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响应面优化辛烯基琥珀酸淀粉酯稳定藻油乳液的工艺研究 被引量:4
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作者 甄天元 慕鸿雁 《中国粮油学报》 EI CAS CSCD 北大核心 2020年第12期44-49,61,共7页
以乳化稳定指数(ESI)、粒径、Zeta电位为考察指标,通过单因素响应面优化实验研究了以辛烯基琥珀酸淀粉酯(OSA-淀粉)为乳化剂的裂壶藻油乳液制备工艺,并对其氧化稳定性进行了分析。单因素实验结果表明,OSA-淀粉的质量分数为10%、藻油质... 以乳化稳定指数(ESI)、粒径、Zeta电位为考察指标,通过单因素响应面优化实验研究了以辛烯基琥珀酸淀粉酯(OSA-淀粉)为乳化剂的裂壶藻油乳液制备工艺,并对其氧化稳定性进行了分析。单因素实验结果表明,OSA-淀粉的质量分数为10%、藻油质量分数为4%、超声功率为360~420 W,超声15~20 min可以得到ESI较高的纳米级乳液。响应面优化设计分析后,OSA-淀粉质量分数为10.50%,藻油质量分数为3.50%,超声功率为375 W,超声时间20 min,在此条件下乳液的ESI和粒径分别为96.10%和238.12 nm。该乳液在实验条件下其氧化稳定性显著优于未添加OSA-淀粉组。 展开更多
关键词 osa-淀粉 裂壶藻油 乳液 乳化稳定性 氧化稳定性
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Synthesis and paste properties of octenyl succinic anhydride modified early Indica rice starch 被引量:53
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作者 SONG Xiao-yan CHEN Qi-he RUAN Hui HE Guo-qing XU Qiong 《Journal of Zhejiang University-Science B(Biomedicine & Biotechnology)》 SCIE CAS CSCD 2006年第10期800-805,共6页
Octenyl succinic anhydride (OSA) modified early Indica rice starch was prepared in aqueous slurry systems using response surface methodology. The paste properties of the OSA starch were also investigated. Results in... Octenyl succinic anhydride (OSA) modified early Indica rice starch was prepared in aqueous slurry systems using response surface methodology. The paste properties of the OSA starch were also investigated. Results indicated that the suitable parameters for the preparation of OSA starch from early Indica rice starch were as follows: reaction period 4 h, reaction temperature 33.4℃, pH of reaction system 8.4, concentration of starch slurry 36.8% (in proportion to water, w/w), amount of OSA 3% (in proportion to starch, w/w). The degree of substitution was 0.0188 and the reaction efficiency was 81.0%. The results of paste properties showed that with increased OSA modification, the starch derivatives had higher paste clarity, decreased retrogradation and better freeze-thaw stability. 展开更多
关键词 Early Indica rice OSA starch Response surface methodology Paste properties
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