Mo fibers were added to RMC with different mass ratios of resin and hardener to improve its mechanical properties. The influences of fiber surface state and hardener content on interface bonding strength and mechanica...Mo fibers were added to RMC with different mass ratios of resin and hardener to improve its mechanical properties. The influences of fiber surface state and hardener content on interface bonding strength and mechanical properties of RMC were studied, respectively. Furthermore, strain values of typical measuring points on samples of Mo fiber reinforced RMC(MFRRMC) under different loads were obtained by experiments and finite element analysis. The experimental results prove that scrap Mo fibers can improve interface bonding strength and mechanical properties of RMC better than new smooth Mo fibers because of the discharge pits randomly distributed on the surface of scrap fibers. With the decrease of hardener content, not only interface bonding strength between fiber and matrix, but also compression and flexural strength of MFRRMC increase firstly and then decrease. The properties are best while the mass ratio of resin and hardener reaches 4:1. It is indicated that finite element calculation data basically agree with experimental data by comparison of strain values on typical measuring points, which can provide an important intuitive reference for successive study on other mechanical properties of MFRRMC, validating the correctness of simulation method as well.展开更多
Composite reinforced with continuous Mo fiber reinforcement was prepared by pre placing fiber and vacuum casting. The microstructure, concentration and hardness profiles across the interface in as cast and HIPed sampl...Composite reinforced with continuous Mo fiber reinforcement was prepared by pre placing fiber and vacuum casting. The microstructure, concentration and hardness profiles across the interface in as cast and HIPed samples were investigated. The results showed that the interfacial phases formed between Mo fiber and TiAl matrix in both materials. These include two intermetallic phases, ρ (Ti, Mo) 3Al and β (Ti, Mo)Al with a sequence of Mo ρ β γ (or γ+α 2). Boundaries of Mo/ ρ , and ρ/β are smooth, while the β/γ+α 2 interfaces are serrated with the serration parallel to the lamellar laths in the casting condition. The serration disappeared after HIPing, and the boundary between β and γ becomes smooth. The area containing ρ (Ti, Mo) 3Al and β (Ti, Mo)Al is harder than the TiAl matrix and the Mo fiber. Mo atoms appear to diffuse faster in α 2 Ti 3Al than in γ TiAl.展开更多
A novel carbon fiber pretreatment was proposed.Polyacrylonitrile(PAN)-based carbon fibers were first anodized in H3PO4 electrolyte to achieve an active surface,and then coated with Mo-B catalysts by immersed the carbo...A novel carbon fiber pretreatment was proposed.Polyacrylonitrile(PAN)-based carbon fibers were first anodized in H3PO4 electrolyte to achieve an active surface,and then coated with Mo-B catalysts by immersed the carbon fibers in a uniformly dispersed Mo-B sol.The as-treated carbon fibers were then graphitized at 2 400 ℃ for 2 h.The structural changes were characterized by X-ray diffractometry(XRD),Raman spectroscopy,scanning electron microscopy(SEM) and high-resolution transmission electronic microscopy(HRTEM).The results show that much better graphitization can be achieved in the presence of Mo-B,with an interlayer spacing(d002) of 0.335 8 nm and a crystalline size(Lc) of 28 nm.展开更多
The immobilization of titanium dioxide (TiO2) on activated carbon fiber (ACF), (TiO2/ACF), was accomplished by sol-gel-adsorption method followed by calcination at temperatures varying from 300 to 600℃ in an ar...The immobilization of titanium dioxide (TiO2) on activated carbon fiber (ACF), (TiO2/ACF), was accomplished by sol-gel-adsorption method followed by calcination at temperatures varying from 300 to 600℃ in an argon atmosphere. The material properties were determined by scanning electron microscope (SEM), X-ray diffraction (XRD) and nitrogen adsorption. The photodegradation behavior of TiO2 /ACF was investigated in aqueous solutions using phenol and methyl orange (MO) as target pollutants. The effects of calcination temperature, photocatalyst dosage, initial solution pH and radiation time on the degradation of organic pollutants were studied. It was found that organic pollutants could be removed rapidly from water by the TiO2/ACF photocatalyst and the sample calcined at 500℃ exhibited the highest removal efficiency. Kinetics analysis showed that the photocatalytic degradation reaction can be described by a first-order rate equation. In addition, the possibility of cyclic usage of the photocatalyst was also confirmed. Moreover, TiO2 is tightly bound to ACF and can be easily handled and recovered from water. It can therefore be potentially applied for the treatment of water contaminated by organic pollutants.展开更多
A comprehensive study of yarn architecture of two-step rectangle 3D braided composites is presented. Firstly, the braided surface, the shapes of yarns and the intertwining between braider yarns and axial yarns are ana...A comprehensive study of yarn architecture of two-step rectangle 3D braided composites is presented. Firstly, the braided surface, the shapes of yarns and the intertwining between braider yarns and axial yarns are analyzed from experimentation. With the microstructure being defined, three levels of unit cell structure are identified, i.e. large unit cell, second unit cell and minimal unit cell. Secondly, based on the minimal unit cell in the interior and on the boundary of the entire cross-section, the deformations of axial yarns squashed by braider yarns contribute to the increase of the fiber packing factors of axial yarns. Finally, the predicted fiber volume fraction of the composites decreases with the increase of linear density of the braider yarn and the pitch length. Favorable correlations between the predicted and the experimental results are found for six groups of the composites.展开更多
This paper describes a new approach for designing analog predistorters that can compensate for the nonlinear distortion of laser drivers in a radio-over-fiber(RoF) system.In contrast to previous works,this paper analy...This paper describes a new approach for designing analog predistorters that can compensate for the nonlinear distortion of laser drivers in a radio-over-fiber(RoF) system.In contrast to previous works,this paper analyzes the transfer characteristics of CMOS transistors,by combining parallel currents of CMOS transistors in various W/L and negative bias voltages to realize the tunable analog predistortion function.The circuit is fabricated by a standard 0.18μm CMOS technology.The core circuit current consumption is only 15 mA and the entire driver circuit works in a band-pass from 1 ~2.2GHz.Experimental results of two-tone tests have shown that with an analog predistortoer the IIP3 of the laser driver circuit has an improvement of 4.91 dB.展开更多
The active reflector of FAST(five-hundred-meter aperture spherical radio telescope) is supported by a ring beam and a cable-net structure,in which nodes are actively controlled to form series of real-time paraboloids....The active reflector of FAST(five-hundred-meter aperture spherical radio telescope) is supported by a ring beam and a cable-net structure,in which nodes are actively controlled to form series of real-time paraboloids.To ensure the security and stability of the supporting structure,tension must be monitored for some typical cables.Considering the stringent requirements in accuracy and longterm stability,magnetic flux sensor,vibrating wire strain gauge and fiber bragg grating strain gauge are screened for the cable tension monitoring of the supporting cable-net.Specifically,receivers of radio telescopes have strict restriction on electro magnetic interference(EMI) or radio frequency interference(RFI).These three types of sensors are evaluated from the view of EMI/RFI.Firstly,these fundamentals are theoretically analyzed.Secondly,typical sensor signals are collected in the time and analyzed in the frequency domain,which shows the characteristic in the frequency domain.Finally,typical sensors are tested in an anechoic chamber to get the EMI levels.Theoretical analysis shows that Fiber Bragg Grating strain gauge itself will not lead to EMI/RFI.According to GJB151 A,frequency domain analysis and test results show that for the vibrating wire strain gauge and magnetic flux sensor themselves,testable EMI/RFI levels are typically below the background noise of the anechoic chamber.FAST finally choses these three sensors as the monitoring sensors of its cable tension.The proposed study is also a reference to the monitoring equipment selection of other radio telescopes and large structures.展开更多
基金Funded by the National Natural Science Foundation of China(No.5117 5308)the National Science and Technology Major Project of China(No.2012ZX04010032)
文摘Mo fibers were added to RMC with different mass ratios of resin and hardener to improve its mechanical properties. The influences of fiber surface state and hardener content on interface bonding strength and mechanical properties of RMC were studied, respectively. Furthermore, strain values of typical measuring points on samples of Mo fiber reinforced RMC(MFRRMC) under different loads were obtained by experiments and finite element analysis. The experimental results prove that scrap Mo fibers can improve interface bonding strength and mechanical properties of RMC better than new smooth Mo fibers because of the discharge pits randomly distributed on the surface of scrap fibers. With the decrease of hardener content, not only interface bonding strength between fiber and matrix, but also compression and flexural strength of MFRRMC increase firstly and then decrease. The properties are best while the mass ratio of resin and hardener reaches 4:1. It is indicated that finite element calculation data basically agree with experimental data by comparison of strain values on typical measuring points, which can provide an important intuitive reference for successive study on other mechanical properties of MFRRMC, validating the correctness of simulation method as well.
文摘Composite reinforced with continuous Mo fiber reinforcement was prepared by pre placing fiber and vacuum casting. The microstructure, concentration and hardness profiles across the interface in as cast and HIPed samples were investigated. The results showed that the interfacial phases formed between Mo fiber and TiAl matrix in both materials. These include two intermetallic phases, ρ (Ti, Mo) 3Al and β (Ti, Mo)Al with a sequence of Mo ρ β γ (or γ+α 2). Boundaries of Mo/ ρ , and ρ/β are smooth, while the β/γ+α 2 interfaces are serrated with the serration parallel to the lamellar laths in the casting condition. The serration disappeared after HIPing, and the boundary between β and γ becomes smooth. The area containing ρ (Ti, Mo) 3Al and β (Ti, Mo)Al is harder than the TiAl matrix and the Mo fiber. Mo atoms appear to diffuse faster in α 2 Ti 3Al than in γ TiAl.
基金Project(2006CB600903) supported by the National Basic Research Program of China
文摘A novel carbon fiber pretreatment was proposed.Polyacrylonitrile(PAN)-based carbon fibers were first anodized in H3PO4 electrolyte to achieve an active surface,and then coated with Mo-B catalysts by immersed the carbon fibers in a uniformly dispersed Mo-B sol.The as-treated carbon fibers were then graphitized at 2 400 ℃ for 2 h.The structural changes were characterized by X-ray diffractometry(XRD),Raman spectroscopy,scanning electron microscopy(SEM) and high-resolution transmission electronic microscopy(HRTEM).The results show that much better graphitization can be achieved in the presence of Mo-B,with an interlayer spacing(d002) of 0.335 8 nm and a crystalline size(Lc) of 28 nm.
基金Projects(51201134,51271147)supported by the National Natural Science Foundation of ChinaProject(2015JM5181)supported by the Natural Science Foundation of Shaanxi Province,China+1 种基金Project(115-QP-2014)supported by the Research Fund of the State Key Laboratory of Solidification Processing(NWPU),ChinaProject(3102014JCQ01023)supported by the Fundamental Research Funds for the Central Universities,China
基金supported by the Education Bureau Foundationn of Liaoning Province (No. 2008573) the Doctor Foundation of Shenyang Institute of Chemical Technology (No. 20063202)
文摘The immobilization of titanium dioxide (TiO2) on activated carbon fiber (ACF), (TiO2/ACF), was accomplished by sol-gel-adsorption method followed by calcination at temperatures varying from 300 to 600℃ in an argon atmosphere. The material properties were determined by scanning electron microscope (SEM), X-ray diffraction (XRD) and nitrogen adsorption. The photodegradation behavior of TiO2 /ACF was investigated in aqueous solutions using phenol and methyl orange (MO) as target pollutants. The effects of calcination temperature, photocatalyst dosage, initial solution pH and radiation time on the degradation of organic pollutants were studied. It was found that organic pollutants could be removed rapidly from water by the TiO2/ACF photocatalyst and the sample calcined at 500℃ exhibited the highest removal efficiency. Kinetics analysis showed that the photocatalytic degradation reaction can be described by a first-order rate equation. In addition, the possibility of cyclic usage of the photocatalyst was also confirmed. Moreover, TiO2 is tightly bound to ACF and can be easily handled and recovered from water. It can therefore be potentially applied for the treatment of water contaminated by organic pollutants.
基金This research was funded by Scientific Research Fund of National Ministry of Education (00135)
文摘A comprehensive study of yarn architecture of two-step rectangle 3D braided composites is presented. Firstly, the braided surface, the shapes of yarns and the intertwining between braider yarns and axial yarns are analyzed from experimentation. With the microstructure being defined, three levels of unit cell structure are identified, i.e. large unit cell, second unit cell and minimal unit cell. Secondly, based on the minimal unit cell in the interior and on the boundary of the entire cross-section, the deformations of axial yarns squashed by braider yarns contribute to the increase of the fiber packing factors of axial yarns. Finally, the predicted fiber volume fraction of the composites decreases with the increase of linear density of the braider yarn and the pitch length. Favorable correlations between the predicted and the experimental results are found for six groups of the composites.
基金Supported by the National Natural Science Foundation of China(No.61036002)
文摘This paper describes a new approach for designing analog predistorters that can compensate for the nonlinear distortion of laser drivers in a radio-over-fiber(RoF) system.In contrast to previous works,this paper analyzes the transfer characteristics of CMOS transistors,by combining parallel currents of CMOS transistors in various W/L and negative bias voltages to realize the tunable analog predistortion function.The circuit is fabricated by a standard 0.18μm CMOS technology.The core circuit current consumption is only 15 mA and the entire driver circuit works in a band-pass from 1 ~2.2GHz.Experimental results of two-tone tests have shown that with an analog predistortoer the IIP3 of the laser driver circuit has an improvement of 4.91 dB.
基金Supported by the National Natural Science Foundation of China(No.11173035,11273036,11303059)
文摘The active reflector of FAST(five-hundred-meter aperture spherical radio telescope) is supported by a ring beam and a cable-net structure,in which nodes are actively controlled to form series of real-time paraboloids.To ensure the security and stability of the supporting structure,tension must be monitored for some typical cables.Considering the stringent requirements in accuracy and longterm stability,magnetic flux sensor,vibrating wire strain gauge and fiber bragg grating strain gauge are screened for the cable tension monitoring of the supporting cable-net.Specifically,receivers of radio telescopes have strict restriction on electro magnetic interference(EMI) or radio frequency interference(RFI).These three types of sensors are evaluated from the view of EMI/RFI.Firstly,these fundamentals are theoretically analyzed.Secondly,typical sensor signals are collected in the time and analyzed in the frequency domain,which shows the characteristic in the frequency domain.Finally,typical sensors are tested in an anechoic chamber to get the EMI levels.Theoretical analysis shows that Fiber Bragg Grating strain gauge itself will not lead to EMI/RFI.According to GJB151 A,frequency domain analysis and test results show that for the vibrating wire strain gauge and magnetic flux sensor themselves,testable EMI/RFI levels are typically below the background noise of the anechoic chamber.FAST finally choses these three sensors as the monitoring sensors of its cable tension.The proposed study is also a reference to the monitoring equipment selection of other radio telescopes and large structures.