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Design aspect of a novel L-shaped pulsed column for liquid–liquid extraction applications: Energy consumption and the characteristics velocity concept 被引量:3
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作者 Pouria Amani Elham Mohammadi Sahar Akhgar 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2018年第4期723-730,共8页
This article deals with the evaluation of the consumption of energy for a steady state solvent extraction in a novel L-shaped pulsed sieve-plate column, which is highly required for design and optimization of the peri... This article deals with the evaluation of the consumption of energy for a steady state solvent extraction in a novel L-shaped pulsed sieve-plate column, which is highly required for design and optimization of the periodic flow processes for industrial applications. In this regard, a comprehensive evaluation on the energy consumption in case of a pulsed flow for three different chemical systems is conducted and besides the influence of pulsation intensity, the effect of geometrical parameters including the plate spacing and the plate free area is investigated as well. Moreover, the concept of characteristic velocity models at flooding points is evaluated with respect to the variation of pressure drop along the column at different operational conditions. 展开更多
关键词 solvent extraction Pulsed plate column Pressure drop Energy consumption Pulsed flow Characteristic velocity
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Determination of Sulphonamide Antibiotics and Trimethoprim in Wastewater and Sludge Using Liquid Chromatography with Diode-Array Detection 被引量:1
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作者 Petra Zenatova Milada Vavrova Ludmila Mravcova Hana Lisa 《Journal of Environmental Science and Engineering(A)》 2012年第2期175-180,共6页
This paper investigates the occurrence of sulphonamide and diaminopyrimidine antibiotics in wastewater and sludge from wastewater treatment plants. In our experiment, they were isolated from wastewater using the solid... This paper investigates the occurrence of sulphonamide and diaminopyrimidine antibiotics in wastewater and sludge from wastewater treatment plants. In our experiment, they were isolated from wastewater using the solid phase extraction method. In the case of sludge, pressurized solvent extraction techniques were used followed by solid phase extraction. The solid phase extraction method was used for purification and concentration. Sulphonamide and diaminopyrimidine antibiotics were determined using high performance liquid chromatography with diode-array detection. The selected antibiotics were determined in real sludge samples collected from the wastewater treatment plant in Brno-Mod^ice and in real wastewater samples collected from the wastewater treatment plant located on the grounds of the University of Veterinary and Pharmaceutical Sciences in Brno, using the developed and optimized method. Analyses showed that real samples of wastewater contained sulphathiazole 11.82μg/L at the inflow (7.1 μg/L at the outflow), sulphapyridine 18.57 I.tg/L (12.2 μg/L), sulphamethazine 13.52 μg/L (8.44 μg/L), sulphamethoxazole 14.06 lag/L (9.34 Ixg/L) and trimethoprim 521.4 lag/L (422.29 μg/L). Here it is demonstrated that drugs are removed through the wastewater treatment procedure only partially. 展开更多
关键词 Drug residues ANTIBIOTICS SLUDGE WASTEWATER pressurized solvent extraction liquid chromatography.
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