The precipitation behavior of carbide in K416 B superalloy was investigated by means of creep measurement and microstructure observation. The results show that nanometer M6 C particles discontinuously precipitate in t...The precipitation behavior of carbide in K416 B superalloy was investigated by means of creep measurement and microstructure observation. The results show that nanometer M6 C particles discontinuously precipitate in the γ matrix or along the γ/γ′ interface of the alloy during high temperature tensile creep. Thereinto, the amount of fine M6 C carbide increases as creep goes on, and the coherent interfaces of M6 C phase precipitating from the γ matrix are {100} and {111} planes. The thermodynamics analysis indicates that the solubility of element carbon in the matrix decreases when the alloy is deformed by the axial tensile stress during creep, so as to cause the carbon segregating in the regions of stress concentration and combining with carbide-forming elements M(W, Co), which promotes the fine M6 C carbide to precipitate from the γ matrix.展开更多
High temperature oxidation behaviors of FGH96 P/M superaUoy have been studied in air at temperatures ranging from 600 to 1000℃. By means of isothermal oxidation testing, X-ray diffraction, SEM (scanning electron mic...High temperature oxidation behaviors of FGH96 P/M superaUoy have been studied in air at temperatures ranging from 600 to 1000℃. By means of isothermal oxidation testing, X-ray diffraction, SEM (scanning electron microscopy), and EDS (energy dispersive X-ray spectroscopy) analyses, the oxidation kinetics as well as the composition and morphology of scales were investigated. Thermodynamic calculations were used to explain the oxidation mechanism. The results showed that as the oxidation temperature increased, the oxidation rate, the scale thickness, and scale spallation increased. FGH96 P/M superalloy exhibits good oxidation resistance at temperature below 800℃. The oxidation kinetics follows an approximately parabolic rate law, and the oxide layer was mainly composed of Cr2O3 TiO2 and a little amount of NiCr2O4. The oxidation is controlled by the transmission of chromium. titanium, and oxygen through the oxide scale.展开更多
In situ fatigue tests in special designed SEM were conducted to trace the whole process of crack initiation and propagation fill to fracture in mckel-base P/M superalloy seeded inclusions. The experimental results sho...In situ fatigue tests in special designed SEM were conducted to trace the whole process of crack initiation and propagation fill to fracture in mckel-base P/M superalloy seeded inclusions. The experimental results show that non-metallic inclusions can induce crack initiation. When the inclusion size is larger than the critical one, the crack can propagate as the main crack that induces the specimen to fracture. As a result, the LCF life of the specimen decreases.展开更多
Elevated intraocular pressure(IOP)is one of the causes of retinal ischemia/reperfusion injury,which results in NRP3 inflammasome activation and leads to visual damage.Homerla is repo rted to play a protective role in ...Elevated intraocular pressure(IOP)is one of the causes of retinal ischemia/reperfusion injury,which results in NRP3 inflammasome activation and leads to visual damage.Homerla is repo rted to play a protective role in neuroinflammation in the cerebrum.However,the effects of Homerla on NLRP3inflammasomes in retinal ischemia/reperfusion injury caused by elevated IOP remain unknown.In our study,animal models we re constructed using C57BL/6J and Homer1^(flox/-)/Homerla^(+/-)/Nestin-Cre^(+/-)mice with elevated IOP-induced retinal ischemia/repe rfusion injury.For in vitro expe riments,the oxygen-glucose deprivation/repe rfusion injury model was constructed with M uller cells.We found that Homerla ove rexpression amelio rated the decreases in retinal thickness and Muller cell viability after ischemia/reperfusion injury.Furthermore,Homerla knockdown promoted NF-κB P65^(Ser536)activation via caspase-8,NF-κB P65 nuclear translocation,NLRP3 inflammasome formation,and the production and processing of interleukin-1βand inte rleukin-18.The opposite results we re observed with Homerla ove rexpression.Finally,the combined administration of Homerla protein and JSH-23 significantly inhibited the reduction in retinal thickness in Homer1^(flox/-)Homer1a^(+/-)/Nestin-Cre^(+/-)mice and apoptosis in M uller cells after ischemia/reperfusion injury.Taken together,these studies demonstrate that Homer1a exerts protective effects on retinal tissue and M uller cells via the caspase-8/NF-KB P65/NLRP3 pathway after I/R injury.展开更多
Super-clean and super-spherical FGH4095 superalloy powder is produced by the ceramic-free electrode inductionmelt inert gas atomization(EIGA) technique.A continuous and steady-state liquid metal flow is achieved at ...Super-clean and super-spherical FGH4095 superalloy powder is produced by the ceramic-free electrode inductionmelt inert gas atomization(EIGA) technique.A continuous and steady-state liquid metal flow is achieved at high-frequency(350 k Hz) alternating current and high electric power(100 k W).The superalloy is immersed in a high-frequency induction coil,and the liquid metal falling into a supersonic nozzle is atomized by an Ar gas of high kinetic gas energy.Numerical calculations are performed to optimize the structure parameters for the nozzle tip.The undesired oxidation reaction of alloying elements starts at 1000℃ with the reaction originating from the active sites on the powder surfaces,leading to the formation of oxides,MexOy.The role of active sites and kinetic factors associated with the diffusion of oxygen present in the atomization gas streams are also examined.The observed results reveal that the oxidation process occurring at the surface of the produced powders gradually moves toward the core,and that there exists a clear interface between the product layer and the reactant.The present study lays a theoretical foundation for controlling the oxidation of nickel-based superalloy powders from the powder process step.展开更多
The rupture behavior of a cast Ni-base superalloy M963 at high temperature has been investi- gated. The microstructure examination shows that there exists a large amount of the carbide and γ-γ' eutectic, which i...The rupture behavior of a cast Ni-base superalloy M963 at high temperature has been investi- gated. The microstructure examination shows that there exists a large amount of the carbide and γ-γ' eutectic, which is very harmful to the mechanical properties of M963 superalloy. The tensile strength of M963 superalloy both at room temperature and at high temperatures is higher than that of K17G alloy, but the tensile ductility of the former is much lower than that of the latter. In tensile fracture process with the high strain rate, the open carbides are the initiation site and the carbide/matrix interface is the propagation path of cracks. But in fracture process with the low strain rate, the carbide/matrix interface and cast microvoids are the initiation sites, and the carbide/matrix interface is the propagation path of cracks. The effective ways to improve ductility of M963 superalloy are also suggested.展开更多
In this work,we report observations of three comets:38P/Stephan-Oterma,64P/Swift-Gehrels,and C/2017 M4(ATLAS),conducted with the Nanshan one-meter wide-field telescope in 2018 August and November,and 2019January.We ex...In this work,we report observations of three comets:38P/Stephan-Oterma,64P/Swift-Gehrels,and C/2017 M4(ATLAS),conducted with the Nanshan one-meter wide-field telescope in 2018 August and November,and 2019January.We extracted morphological features through image enhancement techniques and calculated the dust activity parameter,Afρ,along with dust mass loss rates and coma color indices using broadband photometric data.Our morphological analysis uncovered a spectrum of dust characteristics among the observed comets,ranging from a significant twisted structure in comet 38P/Stephan-Oterma’s coma to the regular coma envelope surrounding comet 64P/Swift-Gehrels.The Afρvalues varied between 148.8±0.3 cm for 64P/Swift-Gehrels and1118.5±6.2 cm for C/2017 M4(ATLAS)(measured within a reference aperture radius ofρ=6″),indicating a range from moderate to high activity levels.Dust mass loss rates were estimated from 328.1 kg s^(-1)for comet 64P/Swift-Gehrels to 1395.5 kg s^(-1)for comet C/2017 M4(ATLAS).The color indices of comets 38P/Stephan-Oterma and C/2017 M4(ATLAS)closely resemble the average colors of active short-period comets and active longperiod comets,respectively.In contrast,64P/Swift-Gehrels exhibits a significantly bluer hue than typical Jupiter family comets.展开更多
In the digital age,non-touch communication technologies are reshaping human-device interactions and raising security concerns.A major challenge in current technology is the misinterpretation of gestures by sensors and...In the digital age,non-touch communication technologies are reshaping human-device interactions and raising security concerns.A major challenge in current technology is the misinterpretation of gestures by sensors and cameras,often caused by environmental factors.This issue has spurred the need for advanced data processing methods to achieve more accurate gesture recognition and predictions.Our study presents a novel virtual keyboard allowing character input via distinct hand gestures,focusing on two key aspects:hand gesture recognition and character input mechanisms.We developed a novel model with LSTM and fully connected layers for enhanced sequential data processing and hand gesture recognition.We also integrated CNN,max-pooling,and dropout layers for improved spatial feature extraction.This model architecture processes both temporal and spatial aspects of hand gestures,using LSTM to extract complex patterns from frame sequences for a comprehensive understanding of input data.Our unique dataset,essential for training the model,includes 1,662 landmarks from dynamic hand gestures,33 postures,and 468 face landmarks,all captured in real-time using advanced pose estimation.The model demonstrated high accuracy,achieving 98.52%in hand gesture recognition and over 97%in character input across different scenarios.Its excellent performance in real-time testing underlines its practicality and effectiveness,marking a significant advancement in enhancing human-device interactions in the digital age.展开更多
By means of pre-compressive creep treatment, the cubic γ′ phase in a nickel base single crystal superalloy is transformed into the P-type rafted structure. And the influence of the pre-compressive creep on the inter...By means of pre-compressive creep treatment, the cubic γ′ phase in a nickel base single crystal superalloy is transformed into the P-type rafted structure. And the influence of the pre-compressive creep on the internal friction stress and creep lifetimes of the superalloy are investigated by means of the measurement of the creep curves and microstructure observation. Results show that, compared to the P-type structure alloy, the full heat treated state alloy displays a bigger internal friction stress value of dislocation motion during steady state creep and a longer creep lifetimes. The creep activation energies of the full heat treated and P-type structures alloys are measured to be 462 kJ/mol and 412 kJ/mol, respectively. Thereinto, the P-type rafted γ′ phase in the alloy is transformed into the N-type structure during tensile creep. And the N-type γ′ phase transformed from the P-type structure displays a shorter size in length, this is a main reason of the P-type structure alloy possessing a shorter creep lifetimes due to creep dislocation moving easily over the rafted γ′ phase.展开更多
A special designed experiment was conducted for observing crack initiation and growth in P/M Rene95 superalloy under tension-tension loading by self-made SEM in-situ fatigue loading stag. Several alumina inclusion par...A special designed experiment was conducted for observing crack initiation and growth in P/M Rene95 superalloy under tension-tension loading by self-made SEM in-situ fatigue loading stag. Several alumina inclusion particles exposed at the specimen surface were observed carefully. During fatigue test inclusions led to cracks initiation. The cracks can be formed by two mechanisms. Generally, the cracks nucleated at the interface between inclusion and matrix. Sometimes, cracks were also formed inside the inclusion. As the increase of cycles, some cracks at the interface between inclusion and matrix broadened and propagated along the direction about 45 degrees to the loading axis. On the other hand, the cracks inside the inclusion propagated in the inclusion and towards matrix.展开更多
In this paper,the microstructure and hydrogen embrittlement(HE) susceptibility of an Fe-Ni-Co based superalloy with different contents of trace elements,P and Mn,have been investigated.The results indicated that by lo...In this paper,the microstructure and hydrogen embrittlement(HE) susceptibility of an Fe-Ni-Co based superalloy with different contents of trace elements,P and Mn,have been investigated.The results indicated that by lowering the contents of trace elements P and Mn,the size and distribution of γ' become more homogeneous,and the precipitation of stable phase η can be retarded to longer ageing time.As a result,the hydrogen resistant properties of the alloy are obviously improved.展开更多
This paper examines the interface development between a single crystalline Ag matrix and core-shell AgnCom nanoclusters that have been deposited with energies varying between 0.25 eV and 1.5 eV per atom using computer...This paper examines the interface development between a single crystalline Ag matrix and core-shell AgnCom nanoclusters that have been deposited with energies varying between 0.25 eV and 1.5 eV per atom using computer modeling techniques. Clusters undergo deformation as a result of the slowing down;they may also become epitaxial with the substrate and maintain their core-shell structure. A detailed analysis of the effects of the cluster-surface interaction is conducted over a realistic size and energy range, and a model is created to show how clusters accumulate. It is discovered that both the silver shells and the cobalt cluster cores exhibit limited epitaxy with the substrate, and that the contact produced is only a few atomic layers thick. The effect is higher for Ag shells than for Co cores, and it is not very energy dependent.展开更多
基金Projects(2010CB631200,2010CB631206)supported by the National Basic Research Program of ChinaProject(50931004)supported by the National Natural Science Foundation of China
文摘The precipitation behavior of carbide in K416 B superalloy was investigated by means of creep measurement and microstructure observation. The results show that nanometer M6 C particles discontinuously precipitate in the γ matrix or along the γ/γ′ interface of the alloy during high temperature tensile creep. Thereinto, the amount of fine M6 C carbide increases as creep goes on, and the coherent interfaces of M6 C phase precipitating from the γ matrix are {100} and {111} planes. The thermodynamics analysis indicates that the solubility of element carbon in the matrix decreases when the alloy is deformed by the axial tensile stress during creep, so as to cause the carbon segregating in the regions of stress concentration and combining with carbide-forming elements M(W, Co), which promotes the fine M6 C carbide to precipitate from the γ matrix.
文摘High temperature oxidation behaviors of FGH96 P/M superaUoy have been studied in air at temperatures ranging from 600 to 1000℃. By means of isothermal oxidation testing, X-ray diffraction, SEM (scanning electron microscopy), and EDS (energy dispersive X-ray spectroscopy) analyses, the oxidation kinetics as well as the composition and morphology of scales were investigated. Thermodynamic calculations were used to explain the oxidation mechanism. The results showed that as the oxidation temperature increased, the oxidation rate, the scale thickness, and scale spallation increased. FGH96 P/M superalloy exhibits good oxidation resistance at temperature below 800℃. The oxidation kinetics follows an approximately parabolic rate law, and the oxide layer was mainly composed of Cr2O3 TiO2 and a little amount of NiCr2O4. The oxidation is controlled by the transmission of chromium. titanium, and oxygen through the oxide scale.
文摘In situ fatigue tests in special designed SEM were conducted to trace the whole process of crack initiation and propagation fill to fracture in mckel-base P/M superalloy seeded inclusions. The experimental results show that non-metallic inclusions can induce crack initiation. When the inclusion size is larger than the critical one, the crack can propagate as the main crack that induces the specimen to fracture. As a result, the LCF life of the specimen decreases.
基金supported by the Youth Development Project of Air Force Military Medical University,No.21 QNPY072Key Project of Shaanxi Provincial Natural Science Basic Research Program,No.2023-JC-ZD-48(both to FF)。
文摘Elevated intraocular pressure(IOP)is one of the causes of retinal ischemia/reperfusion injury,which results in NRP3 inflammasome activation and leads to visual damage.Homerla is repo rted to play a protective role in neuroinflammation in the cerebrum.However,the effects of Homerla on NLRP3inflammasomes in retinal ischemia/reperfusion injury caused by elevated IOP remain unknown.In our study,animal models we re constructed using C57BL/6J and Homer1^(flox/-)/Homerla^(+/-)/Nestin-Cre^(+/-)mice with elevated IOP-induced retinal ischemia/repe rfusion injury.For in vitro expe riments,the oxygen-glucose deprivation/repe rfusion injury model was constructed with M uller cells.We found that Homerla ove rexpression amelio rated the decreases in retinal thickness and Muller cell viability after ischemia/reperfusion injury.Furthermore,Homerla knockdown promoted NF-κB P65^(Ser536)activation via caspase-8,NF-κB P65 nuclear translocation,NLRP3 inflammasome formation,and the production and processing of interleukin-1βand inte rleukin-18.The opposite results we re observed with Homerla ove rexpression.Finally,the combined administration of Homerla protein and JSH-23 significantly inhibited the reduction in retinal thickness in Homer1^(flox/-)Homer1a^(+/-)/Nestin-Cre^(+/-)mice and apoptosis in M uller cells after ischemia/reperfusion injury.Taken together,these studies demonstrate that Homer1a exerts protective effects on retinal tissue and M uller cells via the caspase-8/NF-KB P65/NLRP3 pathway after I/R injury.
文摘Super-clean and super-spherical FGH4095 superalloy powder is produced by the ceramic-free electrode inductionmelt inert gas atomization(EIGA) technique.A continuous and steady-state liquid metal flow is achieved at high-frequency(350 k Hz) alternating current and high electric power(100 k W).The superalloy is immersed in a high-frequency induction coil,and the liquid metal falling into a supersonic nozzle is atomized by an Ar gas of high kinetic gas energy.Numerical calculations are performed to optimize the structure parameters for the nozzle tip.The undesired oxidation reaction of alloying elements starts at 1000℃ with the reaction originating from the active sites on the powder surfaces,leading to the formation of oxides,MexOy.The role of active sites and kinetic factors associated with the diffusion of oxygen present in the atomization gas streams are also examined.The observed results reveal that the oxidation process occurring at the surface of the produced powders gradually moves toward the core,and that there exists a clear interface between the product layer and the reactant.The present study lays a theoretical foundation for controlling the oxidation of nickel-based superalloy powders from the powder process step.
基金supported by the Postdoctoral Science Foundation of China
文摘The rupture behavior of a cast Ni-base superalloy M963 at high temperature has been investi- gated. The microstructure examination shows that there exists a large amount of the carbide and γ-γ' eutectic, which is very harmful to the mechanical properties of M963 superalloy. The tensile strength of M963 superalloy both at room temperature and at high temperatures is higher than that of K17G alloy, but the tensile ductility of the former is much lower than that of the latter. In tensile fracture process with the high strain rate, the open carbides are the initiation site and the carbide/matrix interface is the propagation path of cracks. But in fracture process with the low strain rate, the carbide/matrix interface and cast microvoids are the initiation sites, and the carbide/matrix interface is the propagation path of cracks. The effective ways to improve ductility of M963 superalloy are also suggested.
基金supported by the Natural Science Foundation of Xinjiang Uygur Autonomous Region of China(grant No.2021D01B112)Tianshan Talent Training Program through the grant 2023TSYCCX0101。
文摘In this work,we report observations of three comets:38P/Stephan-Oterma,64P/Swift-Gehrels,and C/2017 M4(ATLAS),conducted with the Nanshan one-meter wide-field telescope in 2018 August and November,and 2019January.We extracted morphological features through image enhancement techniques and calculated the dust activity parameter,Afρ,along with dust mass loss rates and coma color indices using broadband photometric data.Our morphological analysis uncovered a spectrum of dust characteristics among the observed comets,ranging from a significant twisted structure in comet 38P/Stephan-Oterma’s coma to the regular coma envelope surrounding comet 64P/Swift-Gehrels.The Afρvalues varied between 148.8±0.3 cm for 64P/Swift-Gehrels and1118.5±6.2 cm for C/2017 M4(ATLAS)(measured within a reference aperture radius ofρ=6″),indicating a range from moderate to high activity levels.Dust mass loss rates were estimated from 328.1 kg s^(-1)for comet 64P/Swift-Gehrels to 1395.5 kg s^(-1)for comet C/2017 M4(ATLAS).The color indices of comets 38P/Stephan-Oterma and C/2017 M4(ATLAS)closely resemble the average colors of active short-period comets and active longperiod comets,respectively.In contrast,64P/Swift-Gehrels exhibits a significantly bluer hue than typical Jupiter family comets.
文摘In the digital age,non-touch communication technologies are reshaping human-device interactions and raising security concerns.A major challenge in current technology is the misinterpretation of gestures by sensors and cameras,often caused by environmental factors.This issue has spurred the need for advanced data processing methods to achieve more accurate gesture recognition and predictions.Our study presents a novel virtual keyboard allowing character input via distinct hand gestures,focusing on two key aspects:hand gesture recognition and character input mechanisms.We developed a novel model with LSTM and fully connected layers for enhanced sequential data processing and hand gesture recognition.We also integrated CNN,max-pooling,and dropout layers for improved spatial feature extraction.This model architecture processes both temporal and spatial aspects of hand gestures,using LSTM to extract complex patterns from frame sequences for a comprehensive understanding of input data.Our unique dataset,essential for training the model,includes 1,662 landmarks from dynamic hand gestures,33 postures,and 468 face landmarks,all captured in real-time using advanced pose estimation.The model demonstrated high accuracy,achieving 98.52%in hand gesture recognition and over 97%in character input across different scenarios.Its excellent performance in real-time testing underlines its practicality and effectiveness,marking a significant advancement in enhancing human-device interactions in the digital age.
基金Supported by the National Natural Science Foundation of China (No 50571070)
文摘By means of pre-compressive creep treatment, the cubic γ′ phase in a nickel base single crystal superalloy is transformed into the P-type rafted structure. And the influence of the pre-compressive creep on the internal friction stress and creep lifetimes of the superalloy are investigated by means of the measurement of the creep curves and microstructure observation. Results show that, compared to the P-type structure alloy, the full heat treated state alloy displays a bigger internal friction stress value of dislocation motion during steady state creep and a longer creep lifetimes. The creep activation energies of the full heat treated and P-type structures alloys are measured to be 462 kJ/mol and 412 kJ/mol, respectively. Thereinto, the P-type rafted γ′ phase in the alloy is transformed into the N-type structure during tensile creep. And the N-type γ′ phase transformed from the P-type structure displays a shorter size in length, this is a main reason of the P-type structure alloy possessing a shorter creep lifetimes due to creep dislocation moving easily over the rafted γ′ phase.
基金the National Natural Science Foundation of China, No. 59871007.]
文摘A special designed experiment was conducted for observing crack initiation and growth in P/M Rene95 superalloy under tension-tension loading by self-made SEM in-situ fatigue loading stag. Several alumina inclusion particles exposed at the specimen surface were observed carefully. During fatigue test inclusions led to cracks initiation. The cracks can be formed by two mechanisms. Generally, the cracks nucleated at the interface between inclusion and matrix. Sometimes, cracks were also formed inside the inclusion. As the increase of cycles, some cracks at the interface between inclusion and matrix broadened and propagated along the direction about 45 degrees to the loading axis. On the other hand, the cracks inside the inclusion propagated in the inclusion and towards matrix.
文摘In this paper,the microstructure and hydrogen embrittlement(HE) susceptibility of an Fe-Ni-Co based superalloy with different contents of trace elements,P and Mn,have been investigated.The results indicated that by lowering the contents of trace elements P and Mn,the size and distribution of γ' become more homogeneous,and the precipitation of stable phase η can be retarded to longer ageing time.As a result,the hydrogen resistant properties of the alloy are obviously improved.
文摘This paper examines the interface development between a single crystalline Ag matrix and core-shell AgnCom nanoclusters that have been deposited with energies varying between 0.25 eV and 1.5 eV per atom using computer modeling techniques. Clusters undergo deformation as a result of the slowing down;they may also become epitaxial with the substrate and maintain their core-shell structure. A detailed analysis of the effects of the cluster-surface interaction is conducted over a realistic size and energy range, and a model is created to show how clusters accumulate. It is discovered that both the silver shells and the cobalt cluster cores exhibit limited epitaxy with the substrate, and that the contact produced is only a few atomic layers thick. The effect is higher for Ag shells than for Co cores, and it is not very energy dependent.