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REACTION OF α-(1H-1,2,4-TRIAZOL-1-YL)ACETOPHENONE WITH PHENYL ISOTHIOCYANATE
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作者 Zheng Ming LI Zhen Nian HUANG Institute of Elemento-Organic Chemistry,Nankai University,Tianjin,300071 《Chinese Chemical Letters》 SCIE CAS CSCD 1993年第9期763-766,共4页
Reaction of α-(1H-1,2,4-triazol-1-yl)acetophenone with phenyl isothiocyanate in the presence of a base and subse- quent alkylation leads to the ketene S,N-acetal(2),(4),(7), (8);thiazolidone(3),thiazolidine(5)and 1,3... Reaction of α-(1H-1,2,4-triazol-1-yl)acetophenone with phenyl isothiocyanate in the presence of a base and subse- quent alkylation leads to the ketene S,N-acetal(2),(4),(7), (8);thiazolidone(3),thiazolidine(5)and 1,3-thiazine(6), 展开更多
关键词 PH TRIAZOL-1-YL)ACETOPHENONE WITH phenyl isothiocyanate REACTION OF REV
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Synthesis and Crystal Structure of N-phenylthiocyano-phenyl-thioformamide bis(η_5-methylcyclopentadienyl)(tetrahydrofuran)Samarium(Ⅲ)
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作者 李焕荣 姚英明 +2 位作者 沈琪 王璐 郁开北 《Journal of Rare Earths》 SCIE EI CAS CSCD 2002年第5期370-373,共4页
The insertion reaction of phenyl isothiocyanate into the Ln S bond was studied. Phenyl isothiocyanate reacted with [(CH 3C 5H 4) 2Sm(SPh)(THF)] 2 to give the title complex, (CH 3C 5H 4) 2Sm[SC(SPh)NPh](THF),... The insertion reaction of phenyl isothiocyanate into the Ln S bond was studied. Phenyl isothiocyanate reacted with [(CH 3C 5H 4) 2Sm(SPh)(THF)] 2 to give the title complex, (CH 3C 5H 4) 2Sm[SC(SPh)NPh](THF), in good yield, which was characterized by elemental analyses, IR, 1H NMR and X ray structural determination. The crystal structure analysis of complex shows that samarium atom is coordinated by two CH 3C 5H 4 groups, one O atom of THF, and N and S atoms from the SC(SPh)NPh ligand to form a distorted trigonal bipyramidal geometry. 展开更多
关键词 rare earths SAMARIUM thiolate complex insertion reaction phenyl isothiocyanate
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Organic Reactions in Ionic Liquids:Ionic Liquid-promoted EfficientSynthesis of Disubstituted and Trisubstituted Thioureas Derivatives 被引量:1
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作者 ZhangGaoLE ZhenChuCHEN +1 位作者 YiHU QinGuoZHENG 《Chinese Chemical Letters》 SCIE CAS CSCD 2005年第2期201-204,共4页
In ionic liquid [Bmim][BF4], a series of disubstituted and trisubstituted thiourea derivativeswere synthesized from phenyl and butyl isothiocyanate with a variety of amine in excellent yield.
关键词 phenyl isothiocyanate butyl isothiocyanate THIOUREA ionic liquid.
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