射仪(XRD)、显微硬度及力学性能测试研究铸造Mg-6Zn-2Sm-0.4Zr合金在铸态、固溶、时效处理下的显微组织和力学性能的变化。结果表明:合金铸态组织主要由基体α-Mg、晶界处呈连续或半连续分布的(α-Mg+Mg_2Zn_3+Mg_(41)Sm_5)共晶和晶内孤立的点状相组成。合金在440和450℃固溶12~36 h时间范围内,随着时间和温度的增加,固溶效果逐渐增强。当在450℃固溶28 h时获得了较好的显微组织,抗拉强度为230 MPa,伸长率为9.58%。随后经200℃时效6~48 h后,合金的力学性能明显提高,时效强化效应随时间的延长呈先增加后减小的趋势,其中时效12 h时同时出现了抗拉强度和伸长率的峰值258 MPa和14.43%,比铸态的分别提高44 MPa和90.80%。 展开更多
关键词 mg-6zn-2Sm-0.4zr镁合金 固溶处理 时效处理 显微组织 力学性能
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Effect of heat treatment on microstructures and mechanical properties of sand-cast Mg-4Y-2Nd-1Gd-0.4Zr magnesium alloy 被引量:7
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作者 刘志杰 吴国华 +2 位作者 刘文才 庞松 丁文江 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2012年第7期1540-1548,共9页
Influence of heat treatment on the microstructures and mechanical properties of sand-cast Mg-4Y-2Nd-1Gd-0.4Zr magnesium alloy was investigated,and the tensile fracture mechanisms of the studied alloys under different ... Influence of heat treatment on the microstructures and mechanical properties of sand-cast Mg-4Y-2Nd-1Gd-0.4Zr magnesium alloy was investigated,and the tensile fracture mechanisms of the studied alloys under different conditions were also discussed.The results show that the optimum T4 and T6 heat treatment conditions for the as-cast Mg-4Y-2Nd-1Gd-0.4Zr alloy are 525°C,8 h and(525°C,8 h)+(225°C,16 h),respectively,with regard to the microstructure observation,DSC heating curve and mechanical properties.The hardness,yield strength,ultimate tensile strength and elongation of the Mg-4Y-2Nd-1Gd-0.4Zr alloy treated by optimum T6 heat treatment are HV91,180 MPa,297 MPa and 7.4%,respectively.Moreover,the Mg-4Y-2Nd-1Gd-0.4Zr alloys under different heat treatment conditions exhibit different tensile fracture modes. 展开更多
关键词 {0.4Y-2Nd-1Gd-0.4zr alloy sand-casting heat treatment mechanical property
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Microstructures and mechanical properties of as-extruded and heat treated Mg-6Zn-1Mn-4Sn-1.5Nd alloy 被引量:3
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作者 胡光山 张丁非 +3 位作者 董于凤 谌夏 蒋璐瑶 潘复生 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2015年第5期1439-1445,共7页
The microstructures and mechanical properties of Mg-6Zn-1Mn-4Sn-1.5Nd alloy subjected to extrusion and T5 treatment were investigated using optical microscopy(OM), X-ray diffractometer(XRD), scanning electron micr... The microstructures and mechanical properties of Mg-6Zn-1Mn-4Sn-1.5Nd alloy subjected to extrusion and T5 treatment were investigated using optical microscopy(OM), X-ray diffractometer(XRD), scanning electron microscopy(SEM), electron back scattered diffraction(EBSD), transmission electron microscopy(TEM), hardness tests and uniaxial tensile tests. The results showed that the as-cast alloy consisted of α(Mg), Mn, Mg7Zn3, Mg2 Sn and Mg Sn Nd phases. Dynamic recrystallization has completed during the extrusion process and the average grain size was 7.2 μm. After T5 treatment, the strength increased obviously, the yield strength and ultimate tensile strength of as-extruded alloy were increased by 94 and 34 MPa, respectively. Microstructure characterization revealed that the improvement of strength was determined by the high number density of β′1 rods. 展开更多
关键词 mg-6zn-1Mn-4Sn-1.5Nd alloy extrusion T5 heat treatment MICROSTRUCTURES mechanical properties
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添加Sm对不同尺寸Mg-6Zn-0.4Zr镁合金坯料非枝晶组织演变的影响 被引量:1
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作者 张玉 黄晓锋 +3 位作者 马颖 闫峰云 李元东 郝远 《材料导报》 EI CAS CSCD 北大核心 2018年第8期1283-1288,共6页
采用半固态等温热处理法对添加0%、2%(质量分数)稀土SmΦ10mm和Φ20mm的Mg-6Zn-0.4Zr合金坯料非枝晶组织演变进行研究。结果表明,未添加Sm的两种尺寸合金坯料的半固态组织都存在明显的尺寸效应。从试样的边缘到芯部,固相颗粒尺寸由小逐... 采用半固态等温热处理法对添加0%、2%(质量分数)稀土SmΦ10mm和Φ20mm的Mg-6Zn-0.4Zr合金坯料非枝晶组织演变进行研究。结果表明,未添加Sm的两种尺寸合金坯料的半固态组织都存在明显的尺寸效应。从试样的边缘到芯部,固相颗粒尺寸由小逐渐变大,圆整度趋于恶化,液相逐渐减少;此外,随着坯料尺寸增大,由边缘到芯部的半固态组织的差异也增大。添加Sm的两种合金坯料经等温热处理后,固相颗粒的尺寸效应基本消除。固相颗粒尺寸整体变得均匀且细小,同时颗粒圆整度趋于完美,适宜触变成形要求。此外,添加2%的Sm使合金的非枝晶组织演变进程加快。 展开更多
关键词 mg-6zn-0.4zr镁合金 Sm添加 等温热处理 尺寸效应 半固态组织
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Effect of heat treatment on microstructures and mechanical properties of high vacuum die casting Mg-8Gd-3Y-0.4Zr magnesium alloy 被引量:7
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作者 王栀沁 张彬 +4 位作者 李德江 Robert FRITZSCH 曾小勤 Hans J.ROVEN 丁文江 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2014年第12期3762-3768,共7页
The microstructure, the content of compounds, mechanical properties and fracture behavior of high vacuum die casting Mg-8Gd-3Y-0.4Zr alloy (mass fraction, %) under T4 condition and T6 condition were investigated. Th... The microstructure, the content of compounds, mechanical properties and fracture behavior of high vacuum die casting Mg-8Gd-3Y-0.4Zr alloy (mass fraction, %) under T4 condition and T6 condition were investigated. The microstructure for the as-cast Mg-8Gd-3Y-0.4Zr alloy mainly consists ofα-Mg and eutectic Mg24(Gd,Y)5 compound. After solution treatment, the eutectic compounds dissolve massively into the Mg matrix. The main composition of solution-treated alloys is supersaturated α-Mg and cuboid-shaped phase. The T4 heat treated samples have increasing cuboidal particles with the increase of heat treatment temperature, which turn out good mechanical properties. The optimum T4 heat treatment for high vacuum die cast Mg-8Gd-3Y-0.4Zr alloy is 475 ℃, 2 h according to microstructure results. The optimum ultimate strength and elongation of solution-treated Mg-8Gd-3Y-0.4Zr alloy are 222.1 MPa and 15.4%, respectively. The tensile fracture mode of the as-cast, and T6 heat treated alloys is transgranular quasi-cleavage fracture. 展开更多
关键词 mg-8Gd-3Y-0.4zr alloy heat treatment MICROSTRUCTURE mechanical property fracture behavior
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挤压速度对Mg-2Y-1Zn-0.4Zr合金组织演变、力学性能和动态腐蚀行为的影响 被引量:5
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作者 任聪林 宽军 +2 位作者 曹鑫 许春香 张金山 《材料热处理学报》 EI CAS CSCD 北大核心 2020年第9期117-125,共9页
采用光学显微镜、扫描电镜、能谱仪、力学性能测试和电化学测试等研究了挤压速度对铸态Mg-2Y-1Zn-0.4Zr镁合金显微组织、力学性能和腐蚀性能的影响。结果表明:挤压速度对Mg-2Y-1Zn-0.4Zr镁合金的显微组织、力学性能和腐蚀性能都有显著... 采用光学显微镜、扫描电镜、能谱仪、力学性能测试和电化学测试等研究了挤压速度对铸态Mg-2Y-1Zn-0.4Zr镁合金显微组织、力学性能和腐蚀性能的影响。结果表明:挤压速度对Mg-2Y-1Zn-0.4Zr镁合金的显微组织、力学性能和腐蚀性能都有显著影响。随着挤压速度的增加,合金的平均晶粒尺寸增大,动态再结晶晶粒的体积分数先增加后减小。在60 mm/min的挤压速度下,合金的动态再结晶程度最高,并且组织中均匀分布着微米级的W-相,综合性能最佳,屈服强度、抗拉强度和伸长率分别为327 MPa、322 MPa和24.9%。 展开更多
关键词 mg-2Y-1zn-0.4zr合金 显微组织 挤压速度 动态再结晶
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Effects of yttrium on recrystallization and grain growth of Mg-4.9Zn-0.7Zr alloy 被引量:4
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作者 方西亚 易丹青 +3 位作者 罗文海 王斌 张小娟 郑峰 《Journal of Rare Earths》 SCIE EI CAS CSCD 2008年第3期392-397,共6页
Recrystallization and grain growth in Mg-4.9Zn-0.7Zr and Mg-4.9Zn-0.9Y-0.7Zr alloys as a function of temperature on deformation were investigated with regards to hot rolling and annealing. The influence of yttrium add... Recrystallization and grain growth in Mg-4.9Zn-0.7Zr and Mg-4.9Zn-0.9Y-0.7Zr alloys as a function of temperature on deformation were investigated with regards to hot rolling and annealing. The influence of yttrium addition on the microstructure was examined by X-ray diffraction (XRD), optical microscopy (OM), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The results indicated that yttrium addition promoted nucleation of recrystallization during hot rolling process. The grain size of Mg-4.9Zn-0.7Zr alloy samples grew significantly with annealing temperature (300-400 ℃) and holding time (0-120 min), while the microstructure of the alloy with yttrium addition remained unchanged and fine. The activation energy of grain boundary migration for Mg-4.9Zn-0.9Y-0.7Zr alloy samples (56.34 kJ/mol) was higher than that for Mg-4.9Zn-0.7Zr (42.66 kJ/mol) owing to the pinning effect of Y-containing particles. The proposed growth models of recrysta/lized grains for the two studied alloys conformed well to E. Robert's grain-growth equation. Besides, the ultimate strength and yield strength of the alloys with yttrium addition were improved with good plasticity. 展开更多
关键词 mg-4.9zn-0.9Y-0.7zr alloy bot-rolling RECRYSTALLIZATION grain growth rare earths
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Grain refinement impact on the mechanical properties and wear behavior of Mg-9Gd-3Y-2Zn-0.5Zr alloy after decreasing temperature reciprocating upsetting-extrusion 被引量:3
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作者 Wenlong Xu Jianmin Yu +5 位作者 Leichen Jia Chang Gao Zhan Miao Guoqin Wu Guojun Li Zhimin Zhang 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2022年第12期3506-3519,共14页
Based on the deforming technique of severe plastic deformation(SPD), the grain refinement of a Mg-9Gd-3Y-2Zn-0.5Zr alloy treated with decreasing temperature reciprocating upsetting-extrusion(RUE) and its influence on ... Based on the deforming technique of severe plastic deformation(SPD), the grain refinement of a Mg-9Gd-3Y-2Zn-0.5Zr alloy treated with decreasing temperature reciprocating upsetting-extrusion(RUE) and its influence on the mechanical properties and wear behavior of the alloy were studied. The RUE process was carried out for 4 passes in total, starting at 0 ℃ and decreasing by 10 ℃ for each pass. The results showed that as the number of RUE passes increased, the grain refinement effect was obvious, and the second phase in the alloy was evenly distributed. Room temperature tensile properties of the alloy and the deepening of the RUE degree showed a positive correlation trend, which was due to the grain refinement, uniform distribution of the second phase and texture weakening. And the microhardness of the alloy showed that the microhardness of RUE is the largest in 2 passes. The change in microhardness was the result of dynamic competition between the softening effect of DRX and the work hardening effect. In addition, the wear resistance of the alloy showed a positive correlation with the degree of RUE under low load conditions. When the applied load was higher, the wear resistance of the alloy treated with RUE decreased compared to the initial state alloy. This phenomenon was mainly due to the presence of oxidative wear on the surface of the alloy, which could balance the positive contribution of severe plastic deformation to wear resistance to a certain extent. 展开更多
关键词 mg-9Gd-3Y-2zn-0.5zr alloy Reciprocating upsetting-extrusion Grain refinement Texture Mechanical properties Wear behavior
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Microstructure and Mechanical Behavior of Squeeze Casting Mg-8Gd-2Y-0.4Zr Alloy 被引量:1
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作者 吴文云 汪东红 +1 位作者 DENG Peiran CAO Yanggen 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2018年第2期466-471,共6页
Microstructure and mechanical behavior of the squeeze-casting and squeeze-casting plus T6 heat-treated Mg-8 Gd-2 Y-0.4 Zr magnesium alloys at room and elevated temperatures were investigated. The experimental results ... Microstructure and mechanical behavior of the squeeze-casting and squeeze-casting plus T6 heat-treated Mg-8 Gd-2 Y-0.4 Zr magnesium alloys at room and elevated temperatures were investigated. The experimental results showed that the T6 treated alloy aged at slightly high temperature exhibited good comprehensive strength and ductility. However, the strength of the tested alloys was not sensitive to the change of tensile temperature, i e, the yield strength and ultimate tensile strength did not decrease significantly with increasing tensile temperature, while the ductility increased greatly. In addition, the squeeze-casting alloy exhibited predominant intergranular fracture accompanied by minor transgranular rupture, and the tensile fracture mode for the T6 treated alloy had typical transgranular cleavage fracture. 展开更多
关键词 squeeze-casting magnesium alloy mg-8Gd-2Y-0.4zr mechanical behavior
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热处理过程中压力对Mg-14Gd-1Zn-0.4Zr合金组织与力学性能的影响
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作者 吴海 王阳阳 +4 位作者 张旻 杨力祥 董喜旺 华溪如 肖旅 《特种铸造及有色合金》 CAS 北大核心 2024年第9期1232-1236,共5页
针对铸造稀土镁合金固溶处理过程中普遍存在的合金元素充分固溶与晶粒长大间的矛盾,从压力角度探索其对合金元素固溶过程的影响。对比研究了真空与常压固溶处理后Mg-14Gd-1Zn-0.4Zr合金的组织与力学性能,以及峰时效态的力学性能,并讨论... 针对铸造稀土镁合金固溶处理过程中普遍存在的合金元素充分固溶与晶粒长大间的矛盾,从压力角度探索其对合金元素固溶过程的影响。对比研究了真空与常压固溶处理后Mg-14Gd-1Zn-0.4Zr合金的组织与力学性能,以及峰时效态的力学性能,并讨论了压力对原子固溶过程的影响机制。结果表明,Mg-14Gd-1Zn-0.4Zr合金铸态组织主要由α-Mg、(Mg,Zn)_(3)Gd、14H型LPSO相组成。常压480℃×20 h固溶处理后LPSO相消失,有少量(Mg,Zn)_(3)Gd残留。常压500℃×20 h与真空480℃×20 h固溶处理后,LPSO相均消失且基本无(Mg,Zn)_(3)Gd相残留,但真空条件下晶粒未显著长大,强塑性均有所提升;二者在225℃时效处理的峰时效时间均为24 h,后者的抗拉强度与伸长率提升明显,抗拉强度为(360.5±1.2)MPa,屈服强度为(234.6±0.8)MPa,伸长率为(5.2±0.3)%。当压力降低至真空时,合金原子的扩散系数增加,提高了固溶效率;在较低固溶温度下也可实现Gd、Zn原子固溶,同时减缓了晶粒长大,因此促进了合金综合强塑性提升。 展开更多
关键词 压力 热处理 mg-14Gd-1zn-0.4zr合金 力学性能
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