This paper proposes a methodology to construct logs of rock strength from the cutting force signal recorded in scratch tests conducted in the ductile regime.The approach,which is based on the application of discrete w...This paper proposes a methodology to construct logs of rock strength from the cutting force signal recorded in scratch tests conducted in the ductile regime.The approach,which is based on the application of discrete wavelet transforms,recognizes the existence of two length scales[c and[r.The strength length scale[c represents the length over which it is meaningful to measure strength,while the repeatability length scale[r is related to the resolution at which the force signal must be observed to become insensitive to the stochastic micro-failure events triggered by the motion of the cutter.It is postulated that the original cutting force signal,assumed to be sampled at a high enough frequency,can be decomposed into a deterministic signal intrinsic to the rock and a stochastic one resulting from discrete rock failure events.The technique of multiresolution analysis based on the maximal overlap discrete wavelet transform is applied as a low-pass filter to the original cutting force signals so as to wipe out the high-frequency components associated with the stochastic rock failure events.A criterion to determine the optimum cutoff frequency of the low-pass filter and the corresponding repeatability length scale is discussed in terms of the correlation coefficients between different filtered signals.It is shown that the low-pass filtered signals obtained at the optimum cutoff frequency have two salient features:(i)repeatability over different tests conducted at the same depth of cut on the same sample,and(ii)variability along the cutting distance.The excellent repeatability reveals that the deterministic background trend of the original force signals is relevant to the rock strength property,and the variability of the background trend captures the spatial variation of the rock strength.展开更多
Micro-scale abrasion testing is widely used to determine the abrasion resistance of thin film coatings; it is a simple technique that can easily be used as part of a quality control procedure, but it has got the disad...Micro-scale abrasion testing is widely used to determine the abrasion resistance of thin film coatings; it is a simple technique that can easily be used as part of a quality control procedure, but it has got the disadvantage of not allowing an easy study of the wear mechanisms involved: it is difficult to estimate the load applied on each abrasive particles in the contact between the loaded ball and the specimen. The possibility of using progressive loading scratch testing, a method widely used to assess the adhesion of thin film coatings, to model the abrasive wear of coatings has been studied in the past; the use of multiple scratch tests to study the wear mechanisms corresponding to a single abrasion scratch event has also been studied in the case of bulk materials (ceramics and hard metals). Two coatings, deposited by Closed Field Unbalanced Magnetron Sputter Ion Plating (CFUBMSIP) on ASP23 powder metallurgy steel substrate are chosen to be representative of the use of protective coatings in industry: titanium nitride, which is widely used to prevent tool wear, and TCL Graphit-iC?, which is widely used as a wear resistant solid lubricant coating. The two coatings are first characterised by using a standard quality control procedure: their thickness is determined by the cap grinding method, their adhesion by progressive loading scratch. Then micro-scale abrasion tests performed with a slurry at a concentration which promotes grooving wear, and medium load multiple scratch tests performed with diamond indenters are completed; the results of these tests are analysed and compared to determine if there is any correlation between the two sets of results; the multiple scratch tests wear tracks are also observed to determine the wear mechanisms involved.展开更多
In this paper based on the experiment principle of evaluating adhesion property by scratch testing, the peeling mechanism of thin films is discussed by applying contact theory and surface physics theory. A mathematica...In this paper based on the experiment principle of evaluating adhesion property by scratch testing, the peeling mechanism of thin films is discussed by applying contact theory and surface physics theory. A mathematical model predicting the critical load is proposed for calculating critical load as determined byscratch testing. The factors for correctly evaluating adhesion of coatings according to the experimental data arediscussed.展开更多
Shale reservoirs have been a significant focus of hydrocarbon production over the past few decades,and the mechanical assessment of target shale reservoirs has been critical to successful field operations,especially i...Shale reservoirs have been a significant focus of hydrocarbon production over the past few decades,and the mechanical assessment of target shale reservoirs has been critical to successful field operations,especially in hydraulic fracturing and well completions.The Unconfined compressive strength(UCS)and Poisson's ratio(ν)are critical mechanical properties in shale reservoir assessment.The estimation and measurement of shale mechanical properties are often erroneous by not accounting for their heterogeneous and pre-existing features,which yield variability of shale mechanical properties along their lithostratigraphy.Thus,there is a need to investigate the degree of correlation and accuracy in multiscale mechanical evaluations of heterogeneous shales,and the correlation between such micromechanical and macromechanical measurements.This study investigated the impact of inherent heterogeneity on the measurement of continuous micromechanical and macromechanical properties of shale reservoirs using scratch test(ST)and uniaxial compression test(UCT)methods,and the degree of correlation(correlation coefficient,r)of measurements in shale was further assessed for the variability of their measured properties.Shale core samples from three distinct shale formations were utilized and studied,and the core samples were subjected to ST and UCT,respectively.The results from this study showed that despite inherent heterogeneous anomalies and natural fractures in the shale samples analyzed,there is a good degree of correlation(UCS:r=0.73;ν:r=0.89)in the micro-and macro-mechanical properties of shales using two independent experimental tests(ST and UCT).This study provides insights for improving the accuracy of mechanical evaluations and numerical modeling in shales with a high degree of heterogeneity and pre-existing natural fractures.The results indicate that when considering the structural complexity and heterogeneity of unconventional reservoirs such as shales,the ST method can provide a better continuous micromechanical assessment of shales.In contrast,the UCT can provide a better bulk macromechanical measurement of shales.展开更多
Fracture toughness is an important index in safety evaluation for materials and structures.Its convenient and accurate characterization has attracted extensive attention.For small specimens,traditional testing methods...Fracture toughness is an important index in safety evaluation for materials and structures.Its convenient and accurate characterization has attracted extensive attention.For small specimens,traditional testing methods of fracture toughness are not suitable due to limitations in sample size and shape.In this work,a new formula is proposed to determine the fracture toughness of glasses using scratch tests with a Vickers indenter based on dimensional analysis and finite element analysis.Fracture toughness of glasses could be calculated with elastic modulus,crack depth of scratched materials and normal force applied during the scratch tests.The effects of plastic deformation and interfacial friction between the Vickers indenter and scratched materials are considered,and the crack shape is consistent with experimental observations.The proposed formula is verified by comparing the fracture toughness of soda-lime and borosilicate glasses obtained from scratch tests with those obtained via indentation tests.This work provides an alternative method to determine the fracture toughness of glass materials.展开更多
The interface adhesion strength(or interface toughness)of a thin film/substrate system is often assessed by the micro-scratch test.For a brittle film material,the interface adhesion strength is easily obtained through...The interface adhesion strength(or interface toughness)of a thin film/substrate system is often assessed by the micro-scratch test.For a brittle film material,the interface adhesion strength is easily obtained through measuring the scratch driving forces.However,to measure the interface adhesion strength(or in- terface toughness)for a metal thin film material(the ductile material)by the micro- scratch test is very difficult,because intense plastic deformation is involved and the problem is a three-dimensional elastic-plastic one.In the present research,using a double-cohesive zone model,the failure characteristics of the thin film/substrate system can be described and further simulated.For a steady-state scratching pro- cess,a three-dimensional elastic-plastic finite element method based on the double cohesive zone model is developed and adopted,and the steady-state fracture work of the total system is calculated.The parameter relations between the horizontal driving forces(or energy release rate of the scratching process)and the separation strength of thin film/substrate interface,and the material shear strength,as well as the material parameters are developed.Furthermore,a scratch experiment for the Al/Si film/substrate system is carried out and the failure mechanisms are explored. Finally,the prediction results are applied to a scratch experiment for the Pt/NiO material system given in the literature.展开更多
The nanoscratch behaviors of La0.7Sr0.3MnO3＋δ films, which were deposited with ratio of O2/（O2＋Ar）, ranging from 4.4% to 45.6% by DC magnetron sputter, were investigated by a nanoindentation technique. The result...The nanoscratch behaviors of La0.7Sr0.3MnO3＋δ films, which were deposited with ratio of O2/（O2＋Ar）, ranging from 4.4% to 45.6% by DC magnetron sputter, were investigated by a nanoindentation technique. The results indicated that the friction coefficient between the films and the diamond tip depended on the loading critical load. The friction coefficient was about 0.08-0.12 when the loading normal load was less than the loading critical load. The films displayed excellent elastic recovery after unloading. When the loading load was larger than the loading critical load, plastic deformation and ploughing appeared for the films. The friction coefficient was about 0.43 when the film was damaged completely. The suitable decrease in ratio of O2/（O2＋Ar） could improve the nanoscratch resistance of the films. The film deposited with O2/（O2＋Ar）=25% possessed better scratch resistance due to good elastic recovery, high nanohardness, and critical load. The loading critical load of the film was larger than 80 raN.展开更多
Objective: To introduce the concept that there might be “nothing to smell” to the Brief Smell Identification Test (B-SIT), with a view to masking olfactory deficits, particularly from healthy control participants in...Objective: To introduce the concept that there might be “nothing to smell” to the Brief Smell Identification Test (B-SIT), with a view to masking olfactory deficits, particularly from healthy control participants in research studies. Methods: Seventy-one elderly individuals, healthy for their age, were recruited to the study. They were blindfolded and carried out a modified B-SIT where one item had been replaced with a placebo, and one odour alternative answer to three other items was replaced by the alternative “none/other” (actual odour unchanged). Results: There was no overall difference in the median or mean score achieved by the cohort compared to results obtained previously using the conventional B-SIT. The replacement of the item “turpentine” with a placebo resulted in an improved score for the item in a Norwegian setting. The overall scores were not improved. Conclusions: It is possible to introduce the concept that there may be “nothing to smell” to the B-SIT without compromising the test for healthy control individuals. This may be a more appropriate approach to olfactory testing of control individuals or patients with suspected early neurodegenerative diseases.展开更多
基金provided by the National Science Foundation of USA(Grant No.1742823)。
文摘This paper proposes a methodology to construct logs of rock strength from the cutting force signal recorded in scratch tests conducted in the ductile regime.The approach,which is based on the application of discrete wavelet transforms,recognizes the existence of two length scales[c and[r.The strength length scale[c represents the length over which it is meaningful to measure strength,while the repeatability length scale[r is related to the resolution at which the force signal must be observed to become insensitive to the stochastic micro-failure events triggered by the motion of the cutter.It is postulated that the original cutting force signal,assumed to be sampled at a high enough frequency,can be decomposed into a deterministic signal intrinsic to the rock and a stochastic one resulting from discrete rock failure events.The technique of multiresolution analysis based on the maximal overlap discrete wavelet transform is applied as a low-pass filter to the original cutting force signals so as to wipe out the high-frequency components associated with the stochastic rock failure events.A criterion to determine the optimum cutoff frequency of the low-pass filter and the corresponding repeatability length scale is discussed in terms of the correlation coefficients between different filtered signals.It is shown that the low-pass filtered signals obtained at the optimum cutoff frequency have two salient features:(i)repeatability over different tests conducted at the same depth of cut on the same sample,and(ii)variability along the cutting distance.The excellent repeatability reveals that the deterministic background trend of the original force signals is relevant to the rock strength property,and the variability of the background trend captures the spatial variation of the rock strength.
文摘Micro-scale abrasion testing is widely used to determine the abrasion resistance of thin film coatings; it is a simple technique that can easily be used as part of a quality control procedure, but it has got the disadvantage of not allowing an easy study of the wear mechanisms involved: it is difficult to estimate the load applied on each abrasive particles in the contact between the loaded ball and the specimen. The possibility of using progressive loading scratch testing, a method widely used to assess the adhesion of thin film coatings, to model the abrasive wear of coatings has been studied in the past; the use of multiple scratch tests to study the wear mechanisms corresponding to a single abrasion scratch event has also been studied in the case of bulk materials (ceramics and hard metals). Two coatings, deposited by Closed Field Unbalanced Magnetron Sputter Ion Plating (CFUBMSIP) on ASP23 powder metallurgy steel substrate are chosen to be representative of the use of protective coatings in industry: titanium nitride, which is widely used to prevent tool wear, and TCL Graphit-iC?, which is widely used as a wear resistant solid lubricant coating. The two coatings are first characterised by using a standard quality control procedure: their thickness is determined by the cap grinding method, their adhesion by progressive loading scratch. Then micro-scale abrasion tests performed with a slurry at a concentration which promotes grooving wear, and medium load multiple scratch tests performed with diamond indenters are completed; the results of these tests are analysed and compared to determine if there is any correlation between the two sets of results; the multiple scratch tests wear tracks are also observed to determine the wear mechanisms involved.
文摘In this paper based on the experiment principle of evaluating adhesion property by scratch testing, the peeling mechanism of thin films is discussed by applying contact theory and surface physics theory. A mathematical model predicting the critical load is proposed for calculating critical load as determined byscratch testing. The factors for correctly evaluating adhesion of coatings according to the experimental data arediscussed.
文摘Shale reservoirs have been a significant focus of hydrocarbon production over the past few decades,and the mechanical assessment of target shale reservoirs has been critical to successful field operations,especially in hydraulic fracturing and well completions.The Unconfined compressive strength(UCS)and Poisson's ratio(ν)are critical mechanical properties in shale reservoir assessment.The estimation and measurement of shale mechanical properties are often erroneous by not accounting for their heterogeneous and pre-existing features,which yield variability of shale mechanical properties along their lithostratigraphy.Thus,there is a need to investigate the degree of correlation and accuracy in multiscale mechanical evaluations of heterogeneous shales,and the correlation between such micromechanical and macromechanical measurements.This study investigated the impact of inherent heterogeneity on the measurement of continuous micromechanical and macromechanical properties of shale reservoirs using scratch test(ST)and uniaxial compression test(UCT)methods,and the degree of correlation(correlation coefficient,r)of measurements in shale was further assessed for the variability of their measured properties.Shale core samples from three distinct shale formations were utilized and studied,and the core samples were subjected to ST and UCT,respectively.The results from this study showed that despite inherent heterogeneous anomalies and natural fractures in the shale samples analyzed,there is a good degree of correlation(UCS:r=0.73;ν:r=0.89)in the micro-and macro-mechanical properties of shales using two independent experimental tests(ST and UCT).This study provides insights for improving the accuracy of mechanical evaluations and numerical modeling in shales with a high degree of heterogeneity and pre-existing natural fractures.The results indicate that when considering the structural complexity and heterogeneity of unconventional reservoirs such as shales,the ST method can provide a better continuous micromechanical assessment of shales.In contrast,the UCT can provide a better bulk macromechanical measurement of shales.
基金the financial support from National Natural Science Foundation of China(Nos.12072324 and U1804254)Natural Science Foundation of Henan Province for Excellent Young Scholars(212300410087).
文摘Fracture toughness is an important index in safety evaluation for materials and structures.Its convenient and accurate characterization has attracted extensive attention.For small specimens,traditional testing methods of fracture toughness are not suitable due to limitations in sample size and shape.In this work,a new formula is proposed to determine the fracture toughness of glasses using scratch tests with a Vickers indenter based on dimensional analysis and finite element analysis.Fracture toughness of glasses could be calculated with elastic modulus,crack depth of scratched materials and normal force applied during the scratch tests.The effects of plastic deformation and interfacial friction between the Vickers indenter and scratched materials are considered,and the crack shape is consistent with experimental observations.The proposed formula is verified by comparing the fracture toughness of soda-lime and borosilicate glasses obtained from scratch tests with those obtained via indentation tests.This work provides an alternative method to determine the fracture toughness of glass materials.
基金The project supported by the National Natural Science Foundation of China (19891180 and 19925211)Bai Ren Plan of CAS
文摘The interface adhesion strength(or interface toughness)of a thin film/substrate system is often assessed by the micro-scratch test.For a brittle film material,the interface adhesion strength is easily obtained through measuring the scratch driving forces.However,to measure the interface adhesion strength(or in- terface toughness)for a metal thin film material(the ductile material)by the micro- scratch test is very difficult,because intense plastic deformation is involved and the problem is a three-dimensional elastic-plastic one.In the present research,using a double-cohesive zone model,the failure characteristics of the thin film/substrate system can be described and further simulated.For a steady-state scratching pro- cess,a three-dimensional elastic-plastic finite element method based on the double cohesive zone model is developed and adopted,and the steady-state fracture work of the total system is calculated.The parameter relations between the horizontal driving forces(or energy release rate of the scratching process)and the separation strength of thin film/substrate interface,and the material shear strength,as well as the material parameters are developed.Furthermore,a scratch experiment for the Al/Si film/substrate system is carried out and the failure mechanisms are explored. Finally,the prediction results are applied to a scratch experiment for the Pt/NiO material system given in the literature.
基金supported by the Program for New Century Excellent Talents in University
文摘The nanoscratch behaviors of La0.7Sr0.3MnO3＋δ films, which were deposited with ratio of O2/（O2＋Ar）, ranging from 4.4% to 45.6% by DC magnetron sputter, were investigated by a nanoindentation technique. The results indicated that the friction coefficient between the films and the diamond tip depended on the loading critical load. The friction coefficient was about 0.08-0.12 when the loading normal load was less than the loading critical load. The films displayed excellent elastic recovery after unloading. When the loading load was larger than the loading critical load, plastic deformation and ploughing appeared for the films. The friction coefficient was about 0.43 when the film was damaged completely. The suitable decrease in ratio of O2/（O2＋Ar） could improve the nanoscratch resistance of the films. The film deposited with O2/（O2＋Ar）=25% possessed better scratch resistance due to good elastic recovery, high nanohardness, and critical load. The loading critical load of the film was larger than 80 raN.
文摘Objective: To introduce the concept that there might be “nothing to smell” to the Brief Smell Identification Test (B-SIT), with a view to masking olfactory deficits, particularly from healthy control participants in research studies. Methods: Seventy-one elderly individuals, healthy for their age, were recruited to the study. They were blindfolded and carried out a modified B-SIT where one item had been replaced with a placebo, and one odour alternative answer to three other items was replaced by the alternative “none/other” (actual odour unchanged). Results: There was no overall difference in the median or mean score achieved by the cohort compared to results obtained previously using the conventional B-SIT. The replacement of the item “turpentine” with a placebo resulted in an improved score for the item in a Norwegian setting. The overall scores were not improved. Conclusions: It is possible to introduce the concept that there may be “nothing to smell” to the B-SIT without compromising the test for healthy control individuals. This may be a more appropriate approach to olfactory testing of control individuals or patients with suspected early neurodegenerative diseases.
