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新型含多吡啶Ru-Mn配合物的合成及其抗肿瘤活性
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作者 黄莉 耿艺 +3 位作者 王慧 熊一萍 张诗琪 王勇 《合成化学》 CAS 2024年第11期1007-1012,共6页
多吡啶钌配合物有着较强的生物活性、较低的毒性和较快的代谢速率等优点,被认为是最有潜力的非铂金属抗肿瘤药物。本文以物质的量之比为1∶1的单核化合物[Mn^(Ⅲ)(salen)](ClO_(4))]和K[Ru^(Ⅱ)(L)(CN)_(3)](L=4′-苯基-2,2′∶6′,2”... 多吡啶钌配合物有着较强的生物活性、较低的毒性和较快的代谢速率等优点,被认为是最有潜力的非铂金属抗肿瘤药物。本文以物质的量之比为1∶1的单核化合物[Mn^(Ⅲ)(salen)](ClO_(4))]和K[Ru^(Ⅱ)(L)(CN)_(3)](L=4′-苯基-2,2′∶6′,2”-三联吡啶)作为原料,设计并合成了新型含多吡啶Ru-Mn配合物[Ru^(Ⅱ)(L)(CN)_(3)][Mn^(Ⅲ)(salen)](1),利用元素分析、红外光谱、紫外-可见光谱和X-射线单晶衍射分析对其结构进行表征,并采用CCK8法研究了化合物1的抗肿瘤活性。结果表明:化合物1的单晶结构为正交晶系Pbca空间群,对Hela细胞生长有抑制作用,当其质量浓度为1000μg/mL时,Hela细胞的相对活性降低至65.82%。 展开更多
关键词 ru-mn配合物 多吡啶 合成 抗肿瘤活性 晶体结构
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Modeling time-dependent mechanical behavior of hard rock considering excavation-induced damage and complex 3D stress states 被引量:1
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作者 Peiyang Yu Xiuli Ding +3 位作者 Peng-Zhi Pan Shuting Miao Zhaofeng Wang Shuling Huang 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2024年第10期4046-4065,共20页
To investigate the long-term stability of deep rocks,a three-dimensional(3D)time-dependent model that accounts for excavation-induced damage and complex stress state is developed.This model comprises three main compon... To investigate the long-term stability of deep rocks,a three-dimensional(3D)time-dependent model that accounts for excavation-induced damage and complex stress state is developed.This model comprises three main components:a 3D viscoplastic isotropic constitutive relation that considers excavation damage and complex stress state,a quantitative relationship between critical irreversible deformation and complex stress state,and evolution characteristics of strength parameters.The proposed model is implemented in a self-developed numerical code,i.e.CASRock.The reliability of the model is validated through experiments.It is indicated that the time-dependent fracturing potential index(xTFPI)at a given time during the attenuation creep stage shows a negative correlation with the extent of excavationinduced damage.The time-dependent fracturing process of rock demonstrates a distinct interval effect of the intermediate principal stress,thereby highlighting the 3D stress-dependent characteristic of the model.Finally,the influence of excavation-induced damage and intermediate principal stress on the time-dependent fracturing characteristics of the surrounding rocks around the tunnel is discussed. 展开更多
关键词 Hard rock Excavation damage complex stress state Three-dimensional(3D)time-dependent model
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Saturation Estimation with Complex Electrical Conductivity for Hydrate-Bearing Clayey Sediments:An Experimental Study 被引量:1
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作者 XING Lanchang ZHANG Shuli +8 位作者 ZHANG Huanhuan WU Chenyutong WANG Bin LAO Liyun WEI Wei HAN Weifeng WEI Zhoutuo GE Xinmin DENG Shaogui 《Journal of Ocean University of China》 CAS CSCD 2024年第1期173-189,共17页
Clays have considerable influence on the electrical properties of hydrate-bearing sediments.It is desirable to understand the electrical properties of hydrate-bearing clayey sediments and to build hydrate saturation(S... Clays have considerable influence on the electrical properties of hydrate-bearing sediments.It is desirable to understand the electrical properties of hydrate-bearing clayey sediments and to build hydrate saturation(S_(h))models for reservoir evaluation and monitoring.The electrical properties of tetrahydrofuran-hydrate-bearing sediments with montmorillonite are characterized by complex conductivity at frequencies from 0.01 Hz to 1 kHz.The effects of clay and Sh on the complex conductivity were analyzed.A decrease and increase in electrical conductance result from the clay-swelling-induced blockage and ion migration in the electrical double layer(EDL),respectively.The quadrature conductivity increases with the clay content up to 10%because of the increased surface site density of counterions in EDL.Both the in-phase conductivity and quadrature conductivity decrease consistently with increasing Sh from 0.50 to 0.90.Three sets of models for Sh evaluation were developed.The model based on the Simandoux equation outperforms Archie’s formula,with a root-mean-square error(E_(RMS))of 1.8%and 3.9%,respectively,highlighting the clay effects on the in-phase conductivity.The fre-quency effect correlations based on in-phase and quadrature conductivities exhibit inferior performance(E_(RMS)=11.6%and 13.2%,re-spectively)due to the challenge of choosing an appropriate pair of frequencies and intrinsic uncertainties from two measurements.The second-order Cole-Cole formula can be used to fit the complex-conductivity spectra.One pair of inverted Cole-Cole parameters,i.e.,characteristic time and chargeability,is employed to predict S_(h) with an E_(RMS) of 5.05%and 9.05%,respectively. 展开更多
关键词 gas hydrate complex electrical conductivity hydrate-bearing clayey sediment hydrate saturation Simandoux equation frequency dispersion Cole-Cole formula
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A novel complex-high-order graph convolutional network paradigm:ChyGCN
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作者 郑和翔 苗书宇 顾长贵 《Chinese Physics B》 SCIE EI CAS CSCD 2024年第5期665-672,共8页
In recent years,there has been a growing interest in graph convolutional networks(GCN).However,existing GCN and variants are predominantly based on simple graph or hypergraph structures,which restricts their ability t... In recent years,there has been a growing interest in graph convolutional networks(GCN).However,existing GCN and variants are predominantly based on simple graph or hypergraph structures,which restricts their ability to handle complex data correlations in practical applications.These limitations stem from the difficulty in establishing multiple hierarchies and acquiring adaptive weights for each of them.To address this issue,this paper introduces the latest concept of complex hypergraphs and constructs a versatile high-order multi-level data correlation model.This model is realized by establishing a three-tier structure of complexes-hypergraphs-vertices.Specifically,we start by establishing hyperedge clusters on a foundational network,utilizing a second-order hypergraph structure to depict potential correlations.For this second-order structure,truncation methods are used to assess and generate a three-layer composite structure.During the construction of the composite structure,an adaptive learning strategy is implemented to merge correlations across different levels.We evaluate this model on several popular datasets and compare it with recent state-of-the-art methods.The comprehensive assessment results demonstrate that the proposed model surpasses the existing methods,particularly in modeling implicit data correlations(the classification accuracy of nodes on five public datasets Cora,Citeseer,Pubmed,Github Web ML,and Facebook are 86.1±0.33,79.2±0.35,83.1±0.46,83.8±0.23,and 80.1±0.37,respectively).This indicates that our approach possesses advantages in handling datasets with implicit multi-level structures. 展开更多
关键词 raph convolutional network complex modeling complex hypergraph
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Discovery of nano organo-clay complex pore-fractures in shale and its scientific significance:A case study of Cretaceous Qingshankou Formation shale,Songliao Basin,NE China
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作者 SUN Longde WANG Fenglan +5 位作者 BAI Xuefeng FENG Zihui SHAO Hongmei ZENG Huasen GAO Bo WANG Yongchao 《Petroleum Exploration and Development》 SCIE 2024年第4期813-825,共13页
A new pore type,nano-scale organo-clay complex pore-fracture was first discovered based on argon ion polishing-field emission scanning electron microscopy,energy dispersive spectroscopy and three-dimensional reconstru... A new pore type,nano-scale organo-clay complex pore-fracture was first discovered based on argon ion polishing-field emission scanning electron microscopy,energy dispersive spectroscopy and three-dimensional reconstruction by focused ion-scanning electron in combination with analysis of TOC,R_(o)values,X-ray diffraction etc.in the Cretaceous Qingshankou Formation shale in the Songliao Basin,NE China.Such pore characteristics and evolution study show that:(1)Organo-clay complex pore-fractures are developed in the shale matrix and in the form of spongy and reticular aggregates.Different from circular or oval organic pores discovered in other shales,a single organo-clay complex pore is square,rectangular,rhombic or slaty,with the pore diameter generally less than 200 nm.(2)With thermal maturity increasing,the elements(C,Si,Al,O,Mg,Fe,etc.)in organo-clay complex change accordingly,showing that organic matter shrinkage due to hydrocarbon generation and clay mineral transformation both affect organo-clay complex pore-fracture formation.(3)At high thermal maturity,the Qingshankou Formation shale is dominated by nano-scale organo-clay complex pore-fractures with the percentage reaching more than 70%of total pore space.The spatial connectivity of organo-clay complex pore-fractures is significantly better than that of organic pores.It is suggested that organo-complex pore-fractures are the main pore space of laminar shale at high thermal maturity and are the main oil and gas accumulation space in the core area of continental shale oil.The discovery of nano-scale organo-clay complex pore-fractures changes the conventional view that inorganic pores are the main reservoir space and has scientific significance for the study of shale oil formation and accumulation laws. 展开更多
关键词 Songliao Basin Cretaceous Qingshankou Formation laminar shale oil nanoscale organo-clay complex pore-fractures organo-clay complex diagenesis
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Complexity Considerations in the Heisenberg Uncertainty Principle
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作者 Logan Nye 《Journal of High Energy Physics, Gravitation and Cosmology》 CAS 2024年第4期1470-1513,共44页
This work introduces a modification to the Heisenberg Uncertainty Principle (HUP) by incorporating quantum complexity, including potential nonlinear effects. Our theoretical framework extends the traditional HUP to co... This work introduces a modification to the Heisenberg Uncertainty Principle (HUP) by incorporating quantum complexity, including potential nonlinear effects. Our theoretical framework extends the traditional HUP to consider the complexity of quantum states, offering a more nuanced understanding of measurement precision. By adding a complexity term to the uncertainty relation, we explore nonlinear modifications such as polynomial, exponential, and logarithmic functions. Rigorous mathematical derivations demonstrate the consistency of the modified principle with classical quantum mechanics and quantum information theory. We investigate the implications of this modified HUP for various aspects of quantum mechanics, including quantum metrology, quantum algorithms, quantum error correction, and quantum chaos. Additionally, we propose experimental protocols to test the validity of the modified HUP, evaluating their feasibility with current and near-term quantum technologies. This work highlights the importance of quantum complexity in quantum mechanics and provides a refined perspective on the interplay between complexity, entanglement, and uncertainty in quantum systems. The modified HUP has the potential to stimulate interdisciplinary research at the intersection of quantum physics, information theory, and complexity theory, with significant implications for the development of quantum technologies and the understanding of the quantum-to-classical transition. 展开更多
关键词 UNCERTAINTY complexITY QUANTUM MEASUREMENT INFORMATION ENTANGLEMENT
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Photocatalyst/metal-free sequential C-N/C-S bond formation:Synthesis of S-arylisothioureas via photoinduced EDA complex activation
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作者 Guoju Guo Xufeng Li +3 位作者 Jie Ma Yongjia Shi Jian Lv Daoshan Yang 《Chinese Chemical Letters》 SCIE CAS CSCD 2024年第11期361-366,共6页
A photocatalyst-free visible-light-promoted three-component reaction of thianthrenium salts,isothiocyanates,and amines is presented,which affords a rapid and efficient approach to S-arylisothioureas under mild conditi... A photocatalyst-free visible-light-promoted three-component reaction of thianthrenium salts,isothiocyanates,and amines is presented,which affords a rapid and efficient approach to S-arylisothioureas under mild conditions.This developed method exhibits the advantages of readily available raw materials,broad substrate scope,good functional tolerance,and operational simplicity.It is worth mentioning that the byproduct thianthrene can be recycled in quantity,ultimately maximizing the atomic economy of the reaction and avoiding chemical waste.Mechanism investigations support the strategy involving a photoinduced EDA complex. 展开更多
关键词 Visible-light Photocatalyst-free EDA complex Thianthrenium salts S-arylisothioureas
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Three-dimensional magnetic reconnection in complex multiple X-point configurations in an ancient solar-lunar terrestrial system
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作者 何向磊 毛傲华 +2 位作者 孙萌萌 邹继同 王晓钢 《Chinese Physics B》 SCIE EI CAS CSCD 2024年第3期488-495,共8页
Magnetic reconnection processes in three-dimensional(3D)complex field configurations have been investigated in different magneto-plasma systems in space,laboratory,and astrophysical systems.Two-dimensional(2D)features... Magnetic reconnection processes in three-dimensional(3D)complex field configurations have been investigated in different magneto-plasma systems in space,laboratory,and astrophysical systems.Two-dimensional(2D)features of magnetic reconnection have been well developed and applied successfully to systems with symmetrical property,such as toroidal fusion plasmas and laboratory experiments with an axial symmetry.But in asymmetric systems,the 3D features are inevitably different from those in the 2D case.Magnetic reconnection structures in multiple celestial body systems,particularly star-planet-Moon systems,bring fresh insights to the understanding of the 3D geometry of reconnection.Thus,we take magnetic reconnection in an ancient solar-lunar terrestrial magneto-plasma system as an example by using its crucial parameters approximately estimated already and also some specific applications in pathways for energy and matter transports among Earth,ancient Moon,and the interplanetary magnetic field(IMF).Then,magnetic reconnection of the ancient lunar-terrestrial magnetospheres with the IMF is investigated numerically in this work.In a 3D simulation for the Earth-Moon-IMF system,topological features of complex magnetic reconnection configurations and dynamical characteristics of magnetic reconnection processes are studied.It is found that a coupled lunar-terrestrial magnetosphere is formed,and under various IMF orientations,multiple X-points emerge at distinct locations,showing three typical magnetic reconnection structures in such a geometry,i.e.,the X-line,the triple current sheets,and the A-B null pairs.The results can conduce to further understanding of reconnection physics in 3D for plasmas in complex magnetic configurations,and also a possible mechanism for energy and matters transport in evolutions of similar astrophysical systems. 展开更多
关键词 magnetic reconnection multiple X-points complex magneto-plasma system
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Synthesis and Physico-Chemical Characterizations of Novel Hydrazone Ligands and Their Metal Complexes against Hormone-Dependent and Independent Cancers
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作者 Sommai Patitungkho Kingkaew Patitungkho 《Open Journal of Medicinal Chemistry》 2024年第1期1-12,共12页
This work deals with the synthesis and physicochemical characterizations of a new group of novel retinoidal ligands and their metal complexes. Their in vitro anti-proliferative activities have shown that ligand L1 is ... This work deals with the synthesis and physicochemical characterizations of a new group of novel retinoidal ligands and their metal complexes. Their in vitro anti-proliferative activities have shown that ligand L1 is effective against human breast cancer BT-20 and MCF-7 cell lines. At the same time, compound L2 exerts its effect on human prostate cancer PC-3 and human breast cancer MDA-MB-231 and MCF-7 cell lines respectively. The retinoid ligands exert their pleiotropic action toward retinoic acid receptors (RARs) than their metal complexes but all compounds exhibit concentration-dependent. 展开更多
关键词 Metal complexes CANCERS ANTIOXIDANT Hydrazone Retinoid Receptors
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Magma Mixing Genesis of the Mafic Enclaves and Related Granitoids in the Kan Granite-Gneiss Complex of Central Côte d’Ivoire: Evidence from Geology, Petrology and Geochemistry
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作者 Koffi Raoul Teha Koffi Kossonou Jean-Marie Pria +3 位作者 Koffi Joseph Brou Alain Nicaise Kouamelan Marc Ephrem Allialy Souad M’Rabet 《Open Journal of Geology》 CAS 2024年第8期760-786,共27页
The mafic enclaves from Paleoproterozoic domain are considered to be the results of large-scale crust-mantle interaction and magma mixing. In this paper, petrography, mineralogy and geochemistry were jointly used to d... The mafic enclaves from Paleoproterozoic domain are considered to be the results of large-scale crust-mantle interaction and magma mixing. In this paper, petrography, mineralogy and geochemistry were jointly used to determine the origin of the mafic enclaves and their relationship with the host granitoids of the Kan granite-gneiss complex. This study also provides new information on crust-mantle interactions. The mafic enclaves of the Kan vary in shape and size and have intermediate chemical compositions. The diagrams used show a number of similarities in the major elements (and often in the trace elements) between the mafic enclaves and the host granitoids. Geochemical show that the Kan rock are metaluminous, enriched in silica, medium to high-K calc-alkaline I-type granite. The similarities reflect a mixing of basic and acid magma. Mafic enclaves have a typical magmatic structure, which is characterized by magma mixing. The genesis of these rocks is associated with the context of subduction. They result from the mixing of a mafic magma originating from the mantle and linked to subduction, and a granitic magma (type I granite) that arises from the partial melting of the crust. 展开更多
关键词 Magma Mixing Mafic Microgranular Enclaves Host Granitoids Kan Granite-Gneiss complex West Africa
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Ecological network analysis reveals complex responses of tree species life stage interactions to stand variables
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作者 Hengchao Zou Huayong Zhang Tousheng Huang 《Journal of Forestry Research》 SCIE EI CAS CSCD 2024年第1期29-43,共15页
Tree interactions are essential for the structure,dynamics,and function of forest ecosystems,but variations in the architecture of life-stage interaction networks(LSINs)across forests is unclear.Here,we constructed 16... Tree interactions are essential for the structure,dynamics,and function of forest ecosystems,but variations in the architecture of life-stage interaction networks(LSINs)across forests is unclear.Here,we constructed 16 LSINs in the mountainous forests of northwest Hebei,China based on crown overlap from four mixed forests with two dominant tree species.Our results show that LSINs decrease the complexity of stand densities and basal areas due to the interaction cluster differentiation.In addition,we found that mature trees and saplings play different roles,the first acting as“hub”life stages with high connectivity and the second,as“bridges”controlling information flow with high centrality.Across the forests,life stages with higher importance showed better parameter stability within LSINs.These results reveal that the structure of tree interactions among life stages is highly related to stand variables.Our efforts contribute to the understanding of LSIN complexity and provide a basis for further research on tree interactions in complex forest communities. 展开更多
关键词 Tree interactions Life stages Interaction networks Ecological complexity
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Channel-Feedback-Free Transmission for Downlink FD-RAN:A Radio Map Based Complex-Valued Precoding Network Approach
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作者 Zhao Jiwei Chen Jiacheng +3 位作者 Sun Zeyu Shi Yuhang Zhou Haibo Xuemin(Sherman)Shen 《China Communications》 SCIE CSCD 2024年第4期10-22,共13页
As the demand for high-quality services proliferates,an innovative network architecture,the fully-decoupled RAN(FD-RAN),has emerged for more flexible spectrum resource utilization and lower network costs.However,with ... As the demand for high-quality services proliferates,an innovative network architecture,the fully-decoupled RAN(FD-RAN),has emerged for more flexible spectrum resource utilization and lower network costs.However,with the decoupling of uplink base stations and downlink base stations in FDRAN,the traditional transmission mechanism,which relies on real-time channel feedback,is not suitable as the receiver is not able to feedback accurate and timely channel state information to the transmitter.This paper proposes a novel transmission scheme without relying on physical layer channel feedback.Specifically,we design a radio map based complex-valued precoding network(RMCPNet)model,which outputs the base station precoding based on user location.RMCPNet comprises multiple subnets,with each subnet responsible for extracting unique modal features from diverse input modalities.Furthermore,the multimodal embeddings derived from these distinct subnets are integrated within the information fusion layer,culminating in a unified representation.We also develop a specific RMCPNet training algorithm that employs the negative spectral efficiency as the loss function.We evaluate the performance of the proposed scheme on the public DeepMIMO dataset and show that RMCPNet can achieve 16%and 76%performance improvements over the conventional real-valued neural network and statistical codebook approach,respectively. 展开更多
关键词 beamforming complex neural networks deep learning FD-RAN
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ATP-induced supramolecular assembly based on chromophoric organic molecules and metal complexes
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作者 Zhu Shu Xin Lei +4 位作者 Yeye Ai Ke Shao Jianliang Shen Zhegang Huang Yongguang Li 《Chinese Chemical Letters》 SCIE CAS CSCD 2024年第11期87-98,共12页
Adenosine triphosphate(ATP),known as a common metabolic product in organism,is not only importance to provide energy in various cellular activities but also is widely explored in the bio-inspired synthetic supramolecu... Adenosine triphosphate(ATP),known as a common metabolic product in organism,is not only importance to provide energy in various cellular activities but also is widely explored in the bio-inspired synthetic supramolecular area which becomes a fascinating topic with the rapid development of biology,chemistry and materials science.In this review,the recent advances about ATP interacted with functional small organic compounds and metal coordinated complexes are summarized.The design principles,its function as an active supramolecular matrix,the associated non-covalent binding modes and assembly induced properties including the optical properties,morphologies are presented in details.Besides,their applications for metal ion detecting,enzyme activity monitoring and drug delivery are described due to their excellently dynamic assembly properties,adjustability,and response to stimuli.Finally,an overview of the existing challenges and future prospects of ATP-induced supramolecular systems are also discussed. 展开更多
关键词 Adenosine triphosphate Metal complexes LUMINESCENCE ASSEMBLY Monitoring application
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Interference in Complex CDMA-OFDM/OQAM for Better Performance at Low SNR
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作者 Chrislin Martial Lélé 《International Journal of Communications, Network and System Sciences》 2024年第8期113-128,共16页
This article is about orthogonal frequency-division multiplexing with quadrature amplitude modulation combined with code division multiplexing access for complex data transmission. It aims to present a method which us... This article is about orthogonal frequency-division multiplexing with quadrature amplitude modulation combined with code division multiplexing access for complex data transmission. It aims to present a method which uses two interfering subsets in order to improve the performance of the transmission scheme. The idea is to spread in a coherent manner some data amongst two different codes belonging to the two different subsets involved in complex orthogonal frequency-division multiplexing with quadrature amplitude modulation and code division multiplexing access. This will improve the useful signal level at the receiving side and therefore improve the decoding process especially at low signal to noise ratio. However, this procedure implies some interference with other codes therefore creating a certain noise which is noticeable at high signal to noise ratio. 展开更多
关键词 CDMA OFDM/OQAM complex Data
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Squeeze and Excitation Convolution with Shortcut for Complex Plasma Image Recognition
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作者 Baoxia Li Wenzhuo Chen +5 位作者 Xiaojiang Tang Shaohuang Bian Yang Liu Junwei Guo Dan Zhang Feng Huang 《Computers, Materials & Continua》 SCIE EI 2024年第8期2221-2236,共16页
Complex plasma widely exists in thin film deposition,material surface modification,and waste gas treatment in industrial plasma processes.During complex plasma discharge,the configuration,distribution,and size of part... Complex plasma widely exists in thin film deposition,material surface modification,and waste gas treatment in industrial plasma processes.During complex plasma discharge,the configuration,distribution,and size of particles,as well as the discharge glow,strongly depend on discharge parameters.However,traditional manual diagnosis methods for recognizing discharge parameters from discharge images are complicated to operate with low accuracy,time-consuming and high requirement of instruments.To solve these problems,by combining the two mechanisms of attention mechanism(strengthening the extraction of the channel feature)and shortcut connection(enabling the input information to be directly transmitted to deep networks and avoiding the disappearance or explosion of gradients),the network of squeeze and excitation convolution with shortcut(SECS)for complex plasma image recognition is proposed to effectively improve the model performance.The results show that the accuracy,precision,recall and F1-Score of our model are superior to other models in complex plasma image recognition,and the recognition accuracy reaches 97.38%.Moreover,the recognition accuracy for the Flowers and Chest X-ray publicly available data sets reaches 97.85%and 98.65%,respectively,and our model has robustness.This study shows that the proposed model provides a new method for the diagnosis of complex plasma images and also provides technical support for the application of plasma in industrial production. 展开更多
关键词 Image recognition complex plasmas deep learning
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Multi-soliton solutions, breather-like and bound-state solitons for complex modified Korteweg–de Vries equation in optical fibers
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作者 兰中周 《Chinese Physics B》 SCIE EI CAS CSCD 2024年第6期119-123,共5页
Under investigation in this paper is a complex modified Korteweg–de Vries(KdV) equation, which describes the propagation of short pulses in optical fibers. Bilinear forms and multi-soliton solutions are obtained thro... Under investigation in this paper is a complex modified Korteweg–de Vries(KdV) equation, which describes the propagation of short pulses in optical fibers. Bilinear forms and multi-soliton solutions are obtained through the Hirota method and symbolic computation. Breather-like and bound-state solitons are constructed in which the signs of the imaginary parts of the complex wave numbers and the initial separations of the two parallel solitons are important factors for the interaction patterns. The periodic structures and position-induced phase shift of some solutions are introduced. 展开更多
关键词 complex modified KdV equation multi-soliton solutions breather-like BOUND-STATE
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Structures and magnetism of dinuclear Co complexes based on imine derivatives
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作者 SUN Yadan LI Xinfeng +2 位作者 LIU Qiang Hiroki Oshio MENG Yinshan 《无机化学学报》 SCIE CAS CSCD 北大核心 2024年第11期2212-2220,共9页
This study presents the synthesis of three dinuclear cobalt complexes based on three imine derivatives:bis-[4-(2-pyridylmethyleneamino)-phenyl]thioether(L1),bis-[4-(2-pyridylmethyleneamino)-phenyl]ether(L2),and bis-[4... This study presents the synthesis of three dinuclear cobalt complexes based on three imine derivatives:bis-[4-(2-pyridylmethyleneamino)-phenyl]thioether(L1),bis-[4-(2-pyridylmethyleneamino)-phenyl]ether(L2),and bis-[4-(2-pyridylmethyleneamino)-phenyl]methane(L3).Single-crystal X-ray diffraction analysis reveals that the complexes[Co_(2)(L1)3](ClO_(4))4·2CH_(3)CN(1),[Co_(2)(L2)3](ClO_(4))4·2CH_(3)OH(2),and[Co_(2)(L3)3](ClO_(4))4·2CH_(3)OH(3)all exhibit a dinuclear structure.Magnetic test results show that complex 3 exhibited irreversible SCO behavior induced by loss of solvent at 300 K,with the average Co-N bond length increasing from 0.2139(3)to 0.2153(3)nm.Meanwhile,the desolvated complex 3 exhibited paramagnetic behavior similar to that of complexes 1 and 2.Variable-temperature UV-Vis spectroscopic studies also indicate that complex 3 undergoes a solvent-loss-induced spin-state transition.CCDC:2347354,1(120 K);2347355,2(120 K);2347356,3(120 K);2347357,3(400 K). 展开更多
关键词 spin crossover dinuclear cobalt complex imine derivatives
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Impurity modes in two-dimensional strongly coupled complex plasma crystals
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作者 吴诗杰 徐韵乔 +2 位作者 冼顺宇 何向磊 杨肖易 《Plasma Science and Technology》 SCIE EI CAS CSCD 2024年第8期1-7,共7页
Complex plasma fluctuation processes have been extensively studied in many aspects,especially lattice waves in strongly coupled plasma crystals,which are of great significance for understanding fundamental physical ph... Complex plasma fluctuation processes have been extensively studied in many aspects,especially lattice waves in strongly coupled plasma crystals,which are of great significance for understanding fundamental physical phenomena.A challenge of experimental investigations in two-dimensional strongly coupled complex plasma crystals is to keep the main body and foreign particles of different masses on the same horizontal plane.To solve the problem,we have proposed a potential well formed by two negatively biased grids to bind the negatively charged particles in a two-dimensional(2D)plane,thus achieving a 2D plasma crystal in the microgravity environment.The study of such phenomena in complex plasma crystals under microgravity environment then becomes possible.In this paper,we focus on the continuum spectrum,including both phonon and optic branches of the impurity mode in a 2D system in microgravity environments.The results show the dispersion relation of the longitudinal and transverse impurity oscillation modes and their properties.Considering the macroscopic visibility of complex mesoscopic particle lattices,theoretical and experimental studies on this kind of complex plasma systems will help us further understand the physical nature of a wide range of condensed matters. 展开更多
关键词 microgravity environment complex plasma lattice dispersion relation
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Structural Analysis for Qazzaz Metamorphic Core Complex,Northwestern Arabian Shield,Saudi Arabia
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作者 Mansour H.AL-HASHIM Osama M.K.KASSEM 《Acta Geologica Sinica(English Edition)》 SCIE CAS CSCD 2024年第5期1187-1201,共15页
Identifying deformational mechanisms and associated structures at various scales,ranging from regional-scale structures to microscopic fabric,is crucial for the assessment of tectonic development.Thirty-three samples ... Identifying deformational mechanisms and associated structures at various scales,ranging from regional-scale structures to microscopic fabric,is crucial for the assessment of tectonic development.Thirty-three samples were taken from the Qazzaz metamorphic core complex to estimate the finite strain for felsic and mafic minerals.These samples included gneisses rocks,monzogranite,and metavolcano-sedimentary rocks for both the Thalbah and Bayda groups.Using the Rf/j and Fry methods,the axial ratios(XZ)range about 2.20 to 7.10 and 1.90 to 9.10,respectively.For various rock units,the strain measurements show moderate to highly deformation.Most of the observed samples show shallow WNW dipping along a N to WNW trend of finite strain(X).The short axes(Z)based to be subvertical foliation related with a subhorizontal foliation.The results demonstrate that contacts generated at semi-brittle to ductile deformation and that the strain of magnitude has the same value for different lithologic units.It concluded that nappe generation in orogens results from pure shear deformation. 展开更多
关键词 Finite strain metamorphic core complex Qazzaz area Saudi Arabia
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3,6-Bis-β-Dicarbonylsubstituted Carbazoles Bearing N-Spacers and Their Eu(III) Complexes as Immunofluorescent Labelling Agents
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作者 Dmitry E. Pugachev Georgy V. Zatonsky +2 位作者 Tatyana S. Kostryukova Anna G. Shubina Nikolay V. Vasiliev 《International Journal of Organic Chemistry》 2024年第1期20-31,共12页
New reagents for immunofluorescence analysis of carbazole series containing fluorinated β-dicarbonyl fragments and carboxylic substituent groups separated by spacers of different lengths from the light-gathering carb... New reagents for immunofluorescence analysis of carbazole series containing fluorinated β-dicarbonyl fragments and carboxylic substituent groups separated by spacers of different lengths from the light-gathering carbazole scaffold have been developed. The markers in complex with Eu<sup>3+</sup> ions possess stability in the aqueous phase, intense and prolonged luminescence (τ 550 - 570 μs) with characteristic emission maxima in the region of 615 nm and excitation wavelengths in the region of 380 - 390 nm, which distinguishes them from most of the analogs used. In the study of marker conjugation with streptavidin, a reagent containing 4 - 5 europium labeling complexes based on spacer-containing carbazole tetraketone was obtained. The marker-doped silicate nanoparticles exhibit intense and long-lived luminescence in the characteristic region. 展开更多
关键词 Fluorescence Immunoassay Fluorinated β-Diketones CARBAZOLE Europium complexes STREPTAVIDIN Nanodispersions
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