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MnNb_2O_6粉体的水热合成
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作者 庄永勇 蒲永平 +1 位作者 许宁 陈凯 《人工晶体学报》 EI CAS CSCD 北大核心 2010年第B06期127-130,共4页
以Mn(NO3)2溶液和氧化铌凝胶为原料,分别选取HF、HCl、NaOH、NH3·H2O等为矿化剂,采用水热法制备了MnNb2O6微波介质陶瓷粉体,利用XRD、SEM等方法表征了所得粉体的相组成,颗粒尺寸大小等。结果表明:以Mn(NO3)2溶液和Nb2O5·nH2O... 以Mn(NO3)2溶液和氧化铌凝胶为原料,分别选取HF、HCl、NaOH、NH3·H2O等为矿化剂,采用水热法制备了MnNb2O6微波介质陶瓷粉体,利用XRD、SEM等方法表征了所得粉体的相组成,颗粒尺寸大小等。结果表明:以Mn(NO3)2溶液和Nb2O5·nH2O为前驱物在碱性环境条件下200℃反应168h后,可制得平均晶粒尺寸约为24nm的MnNb2O6粉体。将合成的粉体在600℃热处理,制得颗粒尺寸约为300nm,高度分散的MnNb2O6粉体。 展开更多
关键词 微波介质陶瓷 铌酸锰粉体 水热法
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The Structure and Properties of Ag(Nb_(0.8)Ta_(0.2))O_3 Ceramic Doped with MnNb_2O_6
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作者 XIAO Mi JIA Cuiran WANG Xin 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2012年第1期50-53,共4页
The influences of doping of MnNb206 on the structure and dielectric properties of Ag(Nb0.sTa0.2)O3 were illustrated. Ag(Nb0.sTa0.2)O3 samples doped with different amount of preformed MnNb206 (1 mol%, 2 mol%, 3 mo... The influences of doping of MnNb206 on the structure and dielectric properties of Ag(Nb0.sTa0.2)O3 were illustrated. Ag(Nb0.sTa0.2)O3 samples doped with different amount of preformed MnNb206 (1 mol%, 2 mol%, 3 mol%, 4 mol%, 6 mol%, 8 mol%) were prepared by traditional solid-state reaction method and characterized by XRD, SEM and EDS, and the dielectric properties of samples were compared. The experiment results indicated that when the doping amount of MnNb206 was greater than 3 mol%, second phase appeared because of the solid solution limit. The permittivity of the Ag(Nb0.sTa0.2)O3 samples doped with MnNb206 firstly increased and then decreased with the sintering temperature, while the dielectric loss decreased first, and then increased slightly. 1 100 ℃seems to be the most proper sintering temperature for most of the samples. When the amount of MnNb206 is about 3 mol%, the samples have the best dielectric properties, larger permittivity and smaller dielectric loss. 展开更多
关键词 Ag(Nbl-xxTax)O3 mnnb206 dielectric properties DOPE
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