The exact classical limits for the coefficient of variation c for the normal distribution are derived. The hand-calculating approximated classical limits for c having high accuracy are given to meet practical engineer...The exact classical limits for the coefficient of variation c for the normal distribution are derived. The hand-calculating approximated classical limits for c having high accuracy are given to meet practical engineering needs. Using Odeh and Owen's computational method and Brent's algorithm, the tables for the r-upper exact classical limits of coefficient of variation for normal distribution are calculated for the different confidence coefficient y, the sample size n=1(1)30,40,60,120, the sample coefficient of variation c=0.01(0.01)0.20. It is shown that if n<8,c<0.20, then the V -upper exact classical limits cu for c are slightly higher than the exact fiducial limits cu,F for c if. n>8, c<0.02,then cu-cu,f<5x10-6展开更多
The identification of soy sauce adulteration can avoid fraud, and protect the rights and interests of producers and consumers. Based on two measurement models (1 mm, 10 mm), the visible and near-infrared (Vis-NIR) spe...The identification of soy sauce adulteration can avoid fraud, and protect the rights and interests of producers and consumers. Based on two measurement models (1 mm, 10 mm), the visible and near-infrared (Vis-NIR) spectroscopy combined with standard normal variate-partial least squares-discriminant analysis (SNV-PLS-DA) was used to establish the discriminant analysis models for adulterated and brewed soy sauces. Chubang soy sauce was selected as an identification brand (negative, 70). The adulteration samples (positive, 72) were prepared by mixing Chubang soy sauce and blended soy sauce with different adulteration rates. Among them, the “blended soy sauce” sample was concocted of salt water (NaCl), monosodium glutamate (C<sub>5</sub>H<sub>10</sub>NNaO<sub>5</sub>) and caramel color (C<sub>6</sub>H<sub>8</sub>O<sub>3</sub>). The rigorous calibration-prediction-validation sample design was adopted. For the case of 1 mm, five waveband models (visible, short-NIR, long-NIR, whole NIR and whole scanning regions) were established respectively;in the case of 10 mm, three waveband models (visible, short-NIR and visible-short-NIR regions) for unsaturated absorption were also established respectively. In independent validation, the models of all wavebands in the cases of 1 mm and 10 mm have achieved good discrimination effects. For the case of 1 mm, the visible model achieved the optimal validation effect, the validation recognition-accuracy rate (RAR<sub>V</sub>) was 99.6%;while in the case of 10 mm, both the visible and visible-short-NIR models achieved the optimal validation effect (RAR<sub>V</sub> = 100%). The detection method does not require reagents and is fast and simple, which is easy to promote the application. The results can provide valuable reference for designing small dedicated spectrometers with different measurement modals and different spectral regions.展开更多
Objective To evaluate the variations of intraocular pressure (lOP) in suspected open-angle glaucoma (OAG) patients. Methods The variations of lOP were measured in 216 eyes of suspected OAG patients at 4-hour inter...Objective To evaluate the variations of intraocular pressure (lOP) in suspected open-angle glaucoma (OAG) patients. Methods The variations of lOP were measured in 216 eyes of suspected OAG patients at 4-hour intervals for 48 h. Based on the results of the serial lOP measurements, optic disc changed and visual field defected, the patients were diagnosed as primary OAG ( POAG ), normal tension glaucoma (NTG), ocular hypertension ( OHT) , or physiologic cup (PC). Results After the serial lOP measurements, 16. 7% of the suspected OAG patients were diagnosed as POAG, 32. 4% as NTG, 24. 5% as OHT, and 26. 4% as PC. The highest percentages of the POAG group had peak lOP at 8 AM (19. 4% ) and their trough lOP at 10 PM (27. 8% ) ; the NTG group had peak lOP at 12 AM (18. 6% ) and their trough lOP at 12 PM (22. 9% ) ; the OHT group had peak lOP at 4 AM (22. 6% ) and their trough lOP at 10 PM (26. 4% ) ; and the PC group had peak lOP at 4 AM ( 21. 1% ) and their trough lOP at 12 PM ( 21. 1% ). The percentages of peak lOP outside clinic ( 8 AM - 4 PM) in the POAG, NTG, OHT and PC groups were 55. 6%, 50. 0%, 58. 4% and 45. 7%, respectively. The mean magnitude of variance was 5. 1 - 6. 7 mmHg in those suspected OAG patients. There was a strong positive correlation in lOP between both eyes at each time point of measurement and the variation curves of the right and left eyes had parallel profiles in those suspected OAG patients. Conclusion Serial measurement of lOP is still needed, in order not to miss the peak and the trough lOP readings in suspected OAG patients, which helps in better management of glaucoma.展开更多
Soil organic matter (SOM) is important for plant growth and production. Conventional analyses of SOM are expensive and time consuming. Hyperspectral remote sensing is an alternative approach for SOM estimation. In thi...Soil organic matter (SOM) is important for plant growth and production. Conventional analyses of SOM are expensive and time consuming. Hyperspectral remote sensing is an alternative approach for SOM estimation. In this study, the diffuse reflectance spectra of soil samples from Qixia City, the Shandong Peninsula, China, were measured with an ASD FieldSpec 3 portable object spectrometer (Analytical Spectral Devices Inc., Boulder, USA). Raw spectral reflectance data were transformed using four methods: nine points weighted moving average (NWMA), NWMA with first derivative (NWMA + FD), NWMA with standard normal variate (NWMA + SNV), and NWMA with min-max standardization (NWMA + MS). These data were analyzed and correlated with SOM content. The evaluation model was established using support vector machine regression (SVM) with sensitive wavelengths. The results showed that NWMA + FD was the best of the four pretreatment methods. The sensitive wavelengths based on NWMA + FD were 917, 991, 1 007, 1 996, and 2 267 nm. The SVM model established with the above-mentioned five sensitive wavelengths was significant ( R 2 = 0.875, root mean square error (RMSE) = 0.107 g kg −1 for calibration set;R 2 = 0.853, RMSE = 0.097 g kg −1 for validation set). The results indicate that hyperspectral remote sensing can quickly and accurately predict SOM content in the brown forest soil areas of the Shandong Peninsula. This is a novel approach for rapid monitoring and accurate diagnosis of brown forest soil nutrients.展开更多
文摘The exact classical limits for the coefficient of variation c for the normal distribution are derived. The hand-calculating approximated classical limits for c having high accuracy are given to meet practical engineering needs. Using Odeh and Owen's computational method and Brent's algorithm, the tables for the r-upper exact classical limits of coefficient of variation for normal distribution are calculated for the different confidence coefficient y, the sample size n=1(1)30,40,60,120, the sample coefficient of variation c=0.01(0.01)0.20. It is shown that if n<8,c<0.20, then the V -upper exact classical limits cu for c are slightly higher than the exact fiducial limits cu,F for c if. n>8, c<0.02,then cu-cu,f<5x10-6
文摘The identification of soy sauce adulteration can avoid fraud, and protect the rights and interests of producers and consumers. Based on two measurement models (1 mm, 10 mm), the visible and near-infrared (Vis-NIR) spectroscopy combined with standard normal variate-partial least squares-discriminant analysis (SNV-PLS-DA) was used to establish the discriminant analysis models for adulterated and brewed soy sauces. Chubang soy sauce was selected as an identification brand (negative, 70). The adulteration samples (positive, 72) were prepared by mixing Chubang soy sauce and blended soy sauce with different adulteration rates. Among them, the “blended soy sauce” sample was concocted of salt water (NaCl), monosodium glutamate (C<sub>5</sub>H<sub>10</sub>NNaO<sub>5</sub>) and caramel color (C<sub>6</sub>H<sub>8</sub>O<sub>3</sub>). The rigorous calibration-prediction-validation sample design was adopted. For the case of 1 mm, five waveband models (visible, short-NIR, long-NIR, whole NIR and whole scanning regions) were established respectively;in the case of 10 mm, three waveband models (visible, short-NIR and visible-short-NIR regions) for unsaturated absorption were also established respectively. In independent validation, the models of all wavebands in the cases of 1 mm and 10 mm have achieved good discrimination effects. For the case of 1 mm, the visible model achieved the optimal validation effect, the validation recognition-accuracy rate (RAR<sub>V</sub>) was 99.6%;while in the case of 10 mm, both the visible and visible-short-NIR models achieved the optimal validation effect (RAR<sub>V</sub> = 100%). The detection method does not require reagents and is fast and simple, which is easy to promote the application. The results can provide valuable reference for designing small dedicated spectrometers with different measurement modals and different spectral regions.
文摘Objective To evaluate the variations of intraocular pressure (lOP) in suspected open-angle glaucoma (OAG) patients. Methods The variations of lOP were measured in 216 eyes of suspected OAG patients at 4-hour intervals for 48 h. Based on the results of the serial lOP measurements, optic disc changed and visual field defected, the patients were diagnosed as primary OAG ( POAG ), normal tension glaucoma (NTG), ocular hypertension ( OHT) , or physiologic cup (PC). Results After the serial lOP measurements, 16. 7% of the suspected OAG patients were diagnosed as POAG, 32. 4% as NTG, 24. 5% as OHT, and 26. 4% as PC. The highest percentages of the POAG group had peak lOP at 8 AM (19. 4% ) and their trough lOP at 10 PM (27. 8% ) ; the NTG group had peak lOP at 12 AM (18. 6% ) and their trough lOP at 12 PM (22. 9% ) ; the OHT group had peak lOP at 4 AM (22. 6% ) and their trough lOP at 10 PM (26. 4% ) ; and the PC group had peak lOP at 4 AM ( 21. 1% ) and their trough lOP at 12 PM ( 21. 1% ). The percentages of peak lOP outside clinic ( 8 AM - 4 PM) in the POAG, NTG, OHT and PC groups were 55. 6%, 50. 0%, 58. 4% and 45. 7%, respectively. The mean magnitude of variance was 5. 1 - 6. 7 mmHg in those suspected OAG patients. There was a strong positive correlation in lOP between both eyes at each time point of measurement and the variation curves of the right and left eyes had parallel profiles in those suspected OAG patients. Conclusion Serial measurement of lOP is still needed, in order not to miss the peak and the trough lOP readings in suspected OAG patients, which helps in better management of glaucoma.
基金supported by the National Nature Science Foundation of China(Nos.41671346 and41301482)the Shandong Province Natural Science Fund of China(No.ZR2012DM007)
文摘Soil organic matter (SOM) is important for plant growth and production. Conventional analyses of SOM are expensive and time consuming. Hyperspectral remote sensing is an alternative approach for SOM estimation. In this study, the diffuse reflectance spectra of soil samples from Qixia City, the Shandong Peninsula, China, were measured with an ASD FieldSpec 3 portable object spectrometer (Analytical Spectral Devices Inc., Boulder, USA). Raw spectral reflectance data were transformed using four methods: nine points weighted moving average (NWMA), NWMA with first derivative (NWMA + FD), NWMA with standard normal variate (NWMA + SNV), and NWMA with min-max standardization (NWMA + MS). These data were analyzed and correlated with SOM content. The evaluation model was established using support vector machine regression (SVM) with sensitive wavelengths. The results showed that NWMA + FD was the best of the four pretreatment methods. The sensitive wavelengths based on NWMA + FD were 917, 991, 1 007, 1 996, and 2 267 nm. The SVM model established with the above-mentioned five sensitive wavelengths was significant ( R 2 = 0.875, root mean square error (RMSE) = 0.107 g kg −1 for calibration set;R 2 = 0.853, RMSE = 0.097 g kg −1 for validation set). The results indicate that hyperspectral remote sensing can quickly and accurately predict SOM content in the brown forest soil areas of the Shandong Peninsula. This is a novel approach for rapid monitoring and accurate diagnosis of brown forest soil nutrients.