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Bamboo Fiber Modified Asphalt Mixture Proportion Design and Road Performances Based on Response Surface Method
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作者 李海滨 SUN Jianmei +3 位作者 WANG Sirui ZHANG Mingming HU Yihong SHENG Yanping 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS CSCD 2023年第1期156-170,共15页
In order to comprehensively utilize the remaining bamboo residue of bamboo products,this paper presents a research on recycling the bamboo fibers from bamboo residue for improving the performance of the asphalt mixtur... In order to comprehensively utilize the remaining bamboo residue of bamboo products,this paper presents a research on recycling the bamboo fibers from bamboo residue for improving the performance of the asphalt mixtures.First of all,the basic performance parameters of sinocalamus affinis fiber,phyllostachys pubescens fiber,green bamboo fiber were tested and analyzed,and the optimal content and length were put forward.Then,the mix ratio design of the bamboo fiber modified asphalt mixture was further designed through the response surface method,and was verified the rationality of the mix ratio.Finally,the mixture specimens were made according to the experimental design mix ratio,and the high temperature,low temperature performance and moisture susceptibility of the bamboo fiber modified mixtures asphalt were tested.The results showed that the high temperature performance,low temperature performance and moisture susceptibility of bamboo fiber modified asphalt mixtures were improved compared with the performance of SBS modified asphalt mixture.When the length of bamboo fiber is 7.25 mm and the content of 0.22%,the road performance of the asphalt mixture was optimal.Consequentially,the decomposition of bamboo residue into bamboo fiber and its application in asphalt pavement can improve the reuse of bamboo waste,with remarkable environmental benefits and great promotion value. 展开更多
关键词 bamboo fiber response surface method asphalt mixture proportion design road performances bamboo waste
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Mechanical and Permeability Analysis and Optimization of Recycled Aggregate Pervious Concrete Based on Response Surface Method
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作者 Fan Li Xin Cai +2 位作者 Yanan Zhang Xingwen Guo Minmin Jiang 《Journal of Renewable Materials》 SCIE EI 2023年第4期1745-1762,共18页
In this paper,the effects of different influencing factors and factor interaction on the compressive strength and permeability of recycled aggregate pervious concrete(RAPC)were studied based on the response surface me... In this paper,the effects of different influencing factors and factor interaction on the compressive strength and permeability of recycled aggregate pervious concrete(RAPC)were studied based on the response surface method(RSM).By selecting the maximum aggregate size,water cement ratio and target porosity as design variables,combined with laboratory tests and numerical analysis,the influences of three factors on the compressive strength and permeability coefficient of RAPC were revealed.The regression equation of compressive strength and permeability coefficient of recycled aggregate pervious concrete were established based on RSM,and the response surface model was optimized to determine the optimal ratio of RAPC under the conditions of meeting the mechanical and permeability properties.The results show that the mismatch item of the model is not significant,the model is credible,and the accuracy and reliability of the test are high,but the degree of uncorrelation between the test data and the model is not obvious.The sensitivity of the three factors to the compressive strength is water cement ratio>maximum coarse aggregate particle size>target porosity,and the sensitivity to the permeability coefficient is target porosity>maximum coarse aggregate particle size>water cement ratio.The absolute errors of the model prediction results and the model optimization results are 1.28 MPa and 0.19 mm/s,and the relative errors are 5.06%and 4.19%,respectively.With high accuracy,RSM can match the measured results of compressive strength and permeability coefficient of RAPC. 展开更多
关键词 Recycled aggregate pervious concrete(RAPC) response surface method(RSM) MECHANICAL PERMEABILITY OPTIMIZATION
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Optimization of Supercritical Extraction Process of Laoshan Black Tea by Response Surface Methodology
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作者 Yongxin LIU Zhiguang LIU +11 位作者 Zengyu WANG Shuai ZHANG Guofeng YU Jianhong SUN Shoutao CAO Qiulin LIU Xulun WEI Cuishu LENG Fuhua MA Xuegang LI Yinlong WANG Shoujie NIE 《Agricultural Biotechnology》 CAS 2023年第1期98-101,共4页
[Objectives]Laoshan black tea was subjected to supercritical CO_(2) extraction. [Methods]The extraction conditions of Laoshan black tea were studied by an orthogonal experiment and optimized by response surface method... [Objectives]Laoshan black tea was subjected to supercritical CO_(2) extraction. [Methods]The extraction conditions of Laoshan black tea were studied by an orthogonal experiment and optimized by response surface methodology. [Results] The optimum extraction conditions of black tea extract by supercritical CO_(2) extraction were as follows: extraction pressure 23.53 MPa, extraction time 1.73 h, and extraction temperature 49.75 ℃, with which the extract yield could reach 5.15% theoretically. [Conclusions] Based on the traditional extraction process, a supercritical extraction method optimized by response surface methodology and a unique extraction process were formed, which enriches the extraction processes and methods of natural raw materials. 展开更多
关键词 Laoshan black tea Supercritical extraction response surface method
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Optimization of High-Protein Glutinous Rice Flour Production Using Response Surface Method 被引量:8
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作者 Kanjanapa EAKKANALUKSAMEE Jirarat ANUNTAGOOL 《Rice science》 SCIE CSCD 2020年第1期75-80,共6页
A response surface method was employed to study the effect of α-amylase concentration, hydrolysis temperature and time on the production of high protein glutinous rice flour(HPGRF). The suspension of glutinous rice f... A response surface method was employed to study the effect of α-amylase concentration, hydrolysis temperature and time on the production of high protein glutinous rice flour(HPGRF). The suspension of glutinous rice flour(15%) that contained 6.52% protein was gelatinized and subsequently hydrolyzed by thermostable α-amylase. The hydrolysis yielded 0.144–0.222 g/g HPGRF with 29.4%–45.4% protein content. Hydrolysis time exerted a significant effect, while enzyme concentration and hydrolysis temperature showed insignificant effect on the protein content and production yield of HPGRF. The result of response surface method showed that the optimum condition for the production of HPGRF that contained at least 36% protein was treating gelatinized 15% glutinous rice flour suspension with 0.90 Kilo Novo α-amylase Unit(KNU)/g α-amylase at 80 oC for 99 min. By carrying out the predicted hydrolysis condition, HPGRF with 35.9% protein and 61.8% carbohydrates was resulted. The process yielded 0.172 g/g HPGRF. HPGRF contained higher amount of essential amino acids compared to glutinous rice flour. HPGRF had higher solubility and lower swelling power, and also showed no pasting peak compared with glutinous rice flour. 展开更多
关键词 high protein flour glutinous rice Α-AMYLASE amino acid response surface method
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Reliability analysis for aeroengine turbine disc fatigue life with multiple random variables based on distributed collaborative response surface method 被引量:2
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作者 高海峰 白广忱 +1 位作者 高阳 鲍天未 《Journal of Central South University》 SCIE EI CAS CSCD 2015年第12期4693-4701,共9页
The fatigue life of aeroengine turbine disc presents great dispersion due to the randomness of the basic variables,such as applied load,working temperature,geometrical dimensions and material properties.In order to am... The fatigue life of aeroengine turbine disc presents great dispersion due to the randomness of the basic variables,such as applied load,working temperature,geometrical dimensions and material properties.In order to ameliorate reliability analysis efficiency without loss of reliability,the distributed collaborative response surface method(DCRSM) was proposed,and its basic theories were established in this work.Considering the failure dependency among the failure modes,the distributed response surface was constructed to establish the relationship between the failure mode and the relevant random variables.Then,the failure modes were considered as the random variables of system response to obtain the distributed collaborative response surface model based on structure failure criterion.Finally,the given turbine disc structure was employed to illustrate the feasibility and validity of the presented method.Through the comparison of DCRSM,Monte Carlo method(MCM) and the traditional response surface method(RSM),the results show that the computational precision for DCRSM is more consistent with MCM than RSM,while DCRSM needs far less computing time than MCM and RSM under the same simulation conditions.Thus,DCRSM is demonstrated to be a feasible and valid approach for improving the computational efficiency of reliability analysis for aeroengine turbine disc fatigue life with multiple random variables,and has great potential value for the complicated mechanical structure with multi-component and multi-failure mode. 展开更多
关键词 complicated mechanical structure reliability analysis multiple random variables multi-component and multi-failure mode distributed collaborative response surface method
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Optimization of Extraction Conditions for SOD in Sedum aizoon by the Response Surface Method 被引量:1
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作者 Mei WANG Jiru WU +1 位作者 Yanfang LIU Wendou WANG 《Asian Agricultural Research》 2017年第1期72-75,共4页
This paper aimed to optimize extracting conditions of SOD in Sedum aizoon by response surface method. First,the single factor optimization tests were carried out. Three single factors were time,p H and liquid-solid ra... This paper aimed to optimize extracting conditions of SOD in Sedum aizoon by response surface method. First,the single factor optimization tests were carried out. Three single factors were time,p H and liquid-solid ratio respectively. By Design expert 8. 0. 5 software,17 kinds of test scheme were designed. The protein yield of each scheme was obtained,and Design expert 8. 0. 5 software was used to conduct variance analysis and interactive analysis among factors,to obtain the corresponding mathematical model. The results showed that in single factor experiments,the optimal time was 1 h,p H was 7. 8,and liquid-solid ratio was 15:1. The interactive analysis indicated that the optimal scheme for extracting SOD in Sedum aizoon was time of 0. 98 h,p H of 7. 79,liquid-solid ratio of 13. 71:1. By the method of pyrogallol autoxidation,the extracted SOD enzyme activity was measured,namely 12 U/g. The results could provide a reference for further utilization and research of Sedum aizoon resource. 展开更多
关键词 Sedum aizoon SOD response surface method
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Vibration reliability analysis for aeroengine compressor blade based on support vector machine response surface method
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作者 高海峰 白广忱 《Journal of Central South University》 SCIE EI CAS CSCD 2015年第5期1685-1694,共10页
To ameliorate reliability analysis efficiency for aeroengine components, such as compressor blade, support vector machine response surface method(SRSM) is proposed. SRSM integrates the advantages of support vector mac... To ameliorate reliability analysis efficiency for aeroengine components, such as compressor blade, support vector machine response surface method(SRSM) is proposed. SRSM integrates the advantages of support vector machine(SVM) and traditional response surface method(RSM), and utilizes experimental samples to construct a suitable response surface function(RSF) to replace the complicated and abstract finite element model. Moreover, the randomness of material parameters, structural dimension and operating condition are considered during extracting data so that the response surface function is more agreeable to the practical model. The results indicate that based on the same experimental data, SRSM has come closer than RSM reliability to approximating Monte Carlo method(MCM); while SRSM(17.296 s) needs far less running time than MCM(10958 s) and RSM(9840 s). Therefore,under the same simulation conditions, SRSM has the largest analysis efficiency, and can be considered a feasible and valid method to analyze structural reliability. 展开更多
关键词 VIBRATION reliability analysis compressor blade support vector machine response surface method natural frequency
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Fluidity Influencing Factor Analysis and Ratio Optimization of New Filling Slurry Based on the Response Surface Method
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作者 Guanfeng Chang Xinzhu Hua +3 位作者 Xiao Liu Chen Li Enqian Wang Bingjun Sun 《Journal of Renewable Materials》 SCIE EI 2022年第5期1439-1458,共20页
The filling mining method is important in realizing the green mining of mineral resources.Aiming at the problems of land resource occupation,environmental pollution,and rational utilization of coal-based solid wastes ... The filling mining method is important in realizing the green mining of mineral resources.Aiming at the problems of land resource occupation,environmental pollution,and rational utilization of coal-based solid wastes such as coal gangue,fly ash,and desulfurization gypsum,a new paste filling material was developed with coal gangue,fly ash,and desulfurization gypsum as raw materials.The microstructure of the raw materials was analyzed by XRD and SEM.Combined with the Box-Behnken experimental design,the effect of each component on the fluidity of the filling slurry was analyzed through the response surface analysis.The significance of each component on its bleeding and fluidity was determined,and the optimal ratio of the filling slurry was obtained.Experimental results show that the microcosmic morphology of coal gangue,desulfurization gypsum,and gasification slag presents an irregular block and rough particle surface;the microcosmic morphology of fly ash and bottom slag presents first out spherical or quasi spherical particles.Moreover,obvious sintering traces exist on the surface of the bottom slag.The main crystal mineral of coal gangue and fly ash is SiO_(2),the desulfurization gypsum is composed of Ca(SO_(4))(H_(2)O)and Ca(CO_(3))crystal minerals,the gasification slag is composed of carbon and nitrogen compounds,and the main crystal mineral components in the bottom slag sample are SiO_(2) and Al_(x)Si_(y)O_(z) compounds.The order of significance of each key factor on slurry fluidity is as follows:C(desulfurization gypsum)>D(gasification slag and bottom slag 1:1)>A(coal gangue)>B(fly ash).The order of the significance of each key factor on slurry bleeding is as follows:B(fly ash)>C(desulfurization gypsum)>D(gasification slag and bottom slag 1:1)>A(coal gangue).Considering the material preparation,field application,and other conditions,the mass percentage of each factor content of the new paste filling material is as follows:49.5%coal gangue,8.3%fly ash,4.1%desulfurization gypsum,6.2%gasification slag,and 6.2%bottom slag. 展开更多
关键词 Coal-based solid waste filling slurry FLOWABILITY proportion optimization response surface method
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Influence of Operating Parameters on Unbalance in Rotating Machinery Using Response Surface Method
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作者 Ameya MMahadeshwar Sangram SPatil +1 位作者 Vishwadeep CHandikherkar Vikas M.Phalle 《Sound & Vibration》 2018年第5期12-21,共10页
Wide range of rotating machinery contains an inherent amount of unbalance which leads to increase in the vibration level and related faults.In this work,the effect of different operating conditions viz.the unbalanced ... Wide range of rotating machinery contains an inherent amount of unbalance which leads to increase in the vibration level and related faults.In this work,the effect of different operating conditions viz.the unbalanced weight,radius,speed and position of the rotor disc on the unbalance in rotating machine are studied experimentally and analyzed by using Response Surface Methodology(RSM).RSM is a technique which consists of mathematical and statistical methods to develop the relationship between the inputs and outputs of a system by distinct functions.L27 Orthogonal Array(OA)was developed by using Design of Experiments(DOE)according to which experimentation has been carried out.Three accelerometer sensors were mounted to record the vibration responses(accelerations)in radially vertical,horizontal and axial directions.The responses recorded as root mean square values are then analysed using RSM.The relationship between response and operating factors has been established by developing a second order,non-linear mathematical model.Analysis of variance(ANOVA)has been performed for verification of the developed mathematical models.Results obtained from the analysis show that the unbalance weight and speed are most significant operating conditions that contribute the most to the effect the unbalance has on the rotating spindle. 展开更多
关键词 Mechanical unbalance response surface method rotating machinery ANOVA design of experiments
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Optimization of Freeze-drying Protective Agents for Lactobacillus plantarum KLDS1.0391 by Response Surface Methodology
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作者 Jia Fang-fang Han Bing +2 位作者 Meng Xiang-chen Zhang Lu-ji Zhou Jin-yu 《Journal of Northeast Agricultural University(English Edition)》 CAS 2017年第2期74-80,共7页
In this study, the Single Factor Test(SFT) was used to optimize the pre-freezing conditions of L. plantarum KLDS1.0391(KLDS1.0391). Further, the Freeze-Drying Protective Agents(FDPA) of KLDS1.0391 was optimized by Res... In this study, the Single Factor Test(SFT) was used to optimize the pre-freezing conditions of L. plantarum KLDS1.0391(KLDS1.0391). Further, the Freeze-Drying Protective Agents(FDPA) of KLDS1.0391 was optimized by Response Surface Methodology(RSM). The optimum pretreatment conditions were as the follows: initial concentration of KLDS1.0391 was 1011 CFU · m L^(-1) and KLDS1.0391 was pre-freezed at –80℃ for 8 h to achieve the survival rate of 46.21%. The main components of FDPA were skim milk, sucrose, sodium glutamate and Tween-80. And the influence of four factors on the survival rate of KLDS1.0391 in freeze-drying was in order as the follows: skim milk>sucrose>Tween-80>sodium glutamate. The optimal FDPA composition was skim milk 11.3%, sucrose 9.8%, sodium glutamate 5.1% and Tween-80 0.2%. Under the above conditions, the survival rate of the cells was 82.98%. Comparing the predicted values, the relative error was 0.37% and the difference was not significant, which indicated that the established model could effectively reflect the actual protection of FDPA to KLDS1.0391. 展开更多
关键词 Lactobacillus plantarum response surface method freeze drying protective agent
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Optimization of the extraction process of total flavonoids from Trichosanthis Fructus by Box-Behnken response surface method combined with differential spectrophotometry
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作者 Qian Hu Wan-Zhi Qian +1 位作者 Chun-Cai Zou Hai-Yan Yan 《Journal of Hainan Medical University》 2021年第11期26-31,共6页
Objective:To optimize the extraction process of total flavones in Trichosanthis Fructus(composed of Trichosanthis pericarpium and Trichosanthis semen in certain proportion).Methods:The effects of the mixture ratio of ... Objective:To optimize the extraction process of total flavones in Trichosanthis Fructus(composed of Trichosanthis pericarpium and Trichosanthis semen in certain proportion).Methods:The effects of the mixture ratio of Trichosanthis pericarpium and Trichosanthis semen,ethanol concentration,ultrasonic extraction time and extraction temperature on the extraction rate of total flavonoids in Trichosanthis Fructus were investigated.The extraction process of total flavonoids in Trichosanthis Fructus was optimized by Box-Behnken response surface method combined with differential spectrophotometry.Results:The optimum extraction conditions of total flavonoids in Trichosanthis Fructus were as follows:The mixture ratio of Trichosanthis pericarpium and Trichosanthis semen was 4:6,the ethanol concentration was 70%,the ultrasonic extraction time was 60min and the extraction temperature was 40℃.Conclusion:Box-Behnken response surface method combined with differential spectrophotometry can optimize the extraction process of total flavonoids from Trichosanthis Fructus,which can provide reference for the extraction and application of total flavonoids in Trichosanthis Fructus. 展开更多
关键词 Trichosanthis pericarpium Semen Trichosanthis Total flavonoids Extraction process Box-Behnken response surface method
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Research and Optimization of Foshou Yam and Honey Nutritional Can by Response Surface Methodology
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作者 Siying CHEN Sui YU +1 位作者 Xia DENG Ting HU 《Agricultural Biotechnology》 CAS 2020年第6期156-161,共6页
[Objectives]This study was conducted to screen best process parameters for making Foshou yam and honey can.[Methods]The Foshou yam produced from Wuxue was used as a raw material to prepare Foshou yam and honey nutriti... [Objectives]This study was conducted to screen best process parameters for making Foshou yam and honey can.[Methods]The Foshou yam produced from Wuxue was used as a raw material to prepare Foshou yam and honey nutritional can by combining Foshou yam with honey through screening,pre-cooking,filling,exhausting,cooling and other technical processes.The optimum technology parameter of Foshou yam and honey nutritional can was studied through single factor tests and response surface optimization.[Results]The optimum technical parameters of Foshou yam and honey nutritional can were citric acid concentration 0.1%,amount of edible salt 0.1%,cooking time 14 min and honey concentration 26%.Under these conditions,the final sensory score was 90.20.The prepared can was not only rich in nutrition,but also had good flavor and taste.[Conclusions]This study provides reference for the development and utilization of Foshou yam and the research and development of functional food. 展开更多
关键词 Foshou yam HONEY CAN Single factor experiment response surface method
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Dynamic optimization analysis of hydraulic pipeline system based on a developed response surface method
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作者 Hongquan QU Jianlin SUN +5 位作者 Xu YAN Yuanlin ZHANG Xuefeng LIU Tao YU HuaweiHAN Langjun XU 《Mechanical Engineering Science》 2020年第2期7-14,I0004,共9页
When designing a complex pipeline with long distance and multi-supports for offshore platform,it is necessary to analyze the vibration characteristics of the complex pipeline system to ensure that there is no harmful ... When designing a complex pipeline with long distance and multi-supports for offshore platform,it is necessary to analyze the vibration characteristics of the complex pipeline system to ensure that there is no harmful resonance in the working conditions.Therefore,the optimal layout of support is an effective method to reduce the vibration response of hydraulic pipeline system.In this paper,a developed dynamic optimization method for the complex pipeline is proposed to investigate the vibration characteristics of complex pipeline with multi-elastic supports.In this method,the Kriging response surface model between the support position and pipeline is established.The position of the clamp in the model is parameterized and the optimal solution of performance index is obtained by genetic algorithm.The number of clamps and the interval between clamps are considered as the constraints of layout optimization,and the optimization objective is the natural frequencies of pipeline.Taking a typical offshore pipeline as example to demonstrate the effectiveness of the proposed method,the results show that the vibration performance of the hydraulic pipeline system is distinctly improved by the optimization procedure,which can provide reasonable guidance for the design of complex hydraulic pipeline system. 展开更多
关键词 Hydraulic pipeline Multi-Support response surface method Optimization analysis
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Box-Behnken response surface method combined with fingerprint to optimize the extraction process of total anthraquinone from Cassia seeds
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作者 Heng Wang Chun-Cai Zou Hai-Yan Yan 《Journal of Hainan Medical University》 2022年第7期26-34,共9页
Objective:The Box-Behnken response surface method combined with fingerprints was used to optimize the extraction process of total anthraquinone from Cassia seeds.Methods:A three-factor,three-level response surface tes... Objective:The Box-Behnken response surface method combined with fingerprints was used to optimize the extraction process of total anthraquinone from Cassia seeds.Methods:A three-factor,three-level response surface test was conducted based on the single-factor test with comprehensive evaluation as the measurement index.The comprehensive evaluation indexes included the extraction rate of total anthraquinone of Cassia seeds or the equivalent amount of herbs per gram of total anthraquinone of Cassia seeds,the normalized value of peak areas of 5 index components such as aurantio obtusin in the fingerprint of each sample to 16 shared peaks and the similarity of fingerprints(the reference fingerprint was established by the extraction solvent for the determination of Cassia seeds content in the Chinese Pharmacopoeia 2020 edition)with the weights of 0.2,0.5 and 0.3,respectively.Results:The best extraction process was obtained:the liquid-to-material ratio was 20:1(mL·g-1),the extraction solvent was mixture of 60%ethanol-ethyl acetate(2:1),and the extraction time was 15.12 min.The results of five sets of validation experiments showed that the overall evaluation of total anthraquinone of cassia seeds by the best process was 0.528(RSD=0.45%),and the prediction result of response surface method model was 0.531,and the relative error with the prediction result was 0.531.The relative error of the predicted results was 0.56%,and the best extraction process was consistent with the model prediction,and the obtained best process could be used for the extraction of total anthraquinone from Cassia seeds.Conclusion:The Box-Behnken response surface method combined with the fingerprint technique can be used to find the best reaction conditions and examine the interactions among the factors in a comprehensive and accurate manner,which can provide reference for the optimization and evaluation of the extraction process of Chinese medicine. 展开更多
关键词 Cassia seeds Total anthraquinone FINGERPRINT response surface design method
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Improved response surface method for anti-slide reliability analysis of gravity dam based on weighted regression 被引量:7
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作者 Jian-yun CHEN Qiang XY +2 位作者 Jing LI Shu-li FAN Qiang xu 《Journal of Zhejiang University-Science A(Applied Physics & Engineering)》 SCIE EI CAS CSCD 2010年第6期432-439,共8页
The aim of this study was to design and construct an improved response surface method(RSM) based on weighted regression for the anti-slide reliability analysis of concrete gravity dam.The limitation and lacuna of the ... The aim of this study was to design and construct an improved response surface method(RSM) based on weighted regression for the anti-slide reliability analysis of concrete gravity dam.The limitation and lacuna of the traditional RSM were briefly analyzed.Firstly,based on small experimental points,research was devoted to an improved RSM with singular value decomposition techniques.Then,the method was used on the basis of weighted regression and deviation coefficient correction to reduce iteration times and experimental points and improve the calculation method of checking point.Finally,a test example was given to verify this method.Compared with other conventional algorithms,this method has some strong advantages:this algorithm not only saves the arithmetic operations but also greatly enhances the calculation efficiency and the storage efficiency. 展开更多
关键词 response surface method(RSM) RELIABILITY Gravity dam Singular value decomposition Weighted regression Deviation coefficient
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Ferric ion-ascorbic acid complex catalyzed calcium peroxide for organic wastewater treatment:Optimized by response surface method 被引量:2
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作者 Deling Yuan Chen Zhang +5 位作者 Shoufeng Tang Zetao Wang Qina Sun Xiaoyu Zhang Tifeng Jiao Qingrui Zhang 《Chinese Chemical Letters》 SCIE CAS CSCD 2021年第11期3387-3392,共6页
Hydrogen peroxide(H_(2)O_(2))disproportionation,iron precipitation,and narrow pH range are the drawbacks of traditional Fenton process.To surmount these barriers,we proposed a ferric ion(Fe^(3+))-ascorbic acid(AA)comp... Hydrogen peroxide(H_(2)O_(2))disproportionation,iron precipitation,and narrow pH range are the drawbacks of traditional Fenton process.To surmount these barriers,we proposed a ferric ion(Fe^(3+))-ascorbic acid(AA)complex catalyzed calcium peroxide(CaO_(2))Fenton-like system to remove organic dyes in water.This collaborative Fe^(3+)/AA/CaO_(2)system presented an obvious improvement in the methyl orange(MO)decolorization,and also effectively eliminated other dyes.Response surface method was employed to optimize the running parameters for this coupling process.Under the optimized arguments(2.76 mmol/L Fe^(3+),0.68 mmol/L AA,and 4 mmol/L CaO_(2)),the MO removal achieved 98.90%after 15 min at pH 6.50,which was close to the computed outcome of 99.30%.Furthermore,this Fenton-like system could perform well in a wide range of pH(3-11),and enhance the H_(2)O_(2)decomposition and Fe ions recycle.The scavenger experiment result indicated that hydroxyl radical,superoxide anion free radical,and singlet oxygen were acted on the dye elimination.Moreover,electron spin resonance analysis corroborated that the existences of these active species in the Fe^(3+)/AA/CaO_(2)system.This study could advance the development of Fenton-like technique in organic effluent disposal. 展开更多
关键词 Ferric ion Ascorbic acid Calcium peroxide response surface method Dye removal
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Optimization of rare earth carbonate reactive-crystallization process based on response surface method 被引量:2
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作者 Dongmei Zhu Qianwen Chen +2 位作者 Tingsheng Qiu Guanfei Zhao Xihui Fang 《Journal of Rare Earths》 SCIE EI CAS CSCD 2021年第1期98-104,I0004,共8页
Rare earth carbonate precipitation is mainly amorphous,of large volume and difficult to filter.To prepare crystalline rare earth carbonate,mother liquor of heavy rare earth was taken as research object,and the experim... Rare earth carbonate precipitation is mainly amorphous,of large volume and difficult to filter.To prepare crystalline rare earth carbonate,mother liquor of heavy rare earth was taken as research object,and the experimental scheme was designed based on the response surface central composite design(CCD)method.The concentration of mother liquor,aging time and seed crystal dosage were taken as independent variables,and the particle size of rare earth carbonate was taken as the response value to establish a quadratic polynomial numerical model to optimize the reactive-crystallization process of rare earth carbonate.The results show that these three factors have significant effect on the particle size of rare earth carbonate,and the influence order is mother liquid concentration>aging time>seed crystal dosage.Moreover,the interaction between mother liquor concentration and seed crystal dosage has a significant effect on the size of rare earth carbonate particles.The optimal parameters predicted by the model are as follows:the concentration of mother liquid is 1.75 g/L,seed crystal dosage is 13.56 wt%,and aging time is 8 h.Under these conditions,the predicted particle size is 28.74μm,and the experiment particle size is 28.23μm,between both,the relative error is 0.73%,which indicates that the established response surface model has a good prediction effect and a certain practical significance to guide the reactive-crystallization process of rare earth carbonate.The obtained rare earth carbonate has a crystallinity of 97.82%,uniform particles size,and low-hydrated crystals with a tengerite structure. 展开更多
关键词 Rare earth carbonate Reactive-crystallization Process optimization response surface method Seed crystal
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Using the Box-Behnken Response Surface Method to Optimize the Preparation and Characterization of Lavender and Fennel Volatile oilβ-cyclodextrin Form Inclusion Complex 被引量:2
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作者 Yuan-Yuan Liu Guo-Song Zhang +3 位作者 Guang-Wei Zhu Ai-Ni-Wa-Er Aikemu Jia-Jia Ai Dong-Xun Li 《World Journal of Traditional Chinese Medicine》 2018年第2期54-61,共8页
Objective:The objective of this study is to study the best inclusion technology of Lavender-and fennel-mixed volatile oil by beta?cyclodextrin(β-CD) and characterize the final product thereafter.Methods:Using the sat... Objective:The objective of this study is to study the best inclusion technology of Lavender-and fennel-mixed volatile oil by beta?cyclodextrin(β-CD) and characterize the final product thereafter.Methods:Using the saturated water solution method,the volatile β-CD inclusion complex was produced.The effect of volatile oil weight ratio,inclusion temperature and inclusion time on the inclusive quality was studied by measuring the yield of inclusion and inclusion rate of volatile oil as evaluation indexes.The preparation method of inclusion complex was then optimized by the Box-Behnken response surface method.The inclusion complex was characterized by ultraviolet spectrophotometry,thin-layer chromatography,thermogravimetry and differential thermal analysis,and the microscopic imaging method.Results:The optimized conditions were the weight ratio of β-CD to volatile oil was 8.13:1(g/ml).The inclusion temperature was 44°C.The inclusion time was 1 h.Conclusion:We were able to produce an inclusion complex with high inclusion rate of volatile oil and high yield of inclusion using the preparation method mentioned above.Furthermore,the method can also improve the stability of volatile oil in abnormal savda munziq.This study can provide a good reference for the development of new preparations. 展开更多
关键词 FENNEL inclusion complex LAVENDER response surface method volatile oil Β-CYCLODEXTRIN
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Optimization via response surface methodology of the synthesis of a dust suppressant and its performance characterization for use in open cut coal mines 被引量:1
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作者 Hu Jin Yansong Zhang +2 位作者 Guangan Wu Junjie Yang Nan Li 《Journal of Environmental Sciences》 SCIE EI CAS CSCD 2022年第11期211-223,共13页
To relieve dust pollution in open cut coal mines and reduce the hazards of coal dust pollution to the environment and workers we optimized the synthesis of a dust suppressant by graft copolymerization of environmental... To relieve dust pollution in open cut coal mines and reduce the hazards of coal dust pollution to the environment and workers we optimized the synthesis of a dust suppressant by graft copolymerization of environmentally friendly soy protein isolate with methyl methacrylate.This dust suppressant could effectively control dust pollution in open cut coal mines. The optimized conditions for graft copolymerization in this case were determined by a response surface experiment designed with Design-Expert 10 software. Characterization by scanning electron microscopy showed a significant morphology change of the dust suppressant and the generation of a rigid and dense layer on its surface after interacting with coal dust.The layer exhibited good bonding and dust suppression performance. The analysis with Fourier-transform infrared spectroscopy revealed the appearance of new absorption peaks near 1300, 1072, and 1631 cm, demonstrating effective graft copolymerization. The proposed dust suppressant exhibited excellent wind erosion resistance, with a resistance that exceeded 90% at a wind speed of 6.5 m/sec. The successful graft copolymerization and effective bonding and curing of the dust suppressant on coal dust were experimentally verified.This is of great significance to the control of coal dust pollution. 展开更多
关键词 Environmental dust control Dust suppressant response surface method Graft copolymerization Performance characterization Single factor method
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Optimization of fermentation process of papaya sauerkraut using response surface method 被引量:1
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作者 Zhang Lijuan Yang Jinsong +1 位作者 Ma Liwei Tan Haisheng 《International Journal of Agricultural and Biological Engineering》 SCIE EI CAS 2014年第3期102-106,共5页
Papaya,a tropical fruit was used as the raw material to produce sauerkraut in the study.Three lactic acid bacteria strains isolated from papaya were added to the sauerkraut to facilitate the fermentation of papaya sau... Papaya,a tropical fruit was used as the raw material to produce sauerkraut in the study.Three lactic acid bacteria strains isolated from papaya were added to the sauerkraut to facilitate the fermentation of papaya sauerkraut.In the fermentation process,the dynamic changes of total acid in sauerkrauts at different levels of sugar concentration,salt concentration,inoculation and temperature were studied.The response surface method was used to study the effects of changes in multiple factors at the same time.On the basis of“one-variable-at-a-time”approach,the response surface method optimized papaya sauerkraut fermentation process.According to the change of total acid in single factor,29 experiments were designed by 4×3 factorial central composite design.The optimum fermentation conditions were obtained as follows:sugar at 3.8%,salt at 2.8%,inoculation at 5%,and temperature at 31℃. 展开更多
关键词 PAPAYA SAUERKRAUT fermentation process response surface method lactic acid bacteria central composite design
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