The Nb single crystals of both[321]and[110]orientations have been cyclicly deformed in tension-compression at constant strain rate 8×10^(-4)s^(-1)over a range of plastic strain amplitudes between 10^(-3)and 10^(-...The Nb single crystals of both[321]and[110]orientations have been cyclicly deformed in tension-compression at constant strain rate 8×10^(-4)s^(-1)over a range of plastic strain amplitudes between 10^(-3)and 10^(-4).The cyclic hardening,the changes in shape of crystals and the asymmetry of stress have been studied.The hardening curve can be divided into three stages,i.e.first,rapid-hardening and saturated stage. In the first stage of cyclic hardening curve dominant features of dislocation configura- tions are high density networks and debris loops.In the rapid-hardening stage the main fea- ture is the formation of dislocation bundles.In the saturated a well defined bundle structure fully develops and between them it is filled with only screw dislocations and the imposed strain is accommodated mainly by the motion of screw dislocations travelling to and from between the bundles.Three-dimension cell,two-dimension cell or bundle structures are summarized as the saturated structures of bcc metals.展开更多
Pure and Molybdenum (Mo) doped Potassium Titanyl Phosphate (KTP) inorganic crystals were grown by high temperature solution growth (HTSG) from poly phosphate (K6P4O13) flux using different KTP/Flux ratios. The pure an...Pure and Molybdenum (Mo) doped Potassium Titanyl Phosphate (KTP) inorganic crystals were grown by high temperature solution growth (HTSG) from poly phosphate (K6P4O13) flux using different KTP/Flux ratios. The pure and doped KTP crystals of size 20x13x5 mm3 and 7x5x2.5 mm3 respectively were grown successfully by spontaneous nucleation. The grown crystals were characterized by XRD, UV, FTIR and Hardness studies. Micro hardness studies show that the pure crystals are harder than the Mo doped crystals.展开更多
CO2 laser beam welding experiment of Ti3Al-Nb alloy was conducted by adopting overlay welding, the resulting special crystallization phenomenon of welding joint was analyzed. The joints have obvious crystallizing laye...CO2 laser beam welding experiment of Ti3Al-Nb alloy was conducted by adopting overlay welding, the resulting special crystallization phenomenon of welding joint was analyzed. The joints have obvious crystallizing layer phenomenon with clear bond-like contours after laser welding. The results of X-spectrofluorimetry and energy spectrum analysis indicate that the non-uniform distribution of elements exists in crystallizing layer, because the temperature gradient is an important factor that impacts the alloy crystallization behavior. Furthermore, the effects of welding heat source, welding speed, pulse frequency and welding preheat on crystallizing layer distribution were investigated.展开更多
Diode end-pumped solid-state lasers have the potential to yield high quality laser beams with high efficiency for laser range finding and warning receiver applications as well as day and night military laser designati...Diode end-pumped solid-state lasers have the potential to yield high quality laser beams with high efficiency for laser range finding and warning receiver applications as well as day and night military laser designation systems. In this paper we presents theoretical calculations using Advanced Dynamics Professional LASCAD software and experimental studies for a high power pigtailed fiber diode laser module of 8 W operating at 808 nm with a specially designed high efficiency cooling system, end pumped high-efficiency Nd:YVO4 laser of 3 × 3 × 10 mm rod and overall cavity length of 44 mm. To the best of our knowledge a self Q-switching effects was generated in Nd:YVO4 laser by changing the cavity dimensions and the position of the intracavity KTP crystal at certain regime of operation for the first time, in which the cavity length is reduced to be 30 mm and the distance between Nd:YVO4 rod and KTP crystal is only 1mm. Self Q-switched laser pulse at 532 nm with high peak power of 96 W, pulse width of 88 ns at FWHM and repetition rate of 400 kHz was achieved. Experimental studies of a passive Q-switched Nd:YVO4 laser using Cr:YAG crystal with three different transmissions of 30%, 40% and 70% were investigated. Passive Q-switched laser pulse at 1064 nm and narrow line width of less than 1.5 nm with highest peak power of nearly 18 kW, short pulse width of less than 4 ns at FWHM and higher repetition rate of 45 kHz using Cr:YAG with transmission of 30% was achieved for the first time.展开更多
Three experimental single crystal superalloys with 0%Nb,0.5%Nb,1.0%Nb were cast in the directionally solidified furnace,while other alloying element contents were basically kept unchanged.The effect of Nb on the micro...Three experimental single crystal superalloys with 0%Nb,0.5%Nb,1.0%Nb were cast in the directionally solidified furnace,while other alloying element contents were basically kept unchanged.The effect of Nb on the microstructure,stability at1100°C and stress rupture properties at 1070°C and 160 MPa of the single crystal superalloy were investigated.The experiment results show that the primary dendrite arm spacing decreases and the volume fraction ofγ/γ′eutectic of the alloy increases with the increase of Nb content in the as-cast microstructures.The size ofγ′phase particles becomes small and uniform and the cubic shape does not obviously change with the increase of Nb content.The precipitating rate and volume fraction of TCP phases increase significantly with the increase of Nb content in the process of long term aging at 1100°C.The stress rupture lives increase and elongation decreases with increasing Nb content at 1070°C/160 MPa.At last,the relationship between the microstructures stability,stress rupture properties of the alloy and Nb content is discussed based on JMat Pro software and the lastest relevant database for single crystal superalloy.展开更多
利用X射线衍射,差热分析及静态磁性测量,研究了退火温度对不同成分的非晶Fe Nb B合金纳米晶化行为和磁性的影响·实验发现:在纳米晶化过程的初期出现磁硬化,矫顽力与最大磁导率均呈现不同程度的恶化·在硼化物(Fe2B和Fe3B)相析...利用X射线衍射,差热分析及静态磁性测量,研究了退火温度对不同成分的非晶Fe Nb B合金纳米晶化行为和磁性的影响·实验发现:在纳米晶化过程的初期出现磁硬化,矫顽力与最大磁导率均呈现不同程度的恶化·在硼化物(Fe2B和Fe3B)相析出前,具有纳米结构的合金由α Fe固溶体和非晶基体相组成,呈现较佳的软磁特性·随纳米晶相体积分数增加而呈现的磁软化现象可解释为由于纳米晶粒间距的减少,交换耦合增强所致·展开更多
文摘The Nb single crystals of both[321]and[110]orientations have been cyclicly deformed in tension-compression at constant strain rate 8×10^(-4)s^(-1)over a range of plastic strain amplitudes between 10^(-3)and 10^(-4).The cyclic hardening,the changes in shape of crystals and the asymmetry of stress have been studied.The hardening curve can be divided into three stages,i.e.first,rapid-hardening and saturated stage. In the first stage of cyclic hardening curve dominant features of dislocation configura- tions are high density networks and debris loops.In the rapid-hardening stage the main fea- ture is the formation of dislocation bundles.In the saturated a well defined bundle structure fully develops and between them it is filled with only screw dislocations and the imposed strain is accommodated mainly by the motion of screw dislocations travelling to and from between the bundles.Three-dimension cell,two-dimension cell or bundle structures are summarized as the saturated structures of bcc metals.
文摘Pure and Molybdenum (Mo) doped Potassium Titanyl Phosphate (KTP) inorganic crystals were grown by high temperature solution growth (HTSG) from poly phosphate (K6P4O13) flux using different KTP/Flux ratios. The pure and doped KTP crystals of size 20x13x5 mm3 and 7x5x2.5 mm3 respectively were grown successfully by spontaneous nucleation. The grown crystals were characterized by XRD, UV, FTIR and Hardness studies. Micro hardness studies show that the pure crystals are harder than the Mo doped crystals.
文摘CO2 laser beam welding experiment of Ti3Al-Nb alloy was conducted by adopting overlay welding, the resulting special crystallization phenomenon of welding joint was analyzed. The joints have obvious crystallizing layer phenomenon with clear bond-like contours after laser welding. The results of X-spectrofluorimetry and energy spectrum analysis indicate that the non-uniform distribution of elements exists in crystallizing layer, because the temperature gradient is an important factor that impacts the alloy crystallization behavior. Furthermore, the effects of welding heat source, welding speed, pulse frequency and welding preheat on crystallizing layer distribution were investigated.
文摘Diode end-pumped solid-state lasers have the potential to yield high quality laser beams with high efficiency for laser range finding and warning receiver applications as well as day and night military laser designation systems. In this paper we presents theoretical calculations using Advanced Dynamics Professional LASCAD software and experimental studies for a high power pigtailed fiber diode laser module of 8 W operating at 808 nm with a specially designed high efficiency cooling system, end pumped high-efficiency Nd:YVO4 laser of 3 × 3 × 10 mm rod and overall cavity length of 44 mm. To the best of our knowledge a self Q-switching effects was generated in Nd:YVO4 laser by changing the cavity dimensions and the position of the intracavity KTP crystal at certain regime of operation for the first time, in which the cavity length is reduced to be 30 mm and the distance between Nd:YVO4 rod and KTP crystal is only 1mm. Self Q-switched laser pulse at 532 nm with high peak power of 96 W, pulse width of 88 ns at FWHM and repetition rate of 400 kHz was achieved. Experimental studies of a passive Q-switched Nd:YVO4 laser using Cr:YAG crystal with three different transmissions of 30%, 40% and 70% were investigated. Passive Q-switched laser pulse at 1064 nm and narrow line width of less than 1.5 nm with highest peak power of nearly 18 kW, short pulse width of less than 4 ns at FWHM and higher repetition rate of 45 kHz using Cr:YAG with transmission of 30% was achieved for the first time.
文摘Three experimental single crystal superalloys with 0%Nb,0.5%Nb,1.0%Nb were cast in the directionally solidified furnace,while other alloying element contents were basically kept unchanged.The effect of Nb on the microstructure,stability at1100°C and stress rupture properties at 1070°C and 160 MPa of the single crystal superalloy were investigated.The experiment results show that the primary dendrite arm spacing decreases and the volume fraction ofγ/γ′eutectic of the alloy increases with the increase of Nb content in the as-cast microstructures.The size ofγ′phase particles becomes small and uniform and the cubic shape does not obviously change with the increase of Nb content.The precipitating rate and volume fraction of TCP phases increase significantly with the increase of Nb content in the process of long term aging at 1100°C.The stress rupture lives increase and elongation decreases with increasing Nb content at 1070°C/160 MPa.At last,the relationship between the microstructures stability,stress rupture properties of the alloy and Nb content is discussed based on JMat Pro software and the lastest relevant database for single crystal superalloy.
文摘利用X射线衍射,差热分析及静态磁性测量,研究了退火温度对不同成分的非晶Fe Nb B合金纳米晶化行为和磁性的影响·实验发现:在纳米晶化过程的初期出现磁硬化,矫顽力与最大磁导率均呈现不同程度的恶化·在硼化物(Fe2B和Fe3B)相析出前,具有纳米结构的合金由α Fe固溶体和非晶基体相组成,呈现较佳的软磁特性·随纳米晶相体积分数增加而呈现的磁软化现象可解释为由于纳米晶粒间距的减少,交换耦合增强所致·
