The compression behavior of the heavy RE-based BMC Gd40Y16Al24Co20 under high pressure has been investigated by in situ high pressure angle dispersive X-ray diffraction measurements using synchrotron radiation in the ...The compression behavior of the heavy RE-based BMC Gd40Y16Al24Co20 under high pressure has been investigated by in situ high pressure angle dispersive X-ray diffraction measurements using synchrotron radiation in the pressure range of 0-33.42 GPa at room temperature. By fitting the static equation of state at room temperature, we find the value of bulk modulus B is 61.27±4 GPa which is in good agreement with the experimental study by pulse-echo techniques of 58 GPa. The results show that the amorphous structure in the heavy RE-based BMG Gd40Y16Al24Co20 keeps quite stable up to 33.42 GPa although its compressibility is as large as about 33%. The coexistence of normal local structure similar to that of other BMGs and covalent bond structure similar to those of oxide glasses may be the reason for the anomalous property under high pressure of the Gd4oY16Al24Co2o BMG.展开更多
A feasible and convenient method is proposed to suppress higher-harmonics for a varied-line-spacing plane grating monochromator in the soft X-ray region. Related calculations and experiments demonstrate that decreasin...A feasible and convenient method is proposed to suppress higher-harmonics for a varied-line-spacing plane grating monochromator in the soft X-ray region. Related calculations and experiments demonstrate that decreasing the included angle slightly by changing the parameter of the exit arm length can significantly improve light purity. This method is suitable and has been used for experiments of detector calibration in beamline 4B7B at the Beijing Synchrotron Radiation Facility (BSRF).展开更多
基金Supported by Chinese Academy of Sciences (KJCX2-SW-N20, KJCX2-SW-N03)NSFC (50731005)+1 种基金SKPBRC(2007CB616915/2006CB605201)PCSIRT (IRT0650)
文摘The compression behavior of the heavy RE-based BMC Gd40Y16Al24Co20 under high pressure has been investigated by in situ high pressure angle dispersive X-ray diffraction measurements using synchrotron radiation in the pressure range of 0-33.42 GPa at room temperature. By fitting the static equation of state at room temperature, we find the value of bulk modulus B is 61.27±4 GPa which is in good agreement with the experimental study by pulse-echo techniques of 58 GPa. The results show that the amorphous structure in the heavy RE-based BMG Gd40Y16Al24Co20 keeps quite stable up to 33.42 GPa although its compressibility is as large as about 33%. The coexistence of normal local structure similar to that of other BMGs and covalent bond structure similar to those of oxide glasses may be the reason for the anomalous property under high pressure of the Gd4oY16Al24Co2o BMG.
基金Supported by National Natural Science Foundation of China(11375227,61204008)
文摘A feasible and convenient method is proposed to suppress higher-harmonics for a varied-line-spacing plane grating monochromator in the soft X-ray region. Related calculations and experiments demonstrate that decreasing the included angle slightly by changing the parameter of the exit arm length can significantly improve light purity. This method is suitable and has been used for experiments of detector calibration in beamline 4B7B at the Beijing Synchrotron Radiation Facility (BSRF).