Different structure models of a long-period ordered phase in Fe-C martenstie formed during aging have been checked by computer simulation of electron diffraction(ED) patterns based on these models.The results showed t...Different structure models of a long-period ordered phase in Fe-C martenstie formed during aging have been checked by computer simulation of electron diffraction(ED) patterns based on these models.The results showed that the simulated ED pattern of γ'-FexC(Ⅱ) model proposed by the present authors is in good agreement with experimentally observed ED pattern.It was also confirmed that the incommensurate superperiod stems from the coexistence of several γ'-Fe_xC(H) phases with different superperiods.The Fe(144)C(24)(Fe6C) model proposed by Uwakweh et al.generated ED patterns remarkably different from the experimental ones.展开更多
The forms and structures of the phases in Fe-Ni-Co-Nb-Ti-Si low expansion superal-loys have been studied using analytical electron microscopy, high resolution electron microscopy, chemical phase analysis, X-ray diffra...The forms and structures of the phases in Fe-Ni-Co-Nb-Ti-Si low expansion superal-loys have been studied using analytical electron microscopy, high resolution electron microscopy, chemical phase analysis, X-ray diffraction, etc. The effects of yttrium on the microstructures and properties in the superalloys have also been investigated. The results reveal that trace yttrium mainly located in the platelet precipitates makes the crystal structure changed. The platelet precipitates become smaller, denser and rather homogeneous with appropriate yttrium addition. Compared with the conventional low expansion superalloy, the misfit of the platelet phase with the matrix in the yttrium-containing low expansion superalloy decreases from 0.7% to 0.07%, which indicates very low stress at the interface.展开更多
A new type of long periodic structure has been found in ZrO2-Y2O3 ceramics in annealed states. High resolution electron microscopy (HREM), selected area electron diffraction, and computer simulation have been used to ...A new type of long periodic structure has been found in ZrO2-Y2O3 ceramics in annealed states. High resolution electron microscopy (HREM), selected area electron diffraction, and computer simulation have been used to reveal the presence of the long periodic structure. The unit cell of the long periodic structure consists of a cubic ZrO2 unit cell and L10- like phase one.展开更多
With transmission electron microscope, it has been observed and analyzed that the dislocation arrangements and the fatigue damage of eutectoid present in welded metals which are loaded at different fatigue loads and l...With transmission electron microscope, it has been observed and analyzed that the dislocation arrangements and the fatigue damage of eutectoid present in welded metals which are loaded at different fatigue loads and load cycles. The results indicated that the character of fatigue damage in ferrites of welded metals is the dislocation arrangement change and eutectoids of welded metals are the broken cementites. This may produce microcracks.展开更多
A new modulated structure consisting of periodic （1120） stacking faults （SFs） in the α-Fe2O3 nanowires （NWs） formed by the thermal oxidation of Fe foils is reported, using a combination of high-resolution trans...A new modulated structure consisting of periodic （1120） stacking faults （SFs） in the α-Fe2O3 nanowires （NWs） formed by the thermal oxidation of Fe foils is reported, using a combination of high-resolution transmission electron microscopy （HRTEM） observations and HRTEM image simulations. The periodicity of the modulated structure is 1.53 nm, which is ten times （3500） interplanar spacing and can be described by a shift of every ten （3500） planes with 1/2 the interplanar spacing of the （1120） plane. An atomic model for the Fe203 structure is proposed to simulate the modulated structure. HRTEM simulation results confirm that the modulated structure in α-Fe2O3 NWs is caused by SFs.展开更多
文摘Different structure models of a long-period ordered phase in Fe-C martenstie formed during aging have been checked by computer simulation of electron diffraction(ED) patterns based on these models.The results showed that the simulated ED pattern of γ'-FexC(Ⅱ) model proposed by the present authors is in good agreement with experimentally observed ED pattern.It was also confirmed that the incommensurate superperiod stems from the coexistence of several γ'-Fe_xC(H) phases with different superperiods.The Fe(144)C(24)(Fe6C) model proposed by Uwakweh et al.generated ED patterns remarkably different from the experimental ones.
基金Chinese foundation of aeronautical science( N o.96 G2 10 0 3)
文摘The forms and structures of the phases in Fe-Ni-Co-Nb-Ti-Si low expansion superal-loys have been studied using analytical electron microscopy, high resolution electron microscopy, chemical phase analysis, X-ray diffraction, etc. The effects of yttrium on the microstructures and properties in the superalloys have also been investigated. The results reveal that trace yttrium mainly located in the platelet precipitates makes the crystal structure changed. The platelet precipitates become smaller, denser and rather homogeneous with appropriate yttrium addition. Compared with the conventional low expansion superalloy, the misfit of the platelet phase with the matrix in the yttrium-containing low expansion superalloy decreases from 0.7% to 0.07%, which indicates very low stress at the interface.
文摘A new type of long periodic structure has been found in ZrO2-Y2O3 ceramics in annealed states. High resolution electron microscopy (HREM), selected area electron diffraction, and computer simulation have been used to reveal the presence of the long periodic structure. The unit cell of the long periodic structure consists of a cubic ZrO2 unit cell and L10- like phase one.
文摘With transmission electron microscope, it has been observed and analyzed that the dislocation arrangements and the fatigue damage of eutectoid present in welded metals which are loaded at different fatigue loads and load cycles. The results indicated that the character of fatigue damage in ferrites of welded metals is the dislocation arrangement change and eutectoids of welded metals are the broken cementites. This may produce microcracks.
基金Project supported by the National Key Basic Research Development Program of China (Grant No.2012CB722705)the Natural Science Foundation for Outstanding Young Scientists in Shandong Province,China (Grant No.JQ201002)+2 种基金the Program for Foreign Cultural and Educational Experts (Grant No.20123702083)the Program for Higher Education Science and Technology in Shandong Province (Grant No.J12LA17)Wang Yi-Qian would like to thank the financial support from Taishan Outstanding Overseas Scholar Program of Shandong Province,China
文摘A new modulated structure consisting of periodic （1120） stacking faults （SFs） in the α-Fe2O3 nanowires （NWs） formed by the thermal oxidation of Fe foils is reported, using a combination of high-resolution transmission electron microscopy （HRTEM） observations and HRTEM image simulations. The periodicity of the modulated structure is 1.53 nm, which is ten times （3500） interplanar spacing and can be described by a shift of every ten （3500） planes with 1/2 the interplanar spacing of the （1120） plane. An atomic model for the Fe203 structure is proposed to simulate the modulated structure. HRTEM simulation results confirm that the modulated structure in α-Fe2O3 NWs is caused by SFs.
