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吹扫-捕集-气质联用法分析测定侧柏挥发物 被引量:4
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作者 武晓颖 许志春 +2 位作者 关玲 金幼菊 陈华君 《生态学报》 CAS CSCD 北大核心 2009年第10期5708-5712,共5页
采用吹扫捕集-气质联用法分析了侧柏(Platycladus orientalisL.)韧皮部的挥发物,并与常用的热脱附-气质联用法进行了比较。结果表明,仅用0.2g材料,吹扫5min即可得到较好的分离鉴定结果,通过增加2min反吹时间能明显降低空气峰和水峰的影... 采用吹扫捕集-气质联用法分析了侧柏(Platycladus orientalisL.)韧皮部的挥发物,并与常用的热脱附-气质联用法进行了比较。结果表明,仅用0.2g材料,吹扫5min即可得到较好的分离鉴定结果,通过增加2min反吹时间能明显降低空气峰和水峰的影响;该方法测得的各组分与热脱附法测的组分种类相同,均检测到9种单萜和3种倍半萜,但各组分在相对含量上有差异。与热脱附法相比,吹扫捕集法具有采样量少,不受吸附剂干扰和不受穿透体积影响的特点,有利于低沸点挥发物的测定,适于针叶植物挥发物的快速检测。 展开更多
关键词 吹扫捕集-气质联用法 热脱附-气质联用法 侧柏韧皮部 挥发物
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Electroantennogram responses of Adosomus sp. to volatile components from Artemisia ordosica
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作者 LIU Ai-jie YAN Wei +1 位作者 LUO You-qing ZONG Shi-xiang 《Forestry Studies in China》 CAS 2010年第4期223-227,共5页
Adosomus sp. eats the leaves and oviposits on the stems ofArtemisia ordosica Krasch. Based on an analytical PTI-GC/MS method, 21 volatile organic compounds (VOCs) from the leaves ofA. ordosica were identified. The m... Adosomus sp. eats the leaves and oviposits on the stems ofArtemisia ordosica Krasch. Based on an analytical PTI-GC/MS method, 21 volatile organic compounds (VOCs) from the leaves ofA. ordosica were identified. The major operating equipment consisted of a DB-5 column (30 m × 0.32 mm × 0.25 μm) and a flame ionization detector (FID). The amounts of the components from VOCs were determined by a peak area normalization method and 17 VOC components were identified by PTI-GC/MS. The elec- troantennogram (EAG) responses ofAdosomus sp. to 17 of the VOCs were tested. The results show that seven compounds, i.e., oci- mene, myrcene, R-(+)-α-pinene, caryophyllene, S-(+)-2-canene, humulene and (+)limonene elicited strong EAG responses by female Adosomus sp., with myrcene and ocimene eliciting the strongest responses. It is interesting to note that male Adosomus sp. presented different EAG responses from females to those compounds. Four volatile compounds: β-pinene, myrcene, trans-ocimene and longipinene elicited strong EAG responses to males with myrcene eliciting the strongest response. 展开更多
关键词 Artemisia ordosica Adosomus sp. pti-gc-ms electroantennogram responses
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