Various parameters in spark plasma sintering(SPS),such as sintering temperature,holding time,heating rate,and pressure,were adopted to investigate their effects on the densification of pure SnO2 power.The obtained e...Various parameters in spark plasma sintering(SPS),such as sintering temperature,holding time,heating rate,and pressure,were adopted to investigate their effects on the densification of pure SnO2 power.The obtained experimental data show that the SPS process enhances densification.The high-density undoped SnO2 ceramics (96.6% of theoretical) was obtained at much lower temperature (1000℃),within a much shorter time,compared to the conventional sintering process.The high-density undoped SnO2 ceramics (96.6% of theoretical) were obtained by SPS,under the condition of temperature:1000℃,pressure:40MPa,heating-rate:200℃/min,and holding time:3min展开更多
基金Funded by the Program for Innovation Team in Hubei Province(No.2008CDA011)
文摘Various parameters in spark plasma sintering(SPS),such as sintering temperature,holding time,heating rate,and pressure,were adopted to investigate their effects on the densification of pure SnO2 power.The obtained experimental data show that the SPS process enhances densification.The high-density undoped SnO2 ceramics (96.6% of theoretical) was obtained at much lower temperature (1000℃),within a much shorter time,compared to the conventional sintering process.The high-density undoped SnO2 ceramics (96.6% of theoretical) were obtained by SPS,under the condition of temperature:1000℃,pressure:40MPa,heating-rate:200℃/min,and holding time:3min