Microscopic damage evolution of anisotropic rocks under indirect tensile conditions: Insights from acoustic emission and digital image correlation techniques

The anisotropy induced by rock bedding structures is usually manifested in the mechanical behaviors and failure modes of rocks.Brazilian tests are conducted for seven groups of shale specimens featuring different bedding angles. Acoustic emission (AE) and digital image correlation (DIC) technologies are used to monitor the in-situ failure of the specimens. Furthermore, the crack morphology of damaged samples is observed through scanning electron microscopy (SEM). Results reveal the structural dependence on the tensile mechanical behavior of shales. The shale disk exhibits compression in the early stage of the experiment with varying locations and durations. The location of the compression area moves downward and gradually disappears when the bedding angle increases. The macroscopic failure is well characterized by AE event location results, and the dominant frequency distribution is related to the bedding angle. The b-value is found to be stress-dependent.The crack turning angle between layers and the number of cracks crossing the bedding both increase with the bedding angle, indicating competition between crack propagations. SEM results revealed that the failure modes of the samples can be classified into three types:tensile failure along beddings with shear failure of the matrix, ladder shear failure along beddings with tensile failure of the matrix, and shear failure along multiple beddings with tensile failure of the matrix.

Acoustic emission characterization of microcracking in laboratory-scale hydraulic fracturing tests

Understanding microcracking near coalesced fracture generation is critically important for hydrocarbon and geothermal reservoir characterization as well as damage evaluation in civil engineering structures. Dense and sometimes random microcracking near coalesced fracture formation alters the mechanical properties of the nearby virgin material. Individual microcrack characterization is also significant in quantifying the material changes near the fracture faces （i.e. damage）. Acoustic emission （AE） monitoring and analysis provide unique information regarding the microcracking process temporally, and infor- mation concerning the source characterization of individual microcracks can be extracted. In this context, laboratory hydraulic fracture tests were carried out while monitoring the AEs from several piezoelectric transducers. In-depth post-processing of the AE event data was performed for the purpose of under- standing the individual source mechanisms. Several source characterization techniques including moment tensor inversion, event parametric analysis, and volumetric deformation analysis were adopted. Post-test fracture characterization through coring, slicing and micro-computed tomographic imaging was performed to determine the coalesced fracture location and structure. Distinct differences in fracture characteristics were found spatially in relation to the openhole injection interval. Individual microcrack AE analysis showed substantial energy reduction emanating spatially from the injection interval. It was quantitatively observed that the recorded AE signals provided sufficient information to generalize the damage radiating spatially away from the injection wellbore.

Interface fracture toughness and fracture mechanisms of thermal barrier coatings investigated by indentation test and acoustic emission technique

Interface fracture toughness and fracture mechanisms of plasma-/sprayed thermal barrier coatings （TBCs） were investigated by interfacial indentation test （ HT） in combination with acoustic emission （ AE ） measurement. Critical load and AE energy were employed to calculate interface fracture toughness. The critical point at which crack appears at the interface was determined by the HT. AE signals produced during total indentation test not only are used to investigate the interface cracking behavior by Fast Fourier Transform （FFT） and wavelet transforms but also supply the mechanical information. The result shows that the AE signals associated with coating plastic deformation during indentation are of a more continuous type with a lower characteristic frequency content （30 -60 kHz） , whereas the instantaneous relaxation associated with interface crack initiation produces burst type AE signals with a characteristic frequency in the range 70 - 200 kHz. The AE signals energy is concentrated on different scales for the coating plastic deformation, interface crack initiation and interface crack propagation. Interface fracture toughness calculated by AE energy was 1. 19 MPam1/2 close to 1.58 MPam1/2 calculated by critical load. It indicates that the acoustic emission energy is suitable to reflect the interface fracture toughness.

Electrical Emissions from Concrete under Three-point Bending Tests

Electrical emission (EM) signals, which are generated from the concrete specimens under three-point bending tests, were conducted. It is shown that electrical emission phenomena are related to cracking of the specimens, cohesive failure, contact-separation etc. The simultaneous appearance of electric emission signals and visible cracks during the flexure loading of beams was also observed.

Ion Photon Emission Microscope for Single Event Effect Testing in CIAE

Ion photon emission microscopy （IPEM） is a new ion-induced emission microscopy. It employs a broad ion beam with high energy and low fluence rate impinging on a sample. The position of a single ion is detected by an optical system with objective lens, prism, microscope tube and charge coupled device （CCD）. A thin ZnS film doped with Ag ions is used as a luminescent material. Generation efficiency and transmission efficiency of photons in the ZnS（Ag） film created by irradiated Cl ions are calculated. A single Cl ion optical microscopic image is observed by high quantum efficiency CCD. The resolution of a single Cl ion given in this IPEM system is 6μm. Several factors influencing the resolution are discussed. A silicon diode is used to collect the electrical signals caused by the incident ions. Effective and accidental coincidence of optical images and electronic signals are illustrated. A two-dimensional map of single event effect is drawn out according to the data of effective coincidence.

On the Bump Tests of Cracked Shafts Using Acoustic Emission Techniques

An investigation about the application of Acoustic Emission (AE) techniques to analyze the dynamic response of different cracked shafts rendered in bump tests is presented in this work. The experimental apparatus devised for this work complies of six shafts with different transverse crack sizes and a high-frequency data acquisition system. The AE signals generated in the bump tests performed on the different cracked shafts are captured by a wideband AE transducer. Those signals are treated by using statistical moments, wavelet transforms, and frequency- and time-domain procedures. A transverse crack of predetermined depth is etched into each shaft. The experimental results show that the values of kurtosis and skewness estimated for the AE signals can be used to identify the crack size.

Space-time evolution rules of acoustic emission location of unloaded coal sample at different loading rates

By using MTS815 rock mechanics test system,a series of acoustic emission(AE) location experiments were performed under unloading confining pressure,increasing the axial stress.The AE space-time evolution regularities and energy releasing characteristics during deformation and failure process of coal of different loading rates are compared,the influence mechanism of loading rates on the microscopic crack evolution were studied,combining the AE characteristics and the macroscopic failure modes of the specimens,and the precursory characteristics of coal failure were also analyzed quantitatively.The results indicate that as the loading rate is higher,the AE activity and the main fracture will begin earlier.The destruction of coal body is mainly the function of shear strain at lower loading rate and tension strain at higher rate,and will transform from brittleness to ductility at critical velocities.When the deformation of the coal is mainly plasticity,the amplitude of the AE ringing counting rate increases largely and the AE energy curves appear an obvious ''step'',which can be defined as the first failure precursor point.Statics of AE information shows that the strongest AE activity begins when the axial stress level was 92-98%,which can be defined as the other failure precursor point.As the loading rate is smaller,the coal more easily reaches the latter precursor point after the first one,so attention should be aroused to prevent dynamic disaster in coal mining when the AE activity reaches the first precursor point.

Real-world vehicle emission factors in Chinese metropolis city—Beijing

The dynamometer tests with different driving cycles and the real-world tests are presented. Results indicated the pollutants emission factors and fuel consumption factor with ECE15+EUDC driving cycle usually take the lowest value and with real world driving cycle occur the highest value, and different driving cycles will lead to significantly different vehicle emission factors with the same vehicle. Relative to the ECE15+EUDC driving cycle, the increasing rate of pollutant emission factors of CO, NOx and HC are -0.42—2.99, -0.32 —0.81 and -0.11—11 with FTP75 testing, 0.11—1.29, -0.77—0.64 and 0.47—10.50 with Beijing 1997 testing and 0.25—1.83, 0.09—0.75 and -0.58—1.50 with real world testing. Compared to the carburetor vehicles, the retrofit and MPI+TWC vehicles' pollution emission factors decrease with different degree. The retrofit vehicle(Santana) will reduce 4.44%—58.44% CO, -4.95%—36.79% NOx, -32.32%—33.89% HC, and -9.39%—14.29% fuel consumption, and especially that the MPI+TWC vehicle will decrease CO by 82.48%—91.76%, NOx by 44.87%—92.79%, HC by 90.00%—93.89% and fuel consumption by 5.44%—10.55%. Vehicles can cause pollution at a very high rate when operated in high power modes; however, they may not often operate in these high power modes. In analyzing vehicle emissions, it describes the fraction of time that vehicles operate in various power modes. In Beijing, vehicles spend 90% of their operation in low power modes or decelerating.

Uniaxial experimental study of the acoustic emission and deformation behavior of composite rock based on 3D digital image correlation(DIC)

In this paper, uniaxial compression tests were carried out on a series of composite rock specimens with different dip angles, which were made from two types of rock-like material with different strength. The acoustic emission technique was used to monitor the acoustic signal characteristics of composite rock specimens during the entire loading process. At the same time, an optical non-contact 3 D digital image correlation technique was used to study the evolution of axial strain field and the maximal strain field before and after the peak strength at different stress levels during the loading process. The effect of bedding plane inclination on the deformation and strength during uniaxial loading was analyzed. The methods of solving the elastic constants of hard and weak rock were described. The damage evolution process, deformation and failure mechanism, and failure mode during uniaxial loading were fully determined. The experimental results show that the θ = 0?–45?specimens had obvious plastic deformation during loading, and the brittleness of the θ = 60?–90?specimens gradually increased during the loading process. When the anisotropic angle θincreased from 0?to 90?, the peak strength, peak strain,and apparent elastic modulus all decreased initially and then increased. The failure mode of the composite rock specimen during uniaxial loading can be divided into three categories:tensile fracture across the discontinuities(θ = 0?–30?), slid-ing failure along the discontinuities(θ = 45?–75?), and tensile-split along the discontinuities(θ = 90?). The axial strain of the weak and hard rock layers in the composite rock specimen during the loading process was significantly different from that of the θ = 0?–45?specimens and was almost the same as that of the θ = 60?–90?specimens. As for the strain localization highlighted in the maximum principal strain field, the θ = 0?–30?specimens appeared in the rock matrix approximately parallel to the loading direction,while in the θ = 45?–90?specimens it appeared at the hard and weak rock layer interface.

Investigation of active vibration drilling using acoustic emission and cutting size analysis

This paper describes an investigation of active bit vibration on the penetration mechanisms and bit-rock interaction for drilling with a diamond impregnated coring bit. A series of drill-off tests(DOTs) were conducted where the drilling rate-of-penetration(ROP) was measured at a series of step-wise increasing static bit thrusts or weight-on-bits(WOBs). Two active DOTs were conducted by applying 60 Hz axial vibration at the bit-rock interface using an electromagnetic vibrating table mounted underneath the drilling samples, and a passive DOT was conducted where the bit was allowed to vibrate naturally with lower amplitude due to the compliance of the drilling sample mountings. During drilling, an acoustic emission(AE) system was used to record the AE signals generated by the diamond cutter penetration and the cuttings were collected for grain size analysis. The instrumented drilling system recorded the dynamic motions of the bit-rock interface using a laser displacement sensor, a load cell, and an LVDT(linear variable differential transformer) recorded the dynamic WOB and the ROP, respectively. Calibration with the drilling system showed that rotary speed was approximately the same at any given WOB, facilitating comparison of the results at the same WOB. Analysis of the experimental results shows that the ROP of the bit at any given WOB increased with higher amplitude of axial bit-rock vibration, and the drill cuttings increased in size with a higher ROP. Spectral analysis of the AEs indicated that the higher ROP and larger cutting size were correlated with a higher AE energy and a lower AE frequency. This indicated that larger fractures were being created to generate larger cutting size. Overall, these results indicate that a greater magnitude of axial bit-rock vibration produces larger fractures and generates larger cuttings which, at the same rotary speed, results in a higher ROP.

Four types of acoustic emission characteristics during granular stick-slip evolution

The shear behavior of granular materials plays an important role in understanding the occurrence of geological hazards. This study introduces the use of direct shear tests and acoustic emission(AE) technology on glass beads to investigate the distributions features of AE during the stick-slip processes. Results show that the shearing behavior of granular samples was shown as a series of similar, periodic stick-slip events. Some AE features — energy and Root Mean Square(RMS) —showed significant spatial clustering. Combined with the distribution of AE in the stick-slip event, the AE signal can be divided into four types: 1. low-energy and highfrequency AE, which represent particle friction;2. highenergy and low-frequency AE, which represent structural failure, that is, the slip process;3. low-RMS and lowfrequency AE represent internal local failure;and 4.high-RMS and high-frequency AE caused by overall structure failure. The b-value representing the energy distribution of AEs is used to describe the changing of AE sources during shear process. In addition, the amount and energy of AE had a significant positive correlation with normal stress. The shear rate mainly affects the AE representing particle friction, and the faster the shear rate, the lower the incidence of these friction AEs. According to the time sequence of the occurrence of different types of AE, AE rate, b-value and local failure AE signal can be applied to the prediction or early warning of geological hazards.

Study of electromagnetic and acoustic emission in creep experiments of water-containing rock samples

Based on biaxial shear creep tests conducted on rock samples with different water contents, we present the results of our study on the regularities of electromagnetic and acoustic emission during the process of creep experiments in which we have analyzed the contribution of water to the occurrence of electromagnetic radiation. The result shows that in the creep-fracturing course of rock samples, when the water content increases, the initial frequency and amplitude of electromagnetic and acoustic emission also increases, but at a decreasing growth rate caused by loading stress. This can be used as a criterion for the long-term stability of rock masses under conditions of repeated inundation and discharge of water.

Wavelet analysis of acoustic emission signals from thermal barrier coatings

The wavelet transform is applied to the analysis of acoustic emission signals collected during tensile test of the ZrO2-8% Y2O3 (YSZ) thermal barrier coatings (TBCs). The acoustic emission signals are de-noised using the Daubechies discrete wavelets, and then decomposed into different wavelet levels using the programs developed by the authors. Each level is examined for its specific frequency range. The ratio of energy in different levels to the total energy gives information on the failure modes (coating micro-failures and substrate micro-failures) associated with TBCs system.

Experimental investigation of power output and soot emission for micro-emulsification diesel oil using for vehicle

The micro-emulsification diesel oil with water dopant of 5%,10% and 15% was prepared using the NAA micro-emulsification compound developed by the authors.The engine bench testing was carried out on the 485QB diesel engine.From the testing results of velocity,loading and exhaust gas,it can be seen that the power decreases and the fuel consumption increases using the micro-emulsification diesel oil.But based on the actual fuel consumption,the use of emulsification diesel with water dopant of 10% can get the effect of oil saving;while with water dopant of more than 15%,it doesn't work evidently.The investigation shows that using the micro-emulsification diesel oil,we can reduce the exhaust gas pollution and receive better environment benefit.

Measurement of Emissions from a Passenger Truck Fueled with Biodiesel from Different Feedstocks

Biodiesel has generated increased interest recently as an alternative to petroleum-derived diesel. Due to its high oxygen content, biodiesel typically burns more completely than petroleum diesel, and thus has lower emissions of hydrocarbons (HC), carbon monoxide (CO), and particulate matter (PM). However, biodiesel may increase or decrease nitrogen oxide (NOx) and carbon dioxide (CO2) emissions, depending on biodiesel feedstock, engine type, and test cycle. The purpose of this study was to compare emissions from 20% blends of biodiesel made from 4 feedstocks (soybean oil, canola oil, waste cooking oil, and animal fat) with emissions from ultra low sulfur diesel (ULSD). Emissions of NOx and CO2 were made under real-world driving conditions using a Horiba On-Board Measurement System OBS-1300 on a highway route and arterial route;emissions of NOx, CO2, HC, CO, and PM were measured in a controlled setting using a chassis dynamometer with Urban Dynamometer Drive Schedule. Dynamometer test results showed statistically significant lower emissions of HC, CO, and PM from all B20 blends compared to ULSD. For CO2, both on-road testing (arterial, highway, and idling) and dynamometer testing showed no statistically significant difference in emissions among the B20 blends and ULSD. For NOx, dynamometer testing showed only B20 from soybean oil to have statistically significant higher emissions. This is generally consistent with the on-road testing, which showed no statistically significant difference in NOx emissions between ULSD and the B20 blends.

Can environmental sustainability be decoupled from economic growth? Empirical evidence from Eastern Europe using the common correlated effect mean group test

The European Union(EU) and Organisation for Economic Co-operation and Development(OECD) aim to develop long-term policies for their respective member countries. Having observed increasing dangers to the environment posed by rising economic growth, they are seeking pathways to enable policy action on economic growth and environmental sustainability. Given the facts in theoretical and empirical studies, this study assessed the validity of the decoupling hypothesis by investigating asymmetricity in the relationship between environmental sustainability and economic growth in nine Eastern European countries from 1998 to 2017 using the cross-section augmented Dickey-Fuller(CADF) unit root, panel corrected standard error(PCSE), common correlated effect mean group(CCEMG), and Dumitrescu Hurlin causality approaches. Both population growth and drinking water are used as controlled variables. The outcomes establish strong cointegration among all the variables of interest. According to the results of CCEMG test, economic growth exerts short-term environmental degradation but has long-term environmental benefits in Eastern Europe;and population growth and drinking water exert a positive effect on environmental sustainability in both the short-and long-run. The results of Dumitrescu Hurlin causality test indicate that environmental sustainability is unidirectionally affected by economic growth. Based on these outcomes, we suggest the following policies:(1) the EU and OECD should implement member-targeted policies on economic growth and fossil-fuel use towards regulating industrial pollution, water use, and population control;and(2) the EU and OECD member countries should invest in environmental technologies through green research and development(R&D) to transform their dirty industrial processes and ensure productive energy use.