The Influence of Ceramic Coating on Fatigue Crack Growth Behaviour of X17CrNi15-2 Stainless Steel

Fatigue crack growth tests were carried out on the SEN B3 precracked specimens, with dimensions in accordance with ISO 12108 requirements. The specimens were made of martensitic stainless steel, X17CrNi15-2, and some of them were modified by the ceramic coating deposition surface treatment. The effects of ceramic coating, on the fatigue crack growth behaviour of hollow shaft specimens, were experimentally investigated. Fatigue crack growth rates, da/dN, were characterised, using the power law relationship between da/dN (in mm/cycle) and the stress intensity factor range, ΔK (in MPa∙m0.5). The two constants of the correlation are 7.9768 × 10−9 and 2.8107 for the parent material, and those for the coated material are 2.4391 × 10−9 and 3.1990, respectively. Microstructural analyses were carried out on the tested specimens, which shows that the maximum hardness of the ceramic coating is higher than that of substrate by a factor of ~3.2. The dimple fracture dominates the final fracture mechanism for the parent material, and the combination of fatigue, ductile fracture and cleavage dominates the final fracture mechanism for the coated material, based on the SEM analyses. EDS tests’ results reveal that the parent material specimen shows higher levels of C at matrix regions along with Fe- and O-rich regions, compared with the coated material specimen.

Precracking and interfacial delamination in a bi-material structure:Static and dynamic loadings

The behavior of a precracked bi-material structure interface under given static and dynamic axial loading is an interest object in the present paper.Firstly,it is shown that the shear-lag model is a proper tool to analyze a delamination process in a precracked bi-material structure undergoing static loading.Secondly,the＂shear-lag model＂is applied to the structure under dynamic loading.To solve the problem for an interface delamination of the structure and to determine the debond length along the interface,our own 2D boundary element method（BEM）code is proposed in the case of static loading,and the shear-lag model together with the Laplace transforms and half-analytical calculations are used in the case of dynamic loading.The interface layer is assumed as a very thin plate compared with the other two.The parametric（geometric and elastic）analysis of the debond length and interface shear stress is done. The results from the 2D BEM code proved the validity of analytical solutions to the shear-lag model.In the dynamic case,the influence of loading characteristics,i.e.,frequencies and amplitude fluctuations on the shear stress and the value of debond length for an interval of time,is discussed. The analysis of the obtained results is illustrated by an example of the modern ceramic-metal composite,namely cermet, and depicted in figures.

Dynamic caustics test of blast load impact on neighboring different cross-section roadways

Using digital laser dynamic caustics experimental system and conducting simulation experiment researched the influence rule of blasting excavation of a new roadway on neighboring existed different cross-section roadways. The experimental results show that the influence of blast load on adjacent roadway has a good relationship with the cross-section of roadway. The expansion distance of precrack existed in circular, arch-wall, rectangular roadway is respectively 1.76, 1.61 and 0 cm under blast load.At the same time, the direct-blast side of rectangular roadway has more obvious damage compared with circular and arch-wall roadway. It explains that plane reflects more stress wave than arc, so that it exerts more tensile failure in the direct-blast side, which leads to less stress wave diffracting to the precrack in the back-blast side. When the precrack extends, higher value dynamic stress intensity factor in circular roadway works longer than that of arch-wall roadway. Indirectly, it explains that plane's weakening function on stress wave is significantly stronger than arc. Stress wave brings about self-evident influence on the upper and bottom endpoints of the rectangular roadway, and it respectively extends 1.03, 2.06 cm along the line link direction of the center of the blasthole and the upper and bottom endpoints on the right wall.

Fracture behavior and acoustic emission characteristics of sandstone samples with inclined precracks

Sandstone samples with precracks of different dip angles were collected from a coal mine roof and subjected to uniaxial compression tests,and acoustic emission(AE)and scanning electron microscopy(SEM)were used to study how the crack dip angle affected the fracture mechanism.In the precracked sandstone samples,as the dip angle between the crack line and loading direction decreased,so did the peak stress and its completion time.The SEM observations revealed a fracture transition from tensile cleavage to shear slip,which was manifested by a microstructure change from aggregate to staggered.According to energy conversion,a decreased crack dip angle results in gradually decreasing total and dissipative peak energies,whose variation amplitudes at different stages are consistent with those of the peak stress of the samples.The decreased crack dip angle lowered the stress required to trigger the first appearance of AE energy peaks and ring-down counts,as well as shortening the period before the occurrence of the first AE peak signal.However,the AE energy and ring-down count during the failure stage after the stress peak increased gradually.A stepped increase was observed in the AE ring-down count curves,with each step corresponding to a jump in the stress-strain curve.From the characteristics of the AE signal of the fracture of a precracked rock sample,the occurrence of joints or faults in the rock mass can be reasonably inferred.This is expected to provide a new method and approach for predicting coal and rock dynamic disasters.

Studies on the preliminary cracking: The reasons why matrix catalytic function is indispensable for the catalytic cracking of feed with large molecular size

The matrix catalytic function when cracking the feed oil with large molecular size was systematically studied using three different catalyst configurations, including staged bed, partly mixed bed and completely mixed bed. Results showed that molecules in the feed oil with large molecular size indeed preferred to be first precracked on the matrix surface and then entered into the zeolite pores during the practical reaction process. Furthermore, the matrix catalytic function exhibited a great matrix-precracking ability to large feed molecules, which considerably increased the catalyst activity and the light oil selectivity. Besides the much better accessibility, the matrix-precracking ability was also from the similar capability to crack large feed hydrocarbons into the moderate fragments with that of the zeolite component. More interestingly, the interactions between the matrix catalytic function and the zeolite catalytic function made the catalyst not only exhibit much more catalytic advantages of the zeolite component, but also retain the matrix-precracking ability. As a result, the interactions enhanced the catalyst activity and improved the product distribution at the same time. The matrix catalytic function is indispensable for the catalytic cracking of feed with large molecular size, although the matrix component itself presented an inferior catalytic performance than the zeolite component did. (C) 2016 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by Elsevier B.V. and Science Press. All rights reserved.