This paper describes a simple method for the preparation of L-proline stationary phase bonded to silica gel and characterization of the bonded phase by IR spectrometry, elemental analysis and nitrogen adsorption metho...This paper describes a simple method for the preparation of L-proline stationary phase bonded to silica gel and characterization of the bonded phase by IR spectrometry, elemental analysis and nitrogen adsorption method at low temperature.The enantiomeric resolutions of 3-(2-pyridyl)-3-aminopropionic acid and 2,3-diaminobutanoic acid on the bonded phase were carried out.展开更多
A simple and highly-efficient method for numerically evaluating the waves created by a ship that travels at a constant speed in calm water, of large depth or of uniform depth, is given. The method, inspired by Kelvin...A simple and highly-efficient method for numerically evaluating the waves created by a ship that travels at a constant speed in calm water, of large depth or of uniform depth, is given. The method, inspired by Kelvin's classical stationary-phase analysis, is suited for evaluating far-field as well as near-field waves. More generally, the method can be applied to a broad class of integrals with integrands that contain a rapidly oscillatory trigonometric function with a phase function whose first derivative(and possibly also higher derivatives) vanishes at one or several points, commonly called points of stationary phase, with the range of integration.展开更多
文摘This paper describes a simple method for the preparation of L-proline stationary phase bonded to silica gel and characterization of the bonded phase by IR spectrometry, elemental analysis and nitrogen adsorption method at low temperature.The enantiomeric resolutions of 3-(2-pyridyl)-3-aminopropionic acid and 2,3-diaminobutanoic acid on the bonded phase were carried out.
文摘A simple and highly-efficient method for numerically evaluating the waves created by a ship that travels at a constant speed in calm water, of large depth or of uniform depth, is given. The method, inspired by Kelvin's classical stationary-phase analysis, is suited for evaluating far-field as well as near-field waves. More generally, the method can be applied to a broad class of integrals with integrands that contain a rapidly oscillatory trigonometric function with a phase function whose first derivative(and possibly also higher derivatives) vanishes at one or several points, commonly called points of stationary phase, with the range of integration.