The effects of RE on the microstrcture of as-cast Mg-8Zn-4Al magnesium alloys were investigated. The results show that the solidification range of Mg-8Zn-4Al-xRE alloys increases with RE additions. A binary eutectic r...The effects of RE on the microstrcture of as-cast Mg-8Zn-4Al magnesium alloys were investigated. The results show that the solidification range of Mg-8Zn-4Al-xRE alloys increases with RE additions. A binary eutectic reaction can arise and produce a new phase (Mg:Al:Zn:RE) and the temperature of phase transformation point of the new phase is 412.85 C. In Mg-8Zn-4Al-1.5RE alloy, a small amount of Mg:Al:Zn:RE phase and ε phases are found besides a(Mg),φand r phases. Also microstructures of Mg-8Zn-4Al alloys can be refined by addition of 1.5% RE obviously.展开更多
Fine-grained Mg-6Zn-4Y alloy was prepared by an ingot metallurgy process with hot extrusion at 300 ℃.The microstructure was studied by XRD,OM,SEM and TEM,and the tensile properties were tested at room temperature.The...Fine-grained Mg-6Zn-4Y alloy was prepared by an ingot metallurgy process with hot extrusion at 300 ℃.The microstructure was studied by XRD,OM,SEM and TEM,and the tensile properties were tested at room temperature.The results show that the alloy is composed of α-Mg and W-phase.The microstructure of the as-extruded alloy has a bimodal grain size distribution.The fine grains with the mean size of 1.2 μm are formed by dynamic recrystallization.The coarse grains(about 23% in area fraction) are unrecrystallized regions which are elongated along extrusion direction.The engineering stress—strain curve shows a pronounced yield point.The ultimate tensile strength,yield strength,and elongation are(371±10) MPa,(350±5) MPa and(7±2)%,respectively.The high strengths are attributed to the fine-grained matrix structure enhanced by W-phase particles,nano-scaled precipitates,and strong basal plane texture.展开更多
In order to investigate the effect of extrusion on Mg-4Zn-1Y alloy, microstructure and mechanical properties were analyzed by optical microscopy(OM), scanning electron microscopy(SEM), transmission electron micros...In order to investigate the effect of extrusion on Mg-4Zn-1Y alloy, microstructure and mechanical properties were analyzed by optical microscopy(OM), scanning electron microscopy(SEM), transmission electron microscopy(TEM), X-ray diffraction(XRD), energy dispersive spectrum(EDS) and tensile testing.The results indicated that the microstructure was obviously refined by extrusion and dynamic recrystallization.The second phases were dynamic precipitated and distributed more dispersively through extrusion.W-Phases(Mg3Zn3Y2) were twisted and broken, while I-Phases(Mg3Zn6Y) were spheroidized by deformation.Twin bands were formed to achieve the large deformation and hinder the slip of dislocations effectively to improve tensile properties.The tensile strength and elongation of extruded Mg-4Zn-1Y alloy were 254.94 MPa and 17.9% respectively which were improved greatly compared with those of as-cast alloy.The strengthening mechanisms of the extruded alloy were mainly fine-grain strengthening and distortion strengthening.展开更多
文摘The effects of RE on the microstrcture of as-cast Mg-8Zn-4Al magnesium alloys were investigated. The results show that the solidification range of Mg-8Zn-4Al-xRE alloys increases with RE additions. A binary eutectic reaction can arise and produce a new phase (Mg:Al:Zn:RE) and the temperature of phase transformation point of the new phase is 412.85 C. In Mg-8Zn-4Al-1.5RE alloy, a small amount of Mg:Al:Zn:RE phase and ε phases are found besides a(Mg),φand r phases. Also microstructures of Mg-8Zn-4Al alloys can be refined by addition of 1.5% RE obviously.
基金Project (50271054) supported by the National Natural Science Foundation of ChinaProject (20070700003) supported by the Doctorate Programs Foundation of Ministry of Education of China+1 种基金Project (102102210031) supported by the Science and Technologies Foundation of Henan Province, ChinaProject (2010A430008) supported by the Natural Science Foundation of Henan Educational Committee of China
文摘Fine-grained Mg-6Zn-4Y alloy was prepared by an ingot metallurgy process with hot extrusion at 300 ℃.The microstructure was studied by XRD,OM,SEM and TEM,and the tensile properties were tested at room temperature.The results show that the alloy is composed of α-Mg and W-phase.The microstructure of the as-extruded alloy has a bimodal grain size distribution.The fine grains with the mean size of 1.2 μm are formed by dynamic recrystallization.The coarse grains(about 23% in area fraction) are unrecrystallized regions which are elongated along extrusion direction.The engineering stress—strain curve shows a pronounced yield point.The ultimate tensile strength,yield strength,and elongation are(371±10) MPa,(350±5) MPa and(7±2)%,respectively.The high strengths are attributed to the fine-grained matrix structure enhanced by W-phase particles,nano-scaled precipitates,and strong basal plane texture.
基金Project supported by General Program of Liaoning Province Committee of Education(L2012035)Liaoning Province Science and Technology Plan(2013201018)Liaoning Province University Innovation Team Support Plan
文摘In order to investigate the effect of extrusion on Mg-4Zn-1Y alloy, microstructure and mechanical properties were analyzed by optical microscopy(OM), scanning electron microscopy(SEM), transmission electron microscopy(TEM), X-ray diffraction(XRD), energy dispersive spectrum(EDS) and tensile testing.The results indicated that the microstructure was obviously refined by extrusion and dynamic recrystallization.The second phases were dynamic precipitated and distributed more dispersively through extrusion.W-Phases(Mg3Zn3Y2) were twisted and broken, while I-Phases(Mg3Zn6Y) were spheroidized by deformation.Twin bands were formed to achieve the large deformation and hinder the slip of dislocations effectively to improve tensile properties.The tensile strength and elongation of extruded Mg-4Zn-1Y alloy were 254.94 MPa and 17.9% respectively which were improved greatly compared with those of as-cast alloy.The strengthening mechanisms of the extruded alloy were mainly fine-grain strengthening and distortion strengthening.