Two severe plastic deformation(SPD)techniques of simple shear extrusion(SSE)and equal channel angular pressing(ECAP)were employed to process an extruded Mg-6Gd-3Y-1.5Ag(wt%)alloy at 553 K for 1,2,4 and 6 passes.The mi...Two severe plastic deformation(SPD)techniques of simple shear extrusion(SSE)and equal channel angular pressing(ECAP)were employed to process an extruded Mg-6Gd-3Y-1.5Ag(wt%)alloy at 553 K for 1,2,4 and 6 passes.The microstructural evolutions were studied by electron back scattered diffraction(EBSD)analysis and transmission electron microscopy(TEM).The initial grain size of 7.5μm in the extruded alloy was reduced to about 1.3μm after 6 SPD passes.Discontinuous dynamic recrystallization was suggested to be operative in both SSE and ECAP,with also a potential contribution of continuous dynamic recrystallization at the early stages of deformation.The difference in the shear strain paths of the two SPD techniques caused different progression rate of dynamic recrystallization(DRX),so that the alloys processed by ECAP exhibited higher fractions of recrystallization and high angle grain boundaries(HAGBs).It was revealed that crystallographic texture was also significantly influenced by the difference in the strain paths of the two SPD methods,where dissimilar basal plane texture components were obtained.The compression tests,performed along extrusion direction(ED),indicated that the compressive yield stress(CYS)and ultimate compressive strength(UCS)of the alloys after both SEE and ECAP augmented continuously by increasing the number of passes.ECAP-processed alloys had lower values of CYS and UCS compared to their counterparts processed by SSE.This difference in the mechanical responses was attributed to the different configurations of basal planes with respect to the loading direction(ED)of each SPD technique.展开更多
A new severe plastic deformation(SPD)technique for improvement of the metallurgical properties of the magnesium alloys is presented.In this process,a cyclic extrusion compression angular pressing(CECAP)process is foll...A new severe plastic deformation(SPD)technique for improvement of the metallurgical properties of the magnesium alloys is presented.In this process,a cyclic extrusion compression angular pressing(CECAP)process is followed by an extrusion step in the outlet playing the role of additional back pressure.Therefore,more uniform and enhanced mechanical properties are expected in comparison with equal channel angular pressing(ECAP).In order to evaluate the effectiveness and capabilities of this new method,an AM60 magnesium alloy was processed.Finite element results exhibited a significant increase in strain values as well as uniform strain distribution for the new method.In addition,~110%increase in compressive stress was observed in new method compared to the conventional ECAP.Experimental results revealed a noticeable increase in the hardness and strength of the specimens processed by the new technique as a result of the formation of finer grains and more homogeneous microstructure with good distribution of refinedβ-phase along the boundaries.It may be concluded that the new process is very promising for future magnesium alloy products.展开更多
A modem design method, in which traditional design formulas are conjoined with numerical simulation and optimization, is successfully used to design the out-size extrusion flame precisely so that the press cost can be...A modem design method, in which traditional design formulas are conjoined with numerical simulation and optimization, is successfully used to design the out-size extrusion flame precisely so that the press cost can be saved. A new technology used for decompressing by a multi-steps dynamical mode is put forward, which makes it possible to decompress the large flow-volume high-pressure oil in the main cylinders. In addition, a method for realizing the fixed mandrel process by hydraulic support is proposed and its control equation is established. Pre-tightening frame tests are carried out by over-operating pressure on 100 MN aluminium extrusion press with oil-driven double action, which is developed based on the above key techniques and is the largest press so far in the world, and the results show that the frame structure designed is reasonable and reliable, and the modem design method used is an useful tool for designing large and out-size heavy plastic forming machinery. The results of decompressing curve in main cylinder and noise inspection indicate that multi-steps dynamical mode for decompressing the large flow-volume high pressure oil is valid and reliable. Meanwhile, the fixed mandrel process is well realized based on the control equation. These key techniques have been used in the development of 125 MN aluminium extrusion press with oil-driven double action.展开更多
The microstructures and properties of ZK60 alloy were evaluated under four different conditions: extrusion; extrusion and 4 passes of equal channel angular pressing (ECAP); extrusion, 4 passes of ECAP and secondary...The microstructures and properties of ZK60 alloy were evaluated under four different conditions: extrusion; extrusion and 4 passes of equal channel angular pressing (ECAP); extrusion, 4 passes of ECAP and secondary extrusion; and extrusion, 4 passes of ECAP, annealing and secondary extrusion. Secondary extrusion at ambient temperature was successfully processed to produce ultrafine-grained ZK60 alloy. The results show that ECAP introduces significant grain refinement and there is additional refinement in secondary extrusion. High yield strength of 342 MPa is achieved after secondary extrusion at room temperature, but the elongation to failure is only 0.8%. However, by applying annealing before secondary extrusion, the ductility of ZK60 could be greatly improved to 4.5%, meanwhile the yield strength almost remains the same, and the ultimate strength of up to 388 MPa is obtained.展开更多
Rigid-viscoplastic3D finite element simulations(3D FEM)of the equal channel angular pressing(ECAP),thecombination of ECAP+extrusion with different extrusion ratios,and direct extrusion of pure aluminum were performed ...Rigid-viscoplastic3D finite element simulations(3D FEM)of the equal channel angular pressing(ECAP),thecombination of ECAP+extrusion with different extrusion ratios,and direct extrusion of pure aluminum were performed andanalyzed.The3D FEM simulations were carried out to investigate the load-displacement behavior,the plastic deformationcharacteristics and the effective plastic strain homogeneity of Al-1080deformed by different forming processes.The simulationresults were validated by microstructure observations,microhardness distribution maps and the correlation between the effectiveplastic strain and the microhardness values.The3D FEM simulations were performed successfully with a good agreement with theexperimental results.The load-displacement curves and the peak load values of the3D FEM simulations and the experimentalresults were close from each other.The microhardness distribution maps were in a good conformity with the effective plastic straincontours and verifying the3D FEM simulations results.The ECAP workpiece has a higher degree of deformation homogeneity thanthe other deformation processes.The microhardness values were calculated based on the average effective plastic strain.Thepredicted microhardness values fitted the experimental results well.The microstructure observations in the longitudinal andtransverse directions support the3D FEM effective plastic strain and microhardness distributions result in different formingprocesses.展开更多
The rods that were shaped from nanocrystalline WC- 10.21 Co-0.42 VC/ Cr3 C2 ( wt% ) composite powders by using powder extrusion molding (PEM) were investigated. The nanocrystalline WC- 10.21 Co- 0. 42 VC/ Cr3 C2 ...The rods that were shaped from nanocrystalline WC- 10.21 Co-0.42 VC/ Cr3 C2 ( wt% ) composite powders by using powder extrusion molding (PEM) were investigated. The nanocrystalline WC- 10.21 Co- 0. 42 VC/ Cr3 C2 ( wt% ) composite powders were prepared by the spray thermal decomposition-continuous reduction and carburization technology. In order to improve the properties of rods shaped by using powder extrusion molding, the cold isostatic pressing (CIP) technology was used before or after debinding. Specimens were siutered by vacuum siutering and hot isostatic pressing (HIP). The density, Rockwell A hardness, magnetic coercivity , and magnetic saturation induction of siutered specimen were measured. The microstructure of the green bodies and the siutered specimens was studied by scanning electron microscopy (SEM). Results show that the rod formed by using powder extrusion molding after debinding and followed by cold isostatic pressing can be siutered to 99.5% density of composite cemented carbide rods with an average grain size of about 200- 300 nm, magnetic coercivity of 30.4 KA / m, Rockwell A hardness of 92.6 and magnetic saturation induction of 85% . Superfine WC- 10 Co cemented carbide rods with excellent properties were obtained.展开更多
The micro orientation theological behavior of AZ61 Mg alloy during net-shape forming of tensile specimens via close-die pressing of extruded preformed and the effect of the press deformation rate on the microstructure...The micro orientation theological behavior of AZ61 Mg alloy during net-shape forming of tensile specimens via close-die pressing of extruded preformed and the effect of the press deformation rate on the microstructure characteristics were characterized with electron back-scattering diffraction(EBSD)orientation imaging microscopy and metallography.The results indicate that the intensity distribution of basal{0001}<1010>texture on the cross-section of the extruded perform is uniform and parallel to the extrusion direction.Subjected to pressing in extrusion direction,deformation shear stress leads to grain rotation and basal texture {0001}<1010>deviation from the extrusion direction,spreading in the direction perpendicular to pressing direction.The texture intensity increases with the press deformation rate and reaches its peak value at 50%,which is considerably lower than the value reached in extrusion deformation.Then,the texture intensity decreases with the press deformation rate reversely.展开更多
The deformation behavior of equal channel angular pressing(ECAP)was discussed by using plasticity method.The node mapping method is employed to realize the analysis of multi-pass ECAP by using three-dimensional FEM me...The deformation behavior of equal channel angular pressing(ECAP)was discussed by using plasticity method.The node mapping method is employed to realize the analysis of multi-pass ECAP by using three-dimensional FEM methods for pure aluminum.The single-pass ECAP is a non-uniform shear deformation process in the cross-section of the workpiece.The uniform deformation processing routes are obtained during multi-pass ECAP process.In addition,the density of dislocations and defects of crystal lattice are also largely changed for different processing routes.The grain microstructure is gradually refined with the increase of the pressing passes.The grains and their distribution obtained by route Bc are more useful for producing the material with high angle grain boundaries.The grain microstructure of the cross section of the pressed material decreases with the increase of strain,and some grains exhibit transformed grain boundary(PTB)fringes.The dislocation density in the grain decreases,and the grain boundary presents equiaxed distribution.展开更多
A combination of extrusion and equal channel angular pressing (ECAP) was used to deform a plain low carbon steel. This process consists of two successive deformations by extrusion and ECAP in a single die (Ex-ECAP...A combination of extrusion and equal channel angular pressing (ECAP) was used to deform a plain low carbon steel. This process consists of two successive deformations by extrusion and ECAP in a single die (Ex-ECAP). Cylindrical samples were heated to predefined temperatures (650 and 850 ℃) and then pressed through a die channel with crosshead speed of 10 mm/s. Microstructure and resultant mechanical properties of processed material were studied. The results showed that pressing temperature has a significant effect on the resultant microstructure. While at 650 ℃, the cold worked structure with elongated ferrite grains were obtained, and at 850 ℃ the microstructure consisted of elongated ferrite grains and very fine grains at their boundaries as a consequence of continuous dynamic recrystallization (CDRX) of ferrite phase. Also at 850 ℃, a particular microstructure consisted of cold worked ferrite and static recrystallized grains on shear bands was obtained.展开更多
The Mg96Y3Zn1 alloy processed by extrusion and equal channel angular pressing (ECAP) was investigated. It was found that the Mg96Y3Zn1 alloy processed by extrusion and ECAP obtained ultrafine grains and exhibited ex...The Mg96Y3Zn1 alloy processed by extrusion and equal channel angular pressing (ECAP) was investigated. It was found that the Mg96Y3Zn1 alloy processed by extrusion and ECAP obtained ultrafine grains and exhibited excellent mechanical properties. After ECAP, the average grain size of Mg96Y3Zn1 alloy was refined to about 400 nm. The highest strengths with yield strength of 381.45 MPa and ultimate tensile strength of 438.33 MPa were obtained after 2 passes at 623 K. The high strength of Mg96Y3Zn1 alloy was due to the strengthening by the grain refinement, the long period stacking (LPS) structure, solid solution, fine Mg24Y5 particles, and nano-scale precipitates. It was found that the elongation was decreased with pass number increasing. It was because that the cracks were preferentially initiated and propagated in the interior of X-phase during the tensile test.展开更多
基金This research did not receive any specific grant from funding agencies in the public,commercial,or not-for-profit sectors.
文摘Two severe plastic deformation(SPD)techniques of simple shear extrusion(SSE)and equal channel angular pressing(ECAP)were employed to process an extruded Mg-6Gd-3Y-1.5Ag(wt%)alloy at 553 K for 1,2,4 and 6 passes.The microstructural evolutions were studied by electron back scattered diffraction(EBSD)analysis and transmission electron microscopy(TEM).The initial grain size of 7.5μm in the extruded alloy was reduced to about 1.3μm after 6 SPD passes.Discontinuous dynamic recrystallization was suggested to be operative in both SSE and ECAP,with also a potential contribution of continuous dynamic recrystallization at the early stages of deformation.The difference in the shear strain paths of the two SPD techniques caused different progression rate of dynamic recrystallization(DRX),so that the alloys processed by ECAP exhibited higher fractions of recrystallization and high angle grain boundaries(HAGBs).It was revealed that crystallographic texture was also significantly influenced by the difference in the strain paths of the two SPD methods,where dissimilar basal plane texture components were obtained.The compression tests,performed along extrusion direction(ED),indicated that the compressive yield stress(CYS)and ultimate compressive strength(UCS)of the alloys after both SEE and ECAP augmented continuously by increasing the number of passes.ECAP-processed alloys had lower values of CYS and UCS compared to their counterparts processed by SSE.This difference in the mechanical responses was attributed to the different configurations of basal planes with respect to the loading direction(ED)of each SPD technique.
文摘A new severe plastic deformation(SPD)technique for improvement of the metallurgical properties of the magnesium alloys is presented.In this process,a cyclic extrusion compression angular pressing(CECAP)process is followed by an extrusion step in the outlet playing the role of additional back pressure.Therefore,more uniform and enhanced mechanical properties are expected in comparison with equal channel angular pressing(ECAP).In order to evaluate the effectiveness and capabilities of this new method,an AM60 magnesium alloy was processed.Finite element results exhibited a significant increase in strain values as well as uniform strain distribution for the new method.In addition,~110%increase in compressive stress was observed in new method compared to the conventional ECAP.Experimental results revealed a noticeable increase in the hardness and strength of the specimens processed by the new technique as a result of the formation of finer grains and more homogeneous microstructure with good distribution of refinedβ-phase along the boundaries.It may be concluded that the new process is very promising for future magnesium alloy products.
基金This project is supported by National Science Foundation of China for Distinguished Young Scholars (No. 50225518)Foundation of China for Key New Product (No. 2004ED850025)Post-Doctoral Foundation of China Heavy Machinery Research Institute (No. K055412).
文摘A modem design method, in which traditional design formulas are conjoined with numerical simulation and optimization, is successfully used to design the out-size extrusion flame precisely so that the press cost can be saved. A new technology used for decompressing by a multi-steps dynamical mode is put forward, which makes it possible to decompress the large flow-volume high-pressure oil in the main cylinders. In addition, a method for realizing the fixed mandrel process by hydraulic support is proposed and its control equation is established. Pre-tightening frame tests are carried out by over-operating pressure on 100 MN aluminium extrusion press with oil-driven double action, which is developed based on the above key techniques and is the largest press so far in the world, and the results show that the frame structure designed is reasonable and reliable, and the modem design method used is an useful tool for designing large and out-size heavy plastic forming machinery. The results of decompressing curve in main cylinder and noise inspection indicate that multi-steps dynamical mode for decompressing the large flow-volume high pressure oil is valid and reliable. Meanwhile, the fixed mandrel process is well realized based on the control equation. These key techniques have been used in the development of 125 MN aluminium extrusion press with oil-driven double action.
基金Projects (50201005, 50571031) supported by the National Natural Science Foundation of ChinaProject (2009DFA51830) supported by the Program for International Science and Technology Cooperation Projects of China
文摘The microstructures and properties of ZK60 alloy were evaluated under four different conditions: extrusion; extrusion and 4 passes of equal channel angular pressing (ECAP); extrusion, 4 passes of ECAP and secondary extrusion; and extrusion, 4 passes of ECAP, annealing and secondary extrusion. Secondary extrusion at ambient temperature was successfully processed to produce ultrafine-grained ZK60 alloy. The results show that ECAP introduces significant grain refinement and there is additional refinement in secondary extrusion. High yield strength of 342 MPa is achieved after secondary extrusion at room temperature, but the elongation to failure is only 0.8%. However, by applying annealing before secondary extrusion, the ductility of ZK60 could be greatly improved to 4.5%, meanwhile the yield strength almost remains the same, and the ultimate strength of up to 388 MPa is obtained.
文摘Rigid-viscoplastic3D finite element simulations(3D FEM)of the equal channel angular pressing(ECAP),thecombination of ECAP+extrusion with different extrusion ratios,and direct extrusion of pure aluminum were performed andanalyzed.The3D FEM simulations were carried out to investigate the load-displacement behavior,the plastic deformationcharacteristics and the effective plastic strain homogeneity of Al-1080deformed by different forming processes.The simulationresults were validated by microstructure observations,microhardness distribution maps and the correlation between the effectiveplastic strain and the microhardness values.The3D FEM simulations were performed successfully with a good agreement with theexperimental results.The load-displacement curves and the peak load values of the3D FEM simulations and the experimentalresults were close from each other.The microhardness distribution maps were in a good conformity with the effective plastic straincontours and verifying the3D FEM simulations results.The ECAP workpiece has a higher degree of deformation homogeneity thanthe other deformation processes.The microhardness values were calculated based on the average effective plastic strain.Thepredicted microhardness values fitted the experimental results well.The microstructure observations in the longitudinal andtransverse directions support the3D FEM effective plastic strain and microhardness distributions result in different formingprocesses.
基金Funded by Open Foundation of State Key Laboratory of AdvancedTechnologyfor Materials Synthesis and Processing, Wuhan Universi-ty of Technology, the Post PhD Science Foundation of China(2003034504) andthe Foundation of Wuhan University of Technol-ogy(2003XJJ202)
文摘The rods that were shaped from nanocrystalline WC- 10.21 Co-0.42 VC/ Cr3 C2 ( wt% ) composite powders by using powder extrusion molding (PEM) were investigated. The nanocrystalline WC- 10.21 Co- 0. 42 VC/ Cr3 C2 ( wt% ) composite powders were prepared by the spray thermal decomposition-continuous reduction and carburization technology. In order to improve the properties of rods shaped by using powder extrusion molding, the cold isostatic pressing (CIP) technology was used before or after debinding. Specimens were siutered by vacuum siutering and hot isostatic pressing (HIP). The density, Rockwell A hardness, magnetic coercivity , and magnetic saturation induction of siutered specimen were measured. The microstructure of the green bodies and the siutered specimens was studied by scanning electron microscopy (SEM). Results show that the rod formed by using powder extrusion molding after debinding and followed by cold isostatic pressing can be siutered to 99.5% density of composite cemented carbide rods with an average grain size of about 200- 300 nm, magnetic coercivity of 30.4 KA / m, Rockwell A hardness of 92.6 and magnetic saturation induction of 85% . Superfine WC- 10 Co cemented carbide rods with excellent properties were obtained.
基金Project(CSTC2007AA4008)supported by the Scientific and Technological Project in Chongqing of China
文摘The micro orientation theological behavior of AZ61 Mg alloy during net-shape forming of tensile specimens via close-die pressing of extruded preformed and the effect of the press deformation rate on the microstructure characteristics were characterized with electron back-scattering diffraction(EBSD)orientation imaging microscopy and metallography.The results indicate that the intensity distribution of basal{0001}<1010>texture on the cross-section of the extruded perform is uniform and parallel to the extrusion direction.Subjected to pressing in extrusion direction,deformation shear stress leads to grain rotation and basal texture {0001}<1010>deviation from the extrusion direction,spreading in the direction perpendicular to pressing direction.The texture intensity increases with the press deformation rate and reaches its peak value at 50%,which is considerably lower than the value reached in extrusion deformation.Then,the texture intensity decreases with the press deformation rate reversely.
基金Funded by the National Natural Science Foundation of China(No.41305124)the Natural Science Foundation of Shandong Province,China(No.ZR2021ME182)State Key Laboratory of Materials Processing and Die&Mould Technology Foundation(P12)
文摘The deformation behavior of equal channel angular pressing(ECAP)was discussed by using plasticity method.The node mapping method is employed to realize the analysis of multi-pass ECAP by using three-dimensional FEM methods for pure aluminum.The single-pass ECAP is a non-uniform shear deformation process in the cross-section of the workpiece.The uniform deformation processing routes are obtained during multi-pass ECAP process.In addition,the density of dislocations and defects of crystal lattice are also largely changed for different processing routes.The grain microstructure is gradually refined with the increase of the pressing passes.The grains and their distribution obtained by route Bc are more useful for producing the material with high angle grain boundaries.The grain microstructure of the cross section of the pressed material decreases with the increase of strain,and some grains exhibit transformed grain boundary(PTB)fringes.The dislocation density in the grain decreases,and the grain boundary presents equiaxed distribution.
文摘A combination of extrusion and equal channel angular pressing (ECAP) was used to deform a plain low carbon steel. This process consists of two successive deformations by extrusion and ECAP in a single die (Ex-ECAP). Cylindrical samples were heated to predefined temperatures (650 and 850 ℃) and then pressed through a die channel with crosshead speed of 10 mm/s. Microstructure and resultant mechanical properties of processed material were studied. The results showed that pressing temperature has a significant effect on the resultant microstructure. While at 650 ℃, the cold worked structure with elongated ferrite grains were obtained, and at 850 ℃ the microstructure consisted of elongated ferrite grains and very fine grains at their boundaries as a consequence of continuous dynamic recrystallization (CDRX) of ferrite phase. Also at 850 ℃, a particular microstructure consisted of cold worked ferrite and static recrystallized grains on shear bands was obtained.
基金Project supported by the National Natural Science Foundation of China (51001072)
文摘The Mg96Y3Zn1 alloy processed by extrusion and equal channel angular pressing (ECAP) was investigated. It was found that the Mg96Y3Zn1 alloy processed by extrusion and ECAP obtained ultrafine grains and exhibited excellent mechanical properties. After ECAP, the average grain size of Mg96Y3Zn1 alloy was refined to about 400 nm. The highest strengths with yield strength of 381.45 MPa and ultimate tensile strength of 438.33 MPa were obtained after 2 passes at 623 K. The high strength of Mg96Y3Zn1 alloy was due to the strengthening by the grain refinement, the long period stacking (LPS) structure, solid solution, fine Mg24Y5 particles, and nano-scale precipitates. It was found that the elongation was decreased with pass number increasing. It was because that the cracks were preferentially initiated and propagated in the interior of X-phase during the tensile test.